Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Journal of Synthetic Crystals》 2009-05
Add to Favorite Get Latest Update

Study on Size Modulation Effects of Ethanol/Water System and Molten Salts Media in Preparing ZnO Nanoparticles

FENG Xin1,SHI Li-yi1,2,SHI Wen1,ZHANG Jian-ping2,FANG Jian-hui2,MA Shu-rui2 (1.Nano-Science and Technology Research Center,Shanghai University,Shanghai 200444,China;2.Department of Chemistry,College of Science,Shanghai University,Shanghai 200444,China)  
ZnO nanoparticles were synthesized by liquid phase method. The size control effects of Ethanol/Water solvents used in precipitation and the molten alkali salts in calcination were investigated. The products were charaterized by XRD,TEM,BET and PL. The results indicated that particle size decreased in the assisted calcination with NaNO3 and LiNO3 salts. With the same addition amount,the particle size obtained with LiNO3 was smaller than the former. And the size decreased obviously when the ratio of ethanol to water changed from 1∶1 to 3∶1. Finally,the mechanisms of ethanol/water mixed system and molten salts media were also disscussed.
【Fund】: 国家高技术研究发展计划(863)项目(No.2007AA03Z335);; 上海市科委学科带头人计划(No.07XD14014);; 上海高校选拔培养优秀青年教师科研专项基金(No.SHU-07051);; 教育部科学技术研究重点项目(No.208182)
【CateGory Index】: TB383.1
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 2 Hits
1 LI Xuedong,ZHU Boquan,WANG Houzhi(Hubei Province Key Laboratory of Ceramics and Refractories, Wuhan University of Science and Technology, Wuhan 430081);Application of Molten Salt Method in Preparation of Inorganic Material Powders[J];Materials Review;2006-03
2 CAO Shao-mei1,LI Li2,SHI Li-yi1,2,FENG Xin2,ZHANG Yu3,WANG Yuan1(1.College of Science,Shanghai University,Shanghai 200444,China;2.School of Materials Sciences and Engineering,Shanghai University,Shanghai 200072,China;3.School of Environmental and Chemical Engineering,Shanghai University,Shanghai 200444,China);LiNO_3 Molten Salt Assisted Preparation of Well-dispersed Nano-ZrO_2 Particales[J];Journal of Synthetic Crystals;2008-03
【Co-citations】
Chinese Journal Full-text Database 8 Hits
1 LI Yanjie NING Qingju WU Lina (School of Materials Science and Engineering,Shaanxi University of Science & Technology,Xi'an 710021);Progress in Research on Modification and Preparation of Bi_4Ti_3O_(12)by Molten Salt Method[J];Materials Review;2008-12
2 ZHOU Jian1,JIAO Bao-xiang2 (1.College of Materials Science and Engineering,Nanjing University of Technology,Nanjing 210009,Chain) (2.College of Materials Science and Engineering,Yancheng Institute of Technology,Yancheng 224051,Chain);Molten Salt Method for the Preparation of Inorganic Material Powders[J];Journal of Changshu Institute of Technology;2008-02
3 CHEN Ye,ZHANG Zun-bo,LIU Zhi-min,LIU Liang,ZHANG Wei (College of Materials Science and Chemical Engineering,Harbin Engineering University,Harbin 150001,China);Effect of molten salt treatment on electrochemical performance of MnO_2[J];Electronic Components and Materials;2007-10
4 NING Qing-ju, LI Yan-jie, WU Li-na (School of Materials Science and Engineering, Shaanxi University of Science and Technology, Xi’an 710021, China);Study on micromorphology of Bi_4Ti_3O_(12) powder prepared by molten salt method[J];Electronic Components and Materials;2008-10
5 ZHANG Xin,XIAO Qiu-guo,LIU Qing-quan,WU Zhe-guang(School of Chemistry and Chemical Engineering,Hunan University of Science and Technology,Xiangtan 411201,China);Preliminary Study on Preparation of Flaky Alumina by Molten Salt Method[J];Bulletin of the Chinese Ceramic Society;2009-04
6 Zong Rui, Yu Youhua, Zhang Lan, Yuan Lingling, Yu Lifang (College of Materials Science and Engineering, Jingdezhen Ceramics Institute, Jingdezhen 333001);Research Progress on Synthesis Method of Zinc Titanate Powder[J];Jiangsu Ceramics;2008-05
7 ZHOU Jing-jing (College of Chemistry and Materials Engineering,Wenzhou University,Wenzhou 325035,China);Research Progress in Synthesis of Flaky Alumina With the Molten Salt Method and Application of Flaky Alumina[J];Liaoning Chemical Industry;2010-03
8 WANG Yong-fei,LI Qiao-ling,JING Hong-xia(Chemistry Department,North University of China,Taiyuan 030051,China);Progress in Chemical Preparation of Nanometer SrFe_(12)O_(19)[J];Contemporary Chemical Industry;2007-04
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 TIAN Zhongqing LIU Hanxing YU Hongtao Ouyang Shixi (State Key Lab of Advanced Technology for Materials Synthesis and Processing,Wuhan University of Technology,Wuhan 430070);Synthesis Methods of Powder for Microwave Dielectric Ceramics[J];Materials Review;2003-12
2 Liang Liping\ Gao Yinben\ Chen Songying\ Zhang Huining Institute of Coal Chemistry, Academia Sinica, Taiyuan 030001;Influence of Preparation Conditions on Particle Size Distribution of ZrO 2 Ultrafine Powders[J];MATERIALS SCIENCE AND ENGINEERING;1997-01
3 WANG Jian1,2,DENG Xiao-zhi2,QIU Xin-ping2, ZHU Wen-peng1,WU Wen-hong1,LI Jun1(1.The 718th Research Institute,China Shipbuilding Industry Corporation,Handan 056027;2.Department of Chemistry,Tsinghua University,Beijing 100084,China);Synthesis of ZnO Nano-crystal Powder by Molten Salt Method[J];China Powder Science and Technology;2006-06
4 Li Chunhua\ Lou Yanliang\ Guo Wenhua (Department of Material Science and Engineering,Huazhong University of Science and Technology,Wuhan,430074,China);The Technique of Preparing Ultrafine ZrO 2 Powder with Sol Wet Chemical Method[J];JOURNAL OF FUNCTIONAL MATERIALS;1997-03
5 Sun Yaguang\ Yu Lixiu (National Engineering Center for Multipurpose Utilization of Non-Metallic Mineral Resources,Zhengzhou,450006);THE PREPARATIONS AND DEVELOPMENT TREND OF ZIRCONIUM DIOXIDE[J];NEW CHEMICAL MATERIALS;2000-04
6 WANG Huan-ying~1,SONG Xiu-qin~2(1.Department of Chemistry,Hengshui College,Hengshui 053000,China;2.Department of Chemistry,Hebei Normal University,Shijiazhuang 050016,China);Discussion on the Influence of Kinds of Additives on Nanometer ZrO_2 Powder[J];Journal of Synthetic Crystals;2005-05
7 DUAN Guo-rong~(1,2),YANG Xu-jie~1,LU Lu-de~1,WANG Xin~1 (1 Materials Chemistry Laboratory,Nanjing University of Science and Technology,Nanjing 210094,China;2 Nanjing Hydraulic Research Institute,Research and Development High Technology Co.,Nanjing 210024,China);Preparation of Single-phase Nanosized Zirconia by Sol-gel and Distillation Method[J];Journal of Synthetic Crystals;2006-02
8 WANG Huan-ying~1,GUO Zhan-sheng~1,XING Guang-en~1,SONG Xiu-qin~2(1.Department of Application Chemistry,Hengshui College,Hengshui 053000,China;2.Department of Chemistry,Hebei Normal University,Shijiazhuang 050016,China);Study on Preparing Nano-sized ZrO_2 by Different Techniques[J];Journal of Synthetic Crystals;2006-04
9 WANG Huan-ying1,ZHANG Ping2,GUO Zhan-sheng1,XING Guang-en1,QIN Li-juan1,HAN Zhi-min1(1.Department of Application Chemistry,Hengshui University,Hengshui 053000,China;2.Department of Chemistry,Shijiazhuang University,Shijiazhuang 050035,China);Progress in the Preparation and Application of Nanometer ZrO_2 Ceramic Composite Materials[J];Journal of Synthetic Crystals;2007-01
10 GU Hua-zhi,WANG Hui-feng,WANG Hou-zhi,WANG Jiao (The Hubei Province Key Laboratory of Ceramics and Refractories,Wuhan University of Science and Technology,Wuhan 430081,China);Influence of Different Surface Active Agents on the Preparation of Nanometer ZnO/ZrO_2 and the Desulphurization Properties[J];Journal of Synthetic Crystals;2007-03
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved