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《Qilu Pharmaceutical Affairs》 2007-11
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Determination of content and related substances of Picamilon Tablets

LI Yang,JIANG Shou-yi,WANG Min-dong,BI Xiu-li1(Shandong Xinyuan Group Limited Company,Laiyang 265200;1.School of Pharmaceutical Science,Shandong University,Ji′nan 250012)  
OBJECTIVE To establish an UV and HPLC method for determination of content and related substances in Picamilon Tablets.METHODS Determination of content in Picamilon Tablets by UV and determination of related substances in Picamilon Tablets by HPLC.RESULTS The linear range of picamilon measured by UV was 10~60μg·mL-1(r=0.9999),within day and daytime precision RSD was 0.32% and 1.28%,respectively,the recovery rate was 99.49%(RSD=0.79%);The linear range of picamilon measured by HPLC was 10~50μg·mL-1(r=0.9997),the intraday and interday RSD was 0.55% and 0.86%,respectively,with detection limit of 25ng·mL-1,and the impurity and principal agents can be well separated.CONCLUSION This method was available for determination of content and related substances in Picamilon Tablets.
【CateGory Index】: R927
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【Citations】
Chinese Journal Full-text Database 2 Hits
1 LI Ming-xia~1,GU Yi-zhu~2(1.Experimental Center,College of Chemistry and Chemical Engineerjing;2.Department of Pharmacetices,Qilu Hospital,Shandong University,Jinan 250012,Shandong,China);Preparation and quality investigation of pcamilon sodium dispersible tablets[J];Journal of Shandong University(Health Sciences);2006-09
2 TU Shi-Zhong, ZHUANG Ming-Qiang (College of Pharmacy, Second Military Medical University, Shanghai 200433);SYNTHESIS OF NOOTROPIC AGENT PIKAMILONE[J];Chinese Journal of Pharmaceuticals;1993-11
【Co-citations】
Chinese Journal Full-text Database 1 Hits
1 LI Ming-xia~1,GU Yi-zhu~2(1.Experimental Center,College of Chemistry and Chemical Engineerjing;2.Department of Pharmacetices,Qilu Hospital,Shandong University,Jinan 250012,Shandong,China);Preparation and quality investigation of pcamilon sodium dispersible tablets[J];Journal of Shandong University(Health Sciences);2006-09
【Secondary Citations】
Chinese Journal Full-text Database 3 Hits
1 WANG Xu Dong ①,XU Ai Xia ②,ZHU Yu Yu( ①Department of Pharmacy,No.425 Hospital of PLA Navy,Sanya 572000,Hainan China)( ②Institute of Women and Infant Health Profection,Yi'nan County.Yi'nan 276300,Shandong China);Preparation and Quality Control of Flurbiprofen Dispersible Tablet[J];Pharmaceutical Journal of Chinese People's Liberation Army;2003-04
2 Li Ruiming, Rong Yingci, Deng Guixing 1(Department of Pharmacy, The First Affiliated Hospital of Sun Yat Sen University, Guangzhou 510080 ;1.Guangzhou Welman Pharm. Co. Ltd., Guangzhou 510075);Preparation of Ganmaoling Dispersible Tablets[J];Guangdong Pharmaceutical Journal;2003-02
3 TU Shi-Zhong, ZHUANG Ming-Qiang (College of Pharmacy, Second Military Medical University, Shanghai 200433);SYNTHESIS OF NOOTROPIC AGENT PIKAMILONE[J];Chinese Journal of Pharmaceuticals;1993-11
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