Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Journal of Shenyang Ligong University》 2013-06
Add to Favorite Get Latest Update

Study on Preparation of Nanopowder CuO by Room-temperature Solid-station Reaction

FANG Yongguang;WANG Guiping;Shenyang Ligong University;  
Nanopowder CuO was synthesized by 2 methods:(1) Cu(CH3COO)2 ·2H2O and H2C2O4 ·2H2O as the starting materials,precursor w as prepared by solid state reaction at room temperature,then CuO Nanopow der w as obtained by decomposition of the precursor.;(2) one step solid state reaction of NaOH with CuCl 2 ·2H 2 O,and PEG-400 as surfactant at room temperature.The effects of grinding time,ignition temperature and time on products w ere studied.The product nanoparticles w ere characterized by X-ray diffraction(XRD).The experiment result shows that the diameter of copper oxide nanopowders prepared by methed(2) is small,the yield is high.The diameter of copper oxide nanopow ders are affected by reaction time,ignition temperature and ignition time.The best conditions preparing copper oxide nanopow ders are as follow s:The reactants is ground for 30min;the precursor is decomposed at 350℃ for 1h.The average diameter of the product copper oxide is 27.06 nm.,the yield is 93.16%.
【CateGory Index】: TQ131.21
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 10 Hits
1 Luo Mingfeng,Li Lixia,Yang Yi(School of Chemical engineering,Nanjing University of Science and Technology,Nanjing 210094,China);Progress on the Preparation and Application of Nano-CuO[J];Micronanoelectronic Technology;2010-05
2 LI Qun1,WANG Bao-he1,XIA Liang-zhi2,YU Cai-yuan1(1.School of Chemical Engineering,Dalian University of Technology,Dalian 116024,China;2.School of Chemical Machinery,Dalian University of Technology,Dalian 116024,China);Study on Preparation of Copper Oxide Nanopowders[J];Henan Chemical Industry;2012-13
3 HONG Wei-liang 1,LIU Jian-hong 1,CHEN Pei 3,TIAN De-yu 1,2 ,ZHAO Feng-qi 3(1 Dept. of Chemistry and Biology, Normal Coll.,Shenzhen Univ, Shenzhen 518060,China; 2 Inst.of Aerospace and Material Engineering,National Univ. of Defence Technology, C;Synthesis of nanometer-CuO powder and its effect on thermal decomposition characteristics of RDX[J];Journal of Propulsion Technology;2001-03
4 Tian Deyu; Zhu Hui;Deng Pengtu;Zeng Zhicheng;Xu Wenying(Dept.of Material Science and Applied Chemistry,National Univ.of Defense Technology,Changsha,410073)Chen Li; Gong Hua; Liu Xunen; Tang Songqing(Shanghai Inst.of Organic Chemistry,Shanghai,200032);EFFECT OF COPPER-CONTAINING CATALYSTS ON COMBUSTION CHARACTERISTICS OF RDX/HTPB COMPOSITE PROPELLANTS[J];JOURNAL OF PROPULSION TECHNOLOGY;1995-06
5 LI Dong-Mei, XIA Xi (Institute of Applied Chemistry, Xinjiang University, Urumqi 830046, China);Preparation of Nanophase CuO Composite Powder and Its Electrochemical Behavior[J];Journal of Inorganic Materials;2001-06
6 LUO Yuan-Xiang LU Lu-De * LIU Xiao-Heng YANG Xu-Jie WANG Xin(College of Chemical Engineering,Na njing University of Science and Tech nology,Nanjing210094);Synthesis of Nanocrystalline CuO an d its Catalytic Activity on the Thermal Decomposition of NH_4 ClO_4[J];Chinese Journal of Inorganic Chemistry;2002-12
7 LI Dong-Sheng*,1,2 WANG Wen-Liang3 WANG Yao-Yu1 WANG Ji-Wu2 SHI Qi-Zhen1(1Department of Chemistry, Northwest University, Shaanxi Key Laboratory of Physico-Inorganic Chemistry, Xi'an 710069)(2Department of Chemistry &Chemical Engineering Yan'an University,Shaanxi Key Laboratory of Chemical Reaction Engineering, Yan'an 716000)(3School of Chemistry & Materials Science, Shaanxi Normal University, Xi'an 710062);Study on the Nano-CuO Powder Made from the Precursor Synthesized by the Precipitation Method in Mixed Solvent[J];Chinese Journal of Inorganic Chemistry;2004-05
8 YAN Bo1 WANG Xin2 SHAO Chun-Hong3 LI Fen1 JIANG An-Xi,1 (1School of Municipal and Environment Engineering, Harbin Institute of Technology, Harbin 150090) (2China Textile Industrial Engineering Institute, Beijing 100037) (3Heilongjiang Institute of Technology, Harbin 150050);CuO Nanoparticles:Preparation and Desulfurization Performance at Normal Temperature[J];Chinese Journal of Inorganic Chemistry;2007-11
9 SUN Shao-xue~(1),YUAN Guan-ming~(1,2),DONG Zhi-jun~(1,2 ),LIU Xiu-ran~(1),LI Xuan-ke~(1,2)(1 .College of Chemical Engineering, Resources and Environment, Wuhan University of Science and Technology,Wuhan 430081, China;2.Hubei Refractories and High-temperature Ceramics Key Laboratory,Wuhan University of Science and Technology,Wuhan 430081, China);Preparation of Nano-CuO[J];Journal of Wuhan Yejin University of Science and Technology;2005-03
10 WANG Wen-zhong,WANG Li-juan(School of Science,Minzu University of China,Beijing 10081,China);Shape-Controlled Synthesis of CuO Nanocrystals by a Room Temperature Solid-Phase Route[J];Journal of Minzu University of China(Natural Sciences Edition);2012-04
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 XU Ling1,LIU Chang-ling2,XU Hai-Yan1,WU Shi-biao1,WANG Feng1,LI Chun-yan2(1.School of Materials & Chemical Engineering,Anhui University of Architecture,Hefei 230022,China; 2.Department of Chemistry and Chemical Engineering,Hefei Normal University,Hefei 230061,China);Cooperative Photocatalytic Degradation of Methyl Orange by H_2O_2 and CuO Thin Film[J];Journal of Hefei Normal University;2012-03
2 SHI Feng,LI Yuguo,SUN Qinjun(College of Physics and Electronics,Shandong Normal University,Jinan 250014,CHN);Microstructure Analysis of CuO Thin Films Fabricated with Electrophoretic Deposition Method[J];Semiconductor Optoelectronics;2010-01
3 Luo Mingfeng,Li Lixia,Yang Yi(School of Chemical engineering,Nanjing University of Science and Technology,Nanjing 210094,China);Progress on the Preparation and Application of Nano-CuO[J];Micronanoelectronic Technology;2010-05
4 HONG Wei liang, ZHAO Feng qi, LIU Jian hong, TIAN De yu, LUO Zhong kuan (Department of Chemistry and Biology, Normal College, Shenzhen University, Shenzhen 518060, China);A Novel Preparation Method to Nanometer CuO Powder[J];CHINESE JOURNAL OF EXPLOSIVES & PROPELLANTS;2000-03
5 HONG Weiliang, ZHAO Fengqi, LIU Jianhong(Shenzhen University, Shenzhen518060, China;);Synthesis of Nanocomposite Bi_2O_3·SnO_2 and Its Effect on Thermal Decomposition of RDX[J];Chinese Journal of Explosives & Propellants;2003-01
6 ZHANG Wei, LI Jie, LI Xiao-meng, LUO Yun-jun, TAN Hui-min (School of Material Science and Engineering, Beijing Institute of Technology 100081, China);Effect of Nano-catalysts on the Thermal Decomposition of Aminonitrobenzodifuroxan[J];Chinese Journal of Explosives & Propellants;2004-02
7 YANG Yi,LIU Hong-ying,LI Feng-sheng,ZHANG Xiu-yan,LIU Jian-xun(National Special Superfine Powder Engineering Research Center,Nanjing University of Science & Technology,Nanjing 210094,China);The Catalysis of Nanometer Transition Metal Oxide Adulterated with Rare Earth Oxide on the Thermal Decomposition of AP[J];Chinese Journal of Explosives & Propellants;2005-04
8 WANG Han,ZHAO Feng-qi,FAN Xue-zhong,LI Ji-zhen,GAO Hong-xu,SHAO Chong-bin(Xi′an Modern Chemistry Research Institute,Xi′an 710065,China);Effect of Nano-scale Catalysts on Combustion Characteristics of Smokeless Composite Modified Double-base Propellant[J];Chinese Journal of Explosives & Propellants;2008-02
9 Liu Jingfeng Tian Deyu Deng Pengfen (China Defense Science and Technology Information Center, Beijing 100036);Effect of Superfine Cu 2O Powder on the Thermal Decomposition Characteristics of Components of RDX/AP/HTPB Propellants[J];CHINESE JOURNAL OF EXPLOSIVES & PROPELLANTS;1998-02
10 GAO Xi WANG JiDong QU YiXin LI Tao(College of Chemical Engineering,Beijing University of Chemical Technology,Beijing 100029,China);Use of anhydrous ethanol as solvent to prepare nano A1_2O_3 by a supercritical drying method[J];Journal of Beijing University of Chemical Technology(Natural Science Edition);2008-05
China Proceedings of conference Full-text Database 7 Hits
1 ZHU Yiren, MENG Qinghua, Zhao Yunyun, LI Aimei, YU Xi (School of Chemistry & Chemical Engineering, Xuzhou Normal University, Xuzhou, Jiangsu, 221116);Synthesis of Nanometer CuO and Its Application in Papermaking Effluent Treatment[A];[C];2008
2 Wang Xin, Lu Lude, Yang Xujie, Luo Yuanxiang (College of Chemical Engineering, Nanjing University of Science and Technology, Nanjing, 210094);Nanometer Materials in the Applications of Propellants and Explosives[A];[C];2003
3 Wansheng Zhang,Xuqun Zhao,Fei Lv,Xiaodong Wang,Tao Zhang (Dalian Institute of Chemical Physics,Chinese Academy of Sciences,Dalian,116023);Combustion Catalysts for Solid Propellants[A];[C];2011
4 Zhaoxihua1 Xumin2 (Northeast Forestry University, Ministry of Education for Materials Science and Engineering, Key Laboratory, Harbin 150040);Research on Direct Precipitation Preparation Process of Nano-Copper Oxide[A];[C];2009
5 ZHU Yi-ren MENG Qing-hua Zhao Yun-yun LI Ai-mei YU Xi (School of Chemistry & Chemical Engineering,Xuzhou Normal University,Xuzhou,Jiangsu,221116);Synthesis of Nanometer CuO and Its Application in Papermaking Effluent Treatment[A];[C];2008
6 Zhu Yiren~1 Meng qinghua Zhao Yunyun Li Aimei Yu Xin (College of Chemistry and Chemical engineering,Xu zhou Normal University;Xu zhou,China Jiangsu 221116);UV/CuO/H_2O_2 pHotocatalytic Degradation of Wastewater from Paper Mill[A];[C];2008
7 Liu Jun Xu Cheng-hai School of Mechanical Engineering and Automation, Northeastern University, Shenyang 110004 Normal School of Shenyang University, Shenyang 110015;Experimental Study of Nanometer Copper Oxide Powder Prepared by Freeze-drying Process[A];Chinese association of Refrigeration[C];2005
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 MA Feng guo, JI Shu tian, WU Wen hui, TAN Hui min (Beijing Institute of Technology, Beijing 100081,China);Study on the Nanometer-sized Lead Oxide for the Burning Rate Catalysts[J];CHINESE JOURNAL OF EXPLOSIVES & PROPELLANTS;2000-02
2 HONG Wei liang, ZHAO Feng qi, LIU Jian hong, TIAN De yu, LUO Zhong kuan (Department of Chemistry and Biology, Normal College, Shenzhen University, Shenzhen 518060, China);A Novel Preparation Method to Nanometer CuO Powder[J];CHINESE JOURNAL OF EXPLOSIVES & PROPELLANTS;2000-03
3 Zhang Rubing Zhang Fuqing Li Fensheng (Nanjing Institute of Science and Technology, Nanjing 210094);Preparation of Composite Nanometer sized Particle(Ⅰ)[J];Chinese Journal of Explosives & Propellants;1999-01
4 WANG Wenliang 1,2* , LI Dongsheng 1, QIN Zhenping 1, YUE Kefen 2, YANG Wenxuan 1 (1 Department of Chemistry and Chemical Engineering, Provincial Key Laboratory of Chemical Reaction Engineering, Yan'an University, Yan'an 716000, China; 2 Departme;Effects of Cu(Ⅱ) Sources on Catalytic Activity of Copper Oxides for H_2O_2 Decomposition[J];Chinese Journal of Catalysis;2001-03
5 ZHU Jun-wu,CHEN Hai-qun,HAO Yan-xia,YANG Xu-jie,LU Lu-de,WANG Xin (Materials Chemistry Laboratory,Nanjing University of Science and Technology,Nanjing 210094,China);Preparation of Needle-shaped CuO Nanocrystals and its Catalytic Properties[J];Journal of Materials Science and Engineering;2004-03
6 LIU Li-lai,LI Zhe(Analysis and Testing Center,Heilongjiang Institute of Science and Technology,Haerbin 150027,China);Synthesis of CuO Nanostructure on the Basis of Anodic Aluminum Oxide Template by Hydrothermal Method[J];Journal of Materials Science and Engineering;2009-02
7 TAN Ji-ye, ZOU Fan (Department of Chemistry and Chemical Engineering, Dalian University, Dalian 116622, China);Solid-state chemical preparation of the nano copper oxide[J];Journal of Dalian University;2003-02
8 WANG Jisen,YANG Jinkai,BAO Ying, SUN Jinquan,ZHANG Shuqing (School of Power and Control Engineering,Shandong University of Science and Technology,Jinan,250031,China);Novel Method of Synthesis of CuO Nanoparticles[J];China Powder Science and Technology;2003-04
9 Liu Kehui1, Yan Liushui2, Luo Guoan~1 ~ 1(Department of Chemistry, Tsinghua University, Beijing 100084) ~ 2(Department of Enviroment and Chemical Engineering, Nanchang Institute of Aeronautical Technology, Nanchang 330034);Nanosized CuO Catalysed Chemiluminescence Analysis in Amino Acid Analysis[J];Chinese Journal of Analytical Chemistry;2005-06
10 LI Ya-Dong; LI Cheng-Wei; ZHENG Hua-Gui; LI Long-Quan;DUAN Xiang-Feng; QIAN Yi-Tai(Department of Chemistry, Structure Research Laborxitory,University of Science and Technology of China, Hefei, 230026);Preparation and Characterization of Nanocrystalline NiO in Mixed Solvent[J];CHEMICAL RESEARCH IN CHINESE UNIVERSITIES;1997-12
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved