Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《High Power Laser and Particle Beams》 2013-08
Add to Favorite Get Latest Update

Preparation and characterization of polyhedral oligomeric silsesquioxane-zirconia aerogels

Huang Chuangchuang1,2,Wei Zhijun1,2,Zhang Lin1,Luo Xuan1,Ren Hongbo1,Luo Meiming2(1.Science and Technology on Plasma Physics Laboratory, Research Center of Laser Fusion,CAEP,Mianyang 621900,China; 2.College of Chemistry,Sichuan University,Chengdu 610064,China)  
The polyhedral oligomeric silsesquioxane(POSS)-zirconia aerogels which contain three different contents of zirconia were successfully prepared from the POSS-[C2H4Si(OEt)3]8 and Zr(OC4H9)4 by the sol-gel process and subsequently supercritical drying with carbon dioxide.Ethanol was used as the solvent during the process.The samples were characterized by FTIR,SEM,XRD and BET.The results indicate that the three samples all have homogeneous Si-O-Ti bonds,and they are amorphous.The BET surface areas decrease with the increasing of the contents of zirconia,the biggest surface area is 491 m2/g,and all the pore distributions of the three samples are broad.
【Fund】: 国家自然科学基金委员会-中国工程物理研究院联合基金项目(10976020);; 中国工程物理研究院科学技术发展基金项目(2012A032015 2012B032050)
【CateGory Index】: TL632
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 3 Hits
1 ;The Development of Aerogel Applications[J];Materials Review;1999-06
2 REN Hong-bo,WAN Xiao-bo,ZHANG Lin,YUAN Guang-hui,XIU Peng,ZHANG Yong (Research Center of Laser Fusion,CAEP,P.O.Box 919-987,Mianyang 621900,China);Preparation of modified silica aerogel and its appilication in inertial confinement fusion(ICF) experiment[J];High Power Laser and Particle Beams;2006-08
3 DENG Zhong sheng, WEI Jian dong, WANG Jue, SHEN Jun, ZHOU Bin, BAO Yu ping,CHEN Ling yan Pohl Institute of Solid State Physics,Tongji University,Shanghai, 200092 China;STRUCTURE AND VAPOR ADSORPTION OF LOW- DENSITY SILICA AEROGELS[J];HIGH POWER LASER & PARTICLE BEAMS;1999-02
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 Wu Zhijian (College of Materials Science and Engineering,Huaqiao University,Quanzhou 362011,P.R.China);Advances in Research on Inorganic Aerogels[J];Materials Review;2001-11
2 MAO Lingbo,ZHANG Renyuan(Faculty of Material and Energy,Guangdong University of Technology,Guangzhou 510090);Study on Preparation of Alumina Aerogel[J];Materials Review;2006-S2
3 XU Xiang,ZHOU Bin,LIU Chunze,ZHOU Changhe,SHEN Jun,WU Guangmin,XU Chao(Pohl Institute of Solid State Physics,Tongji University,Shanghai 200092);Research and Application Progress of Aerogel Used in ICF Experiments[J];Materials Review;2008-10
4 YIN Shuai1,WU Huijun1,2,DING Yunfei1,2,LIAO Yundan1(1 School of Civil Engineering,Guangzhou University,Guangzhou 510006;2 Guangdong Key Laboratory of Building Efficiency and Application Techniques,Guangzhou University,Guangzhou 510006);Advances in Ambient-dried Preparation and Applications of Hydrophobic SiO_2 Aerogels[J];Materials Review;2011-03
5 Li Jian,Wang Chengyu,Zhai Xianglin(Key Laboratory of Bio-based Material Science and Technology,Ministry of Education(Northeast Forestry University),Harbin 150040,P.R.China);Formation of Aerogel-type Wood[J];Journal of Northeast Forestry University;2008-11
6 Qiu Jian,Gao Jingran(Faculty of Wood Science and Decoration Engineering,Southwest Forestry University,Kunming 650224,P.R.China);Li Jian,Liu Yixing(Key Laboratory of Bio-Based Material Science and Technology,Ministry of Education(Northeast Forestry University));Theoretical analysis of Aerogel-type Wood Based on Natural Biological Structure[J];Journal of Northeast Forestry University;2008-12
7 Ren Hongbo, Du Kai, Zhang Lin, Wan Xiaobo, Zhang Yong (Research Center of Laser Fusion, Chinese Academy of Engineering Physics, Mianyang 621900, China);The Characterization of Hydrophobic Layer Thickness of Silica Aerogel by Means of SAXS[J];Rare Metal Materials and Engineering;2008-S2
8 LI Zhen-min1 JIA Qi2 LV Xu-liang2(1.Nanjing Engineer Quality Supervision Station,General Staff of PLA,Nanjing Jiangsu 210007 China;2.Engineering Institute of Engineer Corps,PLA Univ.of Sci.&Tech.,Nanjing Jiangsu 210007 China);Research on Development and Application in Building Energy-Saving of High Strength and High Thermal Resistant SiO_2-Areogel[J];Jiangsu Construction;2009-S1
9 REN Hong-bo,WAN Xiao-bo,ZHANG Lin,YUAN Guang-hui,XIU Peng,ZHANG Yong (Research Center of Laser Fusion,CAEP,P.O.Box 919-987,Mianyang 621900,China);Preparation of modified silica aerogel and its appilication in inertial confinement fusion(ICF) experiment[J];High Power Laser and Particle Beams;2006-08
10 ZHANG Yong~(1,2),REN Hong-bo~2,XU Jia-jing~2,DU Kai~2,ZHANG Lin~2,XIU Peng~2 (1.School of Material Science and Engineering,Southwest University of Science and Technology,Mianyang 621002,China;2.Research Center of Laser Fusion,CAEP P.O.Box 919-987,Mianyang 621900,China);Synthesis and characterization of MF aerogels[J];High Power Laser and Particle Beams;2006-11
【Secondary Citations】
Chinese Journal Full-text Database 3 Hits
1 ;Structure-controlled Nano-porous Aerogels[J];Materials Review;1997-04
2 DENG Zhong sheng, WEI Jian dong, WANG Jue, SHEN Jun, ZHOU Bin, BAO Yu ping,CHEN Ling yan Pohl Institute of Solid State Physics,Tongji University,Shanghai, 200092 China;STRUCTURE AND VAPOR ADSORPTION OF LOW- DENSITY SILICA AEROGELS[J];HIGH POWER LASER & PARTICLE BEAMS;1999-02
3 DENG Zhong-Sheng, WEI Jian-Dong, Wu Ai-Mei, BAO Yu-Ping; WANG Jue; SHEN Jun; ZHOU Bin; CHEN Ling-Yan (1. Pohl Institute of Solid State Physics, Tongji University, Shanghai 200092, China; 2. Shanghai Institute of Chemical Engineering, Shanghai 200062, Chi;Hydrophobic Sio_2 Aerogels Prepared with Polyethoxydisiloxanes[J];JOURNAL OF INORGANIC MATERIALS;2000-02
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved