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《Journal of Inner Mongolia University》 2010-01
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Determination of Metacycline Based on the SOR Fluorescent Microscopic Technique

YANG Le1,LIU Ying1,2 (1.College of Life and Environmental Science,Minzu University of China,Beijing 100081,China;2.College of Chemistry and Environmental Science,Inner Mongolia Normal University,Hohhot 010022,China)  
The self-ordered ring(SOR) fluorescent microscopic technique is applied to the determination of metacycline based on the capillary effect of solvent on solid supports.In the presence of NH3-NH4Cl buffer solution(pH 10.60) and PVA-124,the droplet of metacycline can form an SOR on the solid supports with the diameter of 1.84 mm and its ring belt width of 59.6 μm.The quantitative analysis of metacycline is achieved with the linear range of 3.39×10-13~2.03×10-12 mol·ring-1(1.13×10-6~6.77×10-6 mol·L-1) and detection limit(3σ) of 1.05×10-13 mol·ring-1(3.50×10-7 mol·L-1) when 0.30 μL droplet was spotted.The technique has been applied to the determination of metacycline in the tablets and residue in four different milk samples with the recoveries of 95.2%~106% and 94.7%~104%,respectively.This technique provided a new way for analysis of medicine and determination of antibiotic residues in food,which shows several advantages such as lower background interference,less consumption,simplicity,non-pollution to the environment,etc.
【Fund】: 国家自然科学基金(20767004);; 中央民族大学“985工程”项目(MUC985);; 中央民族大学“211工程”项目(MUC021211306);; 中央民族大学引进人才启动基金;; 内蒙古自治区自然科学基金重点项目(200711020202);; 内蒙古自治区高等学校科学研究项目(NJ06108)资助
【CateGory Index】: S859.84
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Chinese Journal Full-text Database 6 Hits
1 Wang Lei, Xu Zhixiu, Zhang Xiaosong, Shao Xueguang * (Department of Chemistry, University of Science and Technology of China, Hefei 230026);Rapid Determination of 7 Tetracyclines by Reversed Phase High Performance Liquid Chromatography[J];Chinese Journal of Analytical Chemistry;2003-01
2 Long Liping 1, Wang Kemin 2, Yang Ronghua 2, Yang Xiaohai 2 1 (Department of Chemistry & Environmental Engineering, Hunan City College, Yiyang 413049) 2 (College of Chemistry & Chemical Engineering, Hunan University, Changsha 410082);A Picric Acid Optical Chemical Sensor Based on Fluorescence Quenching[J];Chinese Journal of Analytical Chemistry;2003-04
3 JIA Yannan,WEN Xianghua,LI JiaxiState Key Laboratory of Environmental Simulation & Pollution Control,Department of Environmental Science and Engineering,Tsinghua University,Beijing 100084;A feasibility study on the degradation of tetracycline by ligninolytic enzymes[J];Acta Scientiae Circumstantiae;2008-01
4 ZHANG Hao1, LUO Yi1, ZHOU Qi-xing1,2 (1.Key Laboratory of Pollution Process and Environmental Criteria at Ministry of Education, College of Environmental Science and Engineering, Nankai University,Tianjin 300071,China; 2.Key Laboratory of Terrestrial Ecological Process, Institute of Applied Ecology,Chinese Academy of Sciences, Shenyang 110016, China);Research Advancement of Eco-toxicity of Tetracycline Antibiotics[J];Journal of Agro-Environment Science;2008-02
5 Si-qin,Aodeng Gaowa,LI Hu-dong (College of Chemistry and Chemical Engeneering,Inner Mongolia University,Hohhot 010021,China);Simultaneous Spectrophotometric Determination of Tetracycline,Oxytetracycline and Metacycline by Partial Least Squares Method[J];Journal of Inner Mongolia University(Acta Scientiarum Naturalium Universitatis NeiMongol);2007-01
6 Li Zhao Wang Zunben(Dept. of Chem.,The Res.Lab. of SEDC of Anal.Sci.for Material and Life Chem. Xiamen Univ.,Xiamen 361005);Study on Chemiluminescence Method for Oxytetracycline,Methacycline and Deoxycycline[J];JOURNAL OF XIAMEN UNIVERSITY(NATURAL SCIENCE);1998-04
Chinese Journal Full-text Database 10 Hits
1 LIU Ran, ZHOU Li, YANG Mei(College of Chemistry and Chemical Engineering,Liaoning Normal University,Dalian Liaoning 116029,China);Study of a Fluoride-selective Sensing Membrane Based on Fluorescence Quenching[J];Journal of Anshan Normal University;2005-02
2 MU Hong-sheng1,LI Xiao-mei2,QI Zhen-xiong3,LI Xu-e1 1.College of Life Sciences,South China Normal University,Guangzhou 510631,China;2.College of Life Sciences,Guangzhou University,Guangzhou 510006,China;3.Haida Research Center of Livestock Husbandry and Fisheries in Guangdong,Guangzhou 511400,China);Application of Chinese Herb Medicines in Therapeutic Treatments of Parasitic Fish Diseases[J];Fisheries Science;2008-11
3 XING Chun-yong,SUN Xiao-ai,GAO Min,ZHANG Wen-qin(Department of Chemistry,School of Science,Tianjin 300072,china);Simple Total Synthesis of 1-Carbethoxy-2-Methyl-4-Piperidone[J];Information Recording Materials;2009-01
4 KUANG Hua,ZHANG Ji-zhen,JIA Hong-bin,ZHAO De-jian,WANG Ya-zhen(School of Chemistry and Chemical Engineering,Jiangsu Teachers University of Technology,Changzhou 213001,China);Teaching Reform Attempt of Organic Chemistry[J];Journal of Jiangsu Teachers University of Technology;2007-04
5 Zhao Pei-jin~1,Jia Fang~2 (1 Cangzhou Medical College,Cangzhou 061001,China; 2 Cangzhou Entry-Exit Inspection and Quarantine Bureau,Cangzhou 061001,China);The Preparation of Microcapsule Tetracycline and Their Performance Parameters' Evaluation[J];Chinese Journal of Medicinal Guide;2008-08
6 WANG Ming-hua1,ZHENG Jun-sheng2,LUO Yun-peng3,MI Can1(1Department of Pathology,3Department of Pathophysiology,Faculty of Basic Medical Sciences,Chongqing Medical University,Chongqing 400016;2Department of Gynaecology and Obstetrics,The Third Affiliated Hospital of Sun Yat-sen University,Guangzhou 510630,China);Growth inhibition effects of artesunate on human cervical cancer cell line HeLa[J];Acta Academiae Medicinae Militaris Tertiae;2008-18
7 LI Chao~1,LIU Shu-yuan~1,LI Yuan-yuan~1,DUAN Hong-wei~2(1.School of Chemistry & Chemical Engineering,Jinan University,Jinan 250022,China;2.Shdndong FLIO Environmental Engineering,Jinan 2500101,China);The Development of Chemiluminescence and Their Application[J];Analysis and Testing Technology and Instruments;2006-02
8 CHAI Yi-feng, WU Yu-tian and LI Xiang(Department of Pharmaceutical Analysis, College of Pharmacy, Second Military Medical University, Guohe Road 325, Shanghai 200433), Fenxi Shiyanshi,2004,23(6):71~92;Pharmaceutical Analysis I[J];Analytical Laboratory;2004-06
9 WU Ting1,WANG Chao2 and LI Nan*1(1.College of science,China Agricultural University,Beijing 100094;2.Chinese Academy of Inspection and Quarantine,Beijing 100025),Fenxi Shiyanshi,2007,26(8): 52~55;Study on simultaneous detection of 9 tetracyclines residues in cosmetics by high performance liquid chromatography[J];Chinese Journal of Analysis Laboratory;2007-08
10 LIU Jie,LIU Yan-mei and ZHANG Yong(School of Chemistry and Chemical Engineer,Shanxi University,Taiyuan 030006);Study on electrochemical behaviors and analytical application of doxorubicin hydrochloride at a glassy carbon electrode[J];Chinese Journal of Analysis Laboratory;2008-06
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 Gao Junmin,Zhen Zegen,Wang Yan (College of Municipal Construction & Environmental Engineering,Chongqing University,Chongqing,400045);Study of TiO_2/ZnO Composite Catalyst Photodegradation of Tetracycline[J];Chongqing Environmental Science;2003-01
2 GAO Li-hong~(1),AO Lin~(1),HU Ran~(1),LIU Jin-yi~(1),HUANG Ming-hui~(2),YANG Meng-su~(2),CAO Jia~(1)(~(1)Department of Hygiene Toxicology,College of Preventive Medicine,Third Military Medical University,Chongqing 400038,~(2)Genome Technological Application Institute,City University of Hong Kong);Gene expression profiles of toxicated BALB/c mouse liver exposed to tetracycline[J];Acta Academiae Medicinae Militaris Tertiae;2006-06
3 Pan Jinghao He Mingwei Liu Yanmin (Department of Chemistry,Shanxi University);A Good PVC Matrix Membrane Picrate Ion-selective Electrode[J];Chinese Journal of Analytical Chemistry;1983-07
4 ZHANG Li qing *1 ,WU Xiao hua 2, TANG Xi 1, ZHU Xian liang 1,SU Wen ting 2 (1.The Department of Biological and chemistry Engineering, Zhejiang University of Science and Technology, Hangzhou, 310012; 2.Department of Chemical, Zhejiang Uni;Simultaneous Spectrophotometric Determination of Five-Components in Cough Syrup by Partial Least Squares[J];Journal of Analytical Science;2002-04
5 Lu Jixin (Department of Pharmacy, Tianjin Medical University, Tianjin, 300203) Zhao Peng, Zhang Guizhu, Sun Ying, Wang Yuemei, He Xiwen, Shi Huiming (Department of Chemistry, Nankai University, Tianjin, 300071);Study on the State Medicine of the Tracy Antibiotic in Body[J];JOURNAL OF ANALYTICAL SCIENCE;1998-01
6 Lu Jixin ,Li Juan (Department of Pharmacy,Tianjin Medical University,Tianjin 300203), Zhang Guizhu ,Sun Ying,Wang Yuemei,He Xiwen and Shi Huiming (Department of Chemsitry,Nankai University,Tianjin 300071);Determination of Tetracycline Type Antibiotics by Molybdenum and Europium Complex[J];ANALYTICAL LABORATORY;1997-06
7 ZENG Hui-Hui , WANG Ke-Min, QIN Zhen, YU Ru-Qin (Department of Chemistry and Chemical Engineering, Htman University, Changsha, 410082);A Sulphur Dioxide-Selective Sensing Membrane Based on Fluorescence Quenching[J];Chemical Research In Chinese Universities;1993-02
8 GUO Mei-ting,HU Hong-ying,WANG Chao(ESPC State Key Joint Laboratory,Department of Environmental Science and Engineering,Tsinghua University,Beijing!100084,China);Pharmaceuticals and Personal Care Products in Urban Sewage and Their Removal Characteristics[J];China Water & Wastewater;2005-10
9 ZHANG Yan-fang, LI Hua-zhong, HUA Zhao-zhe, CHEN Jian (Key Laboratory Industrial Biotechnology, Ministry of Education, Biotechnology School, Southern Yangtze University, Wuxi, Jiangsu 214036, China);Roles of Lignin Peroxidase, Manganese Peroxidase and Pellet of Phanerochaete chrysosporium in Decoloration of Dyes[J];The Chinese Journal of Process Engineering;2002-03
10 Lin Gang Wen Xianghua Qian Yi (ESPC, Department of Environmental Science and Engineering, Tsinghua University, Beijing 100084);The study progress on using white-rot fungus in treating refractory organics[J];Technigues and Equipment For Enviro.poll.cont;2001-04
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