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《Chinese Journal of Fisheries》 2014-06
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Detection of Sulfonamides in Chinese Herbal Medicines by High Performance Liquid Chromatography

QIN Dong-li;KANG Kai;WU Song;TANG Shi-zhan;BAI Shu-yan;DU Ning-ning;MOU Zhen-bo;Heilongjiang River Fisheries Research Institute, Chinese Academy of Fishery Sciences;  
A high performance liquid chromatography(HPLC)method was developed for determination of six kinds of sulfa antibiotics in Chinese herbal medicines, compared and optimized the extraction, purification, and chromatographic conditions. The samples were extracted with ethyl acetate and purified by PEP-2 solid phase extraction column, and then acetonitrile, methanol and 2% acetic acid were used as mobile phase for gradient elution. The residues were separated by C18 column, determined by HPLC with ultraviolet detection(270nm)and quantified by external standard method. This method with limits of detection of 50 μg/kg, average recovery of86.8%~96.5%, and relative standard deviations of less than 6.7% can be applied in quantitative detection of sulfa antibiotics in Chinese herbal medicines.
【Fund】: 中央级公益性科研院所基本科研业务费专项(HSY2013007)
【CateGory Index】: R284;O657.72
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