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《Journal of Inner Mongolia University》 2010-01
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Determination of Metacycline Based on the SOR Fluorescent Microscopic Technique

YANG Le1,LIU Ying1,2 (1.College of Life and Environmental Science,Minzu University of China,Beijing 100081,China;2.College of Chemistry and Environmental Science,Inner Mongolia Normal University,Hohhot 010022,China)  
The self-ordered ring(SOR) fluorescent microscopic technique is applied to the determination of metacycline based on the capillary effect of solvent on solid supports.In the presence of NH3-NH4Cl buffer solution(pH 10.60) and PVA-124,the droplet of metacycline can form an SOR on the solid supports with the diameter of 1.84 mm and its ring belt width of 59.6 μm.The quantitative analysis of metacycline is achieved with the linear range of 3.39×10-13~2.03×10-12 mol·ring-1(1.13×10-6~6.77×10-6 mol·L-1) and detection limit(3σ) of 1.05×10-13 mol·ring-1(3.50×10-7 mol·L-1) when 0.30 μL droplet was spotted.The technique has been applied to the determination of metacycline in the tablets and residue in four different milk samples with the recoveries of 95.2%~106% and 94.7%~104%,respectively.This technique provided a new way for analysis of medicine and determination of antibiotic residues in food,which shows several advantages such as lower background interference,less consumption,simplicity,non-pollution to the environment,etc.
【Fund】: 国家自然科学基金(20767004);; 中央民族大学“985工程”项目(MUC985);; 中央民族大学“211工程”项目(MUC021211306);; 中央民族大学引进人才启动基金;; 内蒙古自治区自然科学基金重点项目(200711020202);; 内蒙古自治区高等学校科学研究项目(NJ06108)资助
【CateGory Index】: S859.84
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