Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Journal of Qingdao University of Science and Technology》 2003-06
Add to Favorite Get Latest Update

Study on Quick Detecting Pesticides Multi-residue in Vegetables and Fruits by GC-MS

LIU Yong-bo 1,2 ,JIA Li-hua 2,NIU Shu-yan 1 (1. College of Chemistry and Molecular Engineering, Qingdao University of Science and Technology, Qingdao 266042,China; 2.Qingdao Municipal Drainage Monitoring Center,Qingdao 266002,China)  
A method for detectimg 48 pesticide residues in fruits and vegetables was studied. The detection was performed by SIM-GC-MS technique. Pesticides were positively confirmed by retention times and ion ratios.This method can be used to detect 48 pesticides including organophosphorus,organochlorines, pyrethroids and carbamates in farm products such as fruits and vegetables. The limit of detection ranges from 2.0×10 -10 -2.0×10 -7 (μg·g -1 ) depending on the different pesticides.
【CateGory Index】: O657.63
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
Chinese Journal Full-text Database 10 Hits
1 DING Yi1,NI Xiao-dong2,LI Fei-hong2,LIU Xiao-ying2 (1.Modern Experiment and Tachnology Center,Anhui University, Hefei 230039,China; 2.School of Life Science,Anhui University,Hefei 230039;China);GC-MS analysis for organophosphorus pesticides residues in vegetables[J];Journal of Anhui University(Natural Sciences);2005-03
2 SHI Zheng,HUANG Kaifeng(School of Life Sciences,Guizhou Normal University,Guiyang,Guizhou 550001);Progress of Pesticides Residues in Vegetable[J];Journal of Changjiang Vegetables;2011-04
3 He Yu Chen Jinquan Zhang Lan (Key Laboratory Analysis and Detection Technology for Food Safety,Ministry of Education.The Sport Science Research Center,Fuzhou University,Fuzhou,350002.CHINA);Study of techniques about preparation to the organophosphorus pesticides in foods[J];Fujian Analysis & Testing;2007-03
4 WAN Zheng-kai,HE Juan,KANG Chang-an,LU Kui(The School of Chemistry and Chemical Engineering,Henan University of Technology,Zhengzhou 450052,China);Application and Update Progresses of GC-MS in Determination of Pesticide Residues[J];Analysis and Testing Technology and Instruments;2006-01
5 Fu Ruo-nong(Department of Chemistry Beijing Institute of Technoligy, Beijing 100081);Advances on gas chromatography in China in recent two years(Ⅱ)[J];Analytical Laboratory;2005-05
6 ZHAO Hai-Feng~(1,2),WANG Jian-Hua~(1,3),BING Xin~1,RU Shao-Guo~1(1.Ocean University of China,Qingdao 266003,China;2.Chengyang Agriculture Bureau,Qingdao 266109,China;3.Qingdao Exit-Entry Inspection and Quarantine Bureau,Qingdao 266002,China);An Improvement on the GC-MS Method for Vegetable Pesticide Residues Analysis and Discussion of Matrix Effects[J];Periodical of Ocean University of China;2006-01
7 FANG Haojie1,2(1.Technical Center of Shanghai Electric Environmental Protection Group,Shanghai 201108,China;2.Shanghai Environmental Protection Engineering Whole Sets Co.,Ltd.,Shanghai 201108,China);Recent Researches and Developments in the Field of Soil Pollution and Test Facility[J];Journal of Shanghai Electric Technology;2010-02
8 TONG Ling,YANG Jiajia,WU Shuqi( National Research Center for Geoanalysis,Beijing 100037,China );Sample pretreatment for determination of chlorinated organic pollutants in plants by gas chromatography and gas chromatography-mass spectrometry[J];Chinese Journal of Chromatography;2011-03
9 ZHANG Juan-qin;YUAN Da-wei;ZHENG Xian-qing;LI Shuang-xi;HE Qi-yong;LU Wei-guang;Eco-Environment and Plant Protection Research Institute,Shanghai Academy of Agricultural Sciences,Observation and Experiment Station of Agricultural Environment and Farmland at Shanghai,Ministry of Agriculture,Shanghai Key Lab of Protected Horticultural Technology,Shanghai Agricultural Environment Protection and Monitoring Station;;Research advances in analytical techniques of agricultural products' pesticide residues[J];Acta Agriculturae Shanghai;2013-03
10 QIAN Min1,LIU Jian-zhen2,BAI Wei-dong1,CAI Pei-dian1(1.College of Light Industry and Food,Zhongkai University of Agricultural and Engineering,Guangzhou 510225,China;2.Yingde Vocational & Technical School,Yingde 513000,China);The application of GC-MS on food industry[J];China Condiment;2009-09
Chinese Journal Full-text Database 1 Hits
1 Zhuang Wuji(China Import and Export Commodity Inspection Technology Institute,Beijing,100025)ZhouYu;Liu Shengli(Xiamen Import and Export Commodity Inspection Bureau,Xiamen,361012);A Method for Determination of 22 Organophosphorus Pesticides Residue in Fruits and Vegetables by Capillary Gas Chromatography[J];JOURNAL OF INSTRUMENTAL ANALYSIS;1995-03
Chinese Journal Full-text Database 10 Hits
1 WU Li-hua,LI Jian-ke~* and WU Xiao-hong(Department of Food Engineering,Shanxi Normal University,Xi′an 710062);Determination of multi-pesticide residues in applies by gas chromatography[J];Chinese Journal of Analysis Laboratory;2006-11
2 WU Yu Jie HUANG Zhi Qiang a MA Ming ZHANG Ying a (College of Chemistry and Chemical Engineering,Hunan Normal University,Changsha 410081,P.R.China) a(College of Chemistry and Chemical Engineering,Hunan University,Changsha 410081,P.R.China);Determination of Methamidophos Pesticide Residues in Allium Chinense by Gas Chromatography[J];Chinese Journal of Spectroscopy Laboratory;2004-02
3 ZHOU Zhao-ting,YUAN Jin-peng,YU Tian-hua (1.Yantai Non-Contaminateds Vegetable Supervision Center,Yantai 264000,China;2.Shandong Analysis and Test Center,250014,China;3.Yantai RunCang Corp. Limit,Yantai 264000,China);Determination of residues of pesticides in vegetables with Gas Chromatography spectrometry[J];Shandong Science;2005-04
4 Wu YuJie1,Wou Weiyuan1,Huang Zhiqiang2,Zhang Ying2,Liu Junyi1(1 Guangxi Entry-Exit Inspection and Quarantine Bureau,Nanning 530021,China;2 Hunan Entry-Exit Inspection and Quarantine Bureau,Changsha 410008,China);Research on determination of organophosphorus pesticides residues in tea by gas chromatography[J];Journal of Food Safety & Quality;2010-01
5 PAN Canping, WANG Limin, KONG Xiangyu, JIANG Shuren, QIAN Chuanfan (Department of Applied Chemistry, China Agricultural University, Beijing 100094 , China);Determination of 15 Organophosphorus Pesticides in Cucumber, Tomato and Pepper Samples by Capillary Gas Chromatography with Gel Permeation Chromatographic Clean-up[J];Chinese Journal of Chromatography;2002-06
6 WU Ri-na~1,LI Jian-ke~1,QIU Nong-xue~1,WANG Ping~2,FANG Sheng~2,Shu Ning~1(1 Department of Food Engineering,Shaanxi Normal University,Xi′an 710062,Shaanxi,China;2 Shaanxi Hengxing Fruit Juice Company Limited,Meixian 722300,Shaanxi,China);Residual distribution tendency of methamidophos pesticides in apples[J];Journal of Shaanxi Normal University(Natural Science Edition);2006-01
7 TAN Lei,ZHAN Yan,XU Chao-qun(Sichuan Academy of Chinese Medicine Sciences,Chengdu 610041,China);Determination of organochlorine, pyrethroid and organophosphate pesticides in angelica by GC/MS coupled with SPE[J];China Measurement & Test;2010-05
8 LI Jian-qiang 1 ,JI Yu-ying 2(1.State Assets Department,Tangshan Teachers College,Hebei Tangshan 063000,China;2.No.26 Middle School of Tangshan,Hebei Tangshan 063000,China);Study on Condition of Pesticide Residiues at the Present[J];Journal of Tangshang Teachers College;2005-02
9 WANG Jian-hua,LI Guang-ling and CHEN Xi-ling (Henan Institute of Science and Technology,Xinxiang Henan 453003,China);The Analysis of Amitraz and Buprofezin Residues in Chinese Green Cabbage[J];Acta Agriculturae Boreali-Occidentalis Sinica;2008-04
10 yan Bo Shi Changyun Li Ye, et al;Determination of Pesticide Residues in Cabbages[J];Instrumentation . Analysis . Monitoring;2005-03
Chinese Journal Full-text Database 10 Hits
1 WAN Yu Anhui Research Institute of Chemical Industry,Hefei 230041,China;The New Development of Sampling Preparation Technique in Pesticide Residue Analysis[J];Anhui Chemical Industry;2006-02
2 TAI Hai-jun,ZHU Chuan-ming(1.Anhui Institute of Product Quality Supervision & Inspection,Hefei 230051,China;2.Anhui Center of Chemical Product Quality Supervision & lnspection,Hefei 230041,China);Determination of 10% Cyhalofop-butyl EC by RP-HPLC[J];Anhui Chemical Industry;2010-02
3 ZHANG Jin1,YAN Shu-jun2(1.Department of Environmental Engineering,Anhui University of architecture,Hefei 230022,China;2 Anhui Honglu Steel Construction(Group) Co.,Ltd.,Hefei 231131,China);Development of effect of factors on the leaching and movement of pesticides in soil[J];Journal of Anhui Institute of Architecture & Industry(Natural Science);2008-04
4 Li Jiajing Zhang Weifeng Hong Zhentao(Guangzhou AgricuLturaL Standard and Supervisory Center,Guangzhou,Guangdong,P.R.510308);Determination of Organophosphorous Pesticide Residues in Vegetable by Solid-Phase Extraction-Gas Chromatography[J];Anhui Agricultural Science Bulletin;2007-13
5 Huang Dezhi et al (Teaching Affairs Office, Anhui Agricultural University, Hefei 230036);Research Progress of Analysis of Pesticide Residue[J];Journal of Anhui Agricultural Sciences;2002-04
6 Huang Dezhi et al (Anhui Agricultural University, Hefei,Anhui 230036);Purification, Titration and Identification of Thibenuron-methyl as Standard Sample[J];Journal of Anhui Agricultural Sciences;2004-02
7 Jing Zuoliang et al (Tianjin University of Science and Technology,Tianjin 300222);Study on the Measurement of the Pesticide Residue in Crop[J];Journal of Anhui Agricultural Sciences;2004-05
8 DU Kun et al (Armed Police Engineering College,Xian,Shanxi 710086);Application of HACCP in Food Industry[J];Journal of Anhui Agricultural Sciences;2005-05
9 ZHANG Ning (Yibin College, Yibin, Sichuan 646007);Research on the Method of Rapid Testing for Organic Phosphorus Pesticides Residue in Vegetable[J];Journal of Anhui Agricultural Sciences;2005-08
10 XIAO Jun et al(College of Tourism and Environment Science,Shanxi Normal University,Xian,Shanxi 710062);Influence and Countermeasures of Pesticide Pollution on the Eco-environment[J];Journal of Anhui Agricultural Sciences;2005-12
China Proceedings of conference Full-text Database 1 Hits
1 QIN Shu, QIAO Xiong-wu, WANG Xia, ZHOU Hua (Shanxi Key Laboratory of Pesticide Science & Institute of Plant Protection, Shanxi Academy of Agricultural Sciences, Taiyuan 030031, China);Detection of Pesticide Residues in Mulberry Leaf by Gas Chromatography-Mass Spectrometry[A];[C];2004
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 ZHANG Jun (Shenyang Testing Center of Agriculture, Shenyang, Liaoning 110034);Effects of Solvent Strength on the Recovery of Pesticide Residue[J];Journal of Anhui Agricultural Sciences;2008-08
2 ZHANG Jing et al(Shenyang University of Chemical Technology,Shenyang,Liaoning 110142);Determination of Five Kinds of Deltamethrin Pesticides Residue in Vegetables by GC/MS[J];Journal of Anhui Agricultural Sciences;2011-30
3 LIU Teng-fei 1 XIE Xiu-qing 1 LIU Wen-ting 2(1 School of Horiculture and Plant Protection,Yangzhou University,Yangzhou Jiangsu 225009;2 College of Enviromental Science and Engineering,Yangzhou University);Applications of GC and GC-MS in Pesticide Residue Analysis[J];Modern Agricultural Sciences and Technology;2010-03
4 CHEN Dong-lan XIA Tong WANG Zhi-bo ZHAN Jin-bo (Rugao Agricultural Product Quality Inspection and Testing Center in Jiangsu Province ,Rugao Jiangsu 226500);Overview and Comparison on Several Commonly Used Testing Technology of Pesticide Residue in Vegatables[J];Modern Agricultural Sciences and Technology;2010-09
5 SHI Zheng,HUANG Kaifeng(School of Life Sciences,Guizhou Normal University,Guiyang,Guizhou 550001);Progress of Pesticides Residues in Vegetable[J];Journal of Changjiang Vegetables;2011-04
6 LI Xiaoyu1,LIU Yaguang1,LI Ying2,HE Fuli1,TIAN Lijuan1,HAN Yujun1,TANG Guangshun1(1.College of Agriculture,Northeast Agricultural University, Harbin 150030,China;2.Long-Zhi Agricultural Corporation of Harbin,Harbin 150039,China);Optimization of affecting factors clomazone degradation in contaminated soil by degrading bacterium X[J];Journal of Northeast Agricultural University;2011-11
7 ZHENG Xiao-yan1,LU Wan-ping2,HUANG Hong-xia1,CHEN Jin-quan2,ZHANG Lan2(1Fu jian Provincial Central Inspection Institute,Fuzhou 350002,China;2.Instrumentation Analysis and Measurement Center of Fuzhou University Fuzhou 350002,China);Solid Phase Extraction GC Analysis of Phosphate Pesticide Residue in Vegetables and Fruits[J];Analysis and Testing Technology and Instruments;2009-03
8 YOU Fei-ming1,WU Fang2,LU Wan-ping2,ZHANG Qing2,Zhang Lan2 (1.Fujian Inspection and Research Institute for Product Quality,Fuzhou 350002,China; 2.Instrumentation Analysis and Measurement Center of Fuzhou University,Fuzhou 350002,China);Determination of Organophosphorus Pesticide Residues in Tea by Solid-phase Extraction Gas Chromatography[J];Analysis and Testing Technology and Instruments;2011-01
9 FU Ruo-nong(Department of Chemistry,Beijing Institute of Technoligy,Beijing 100081);Advances on SPE-chromatography in China in recent two years[J];Chinese Journal of Analysis Laboratory;2007-02
10 DAN De-zhong,YAO Yu-ling and JIANG Wen-jing(Department of Environmental Science and Engineering,Sichuan University,Chengdu 610065);Analysis of environmental samples[J];Chinese Journal of Analysis Laboratory;2008-04
China Proceedings of conference Full-text Database 3 Hits
1 Liu Wei,Li Zhiwen,Yu Fuli (Institute for the Control of Agrochemical,Shaanxi Province,Xian 710003);Development in the study on detection of pesticide residues[A];[C];2008
2 CUI Shu-hua 1*,GUO Qing-long 2,LIU Run-zhu 1,LIU Jing-jing 1,GONG Ping 1,ZHANG Xiao-mei 1 (1.Food and Agricultural Products Testing Agency,Shandong Entry-Exit Inspection and Quarantine Bureau,Qingdao 266002,China;2.Huangdao Entry-Exit Inspection and Quarantine Bureau,Qingdao 266555,China);Determination of 49 Bactericids Residues in Welsh Onion Strawberry GC-MS[A];[C];2012
3 ZHANG Xiao-mei *,LIU Jing-jing,GONG Ping,WANG Jian-hua,WANG Jing-tang (Shandong Entry-Exit Inspection and Quarantine Bureau,Qingdao 266700,China);Determination of 17 Pesticide Residues in Pet Food Using Gas Chromatography-Mass Spectrometry[A];[C];2012
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved