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《Journal of Shihezi University(Natural Science)》 2003-04
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Research on Extraction and Separation and Content Measuration of Icariin

LI Bing-qi, CHEN Han-ying, LIU Hong, ZHANG Yan-ping (Department of Chemistry, Teachers College, Shihezi University, Shihezi, Xinjiang 832003, China; College of Animal Science & Technology, Shihezi University, Shihezi, Xinjiang 832003, China)  
Ultrasonic ethanol extraction, ultrasonic water extraction and countercurrent extraction with reflux were applied in the extraction of gluosides from epimedium. And the author separated it preliminarily and then measured its content. The result showed that the sample of highest content 72.2% was obtained with the ultrasonic extraction. The content gained by contercurrent extraction with reflux was 64.3% .The extraction with ultrasonic water gained the content of 62. 8% .The best scheme of this experiment is the ultrasonic extraction. Under the contidition of 401, with 70% reflux twice,30min every time and the quanlity of solvent is as much as 13 times and then 8 times of the quantity of the medicine.
【Key Words】: Icariin extraction and separation content measuration.
【CateGory Index】: O657.3
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【References】
Chinese Journal Full-text Database 1 Hits
1 RAN Xiao-hui1,WANG Yun2,MA Cai-jing1(1.Taihuatang Pharmaceutical Factory in Sichuan,SiChuan 618300,China;2.Chongqing university of posts and telecommunications,Chongqing 400065,China);Determination of icariine in Gu-Gu sustained-release capsule by HPLC[J];Modern Medicine & Health;2009-01
【Citations】
Chinese Journal Full-text Database 1 Hits
1 CHEN Hui ling, WANG Jian ke, ZHANG Li li, WU Zhen yun (Guiyang College of Traditional Chinese Medicine, Guiyang 550002,Guizhou,China );Contents of General Flavonoides in Epimedium acuminatum Franch. and Its Differently processed Products[J];CHINA JOURNAL OF CHINESE MATERIA MEDICA;2000-04
【Co-citations】
Chinese Journal Full-text Database 6 Hits
1 WEI Sheng-hua,GAO Yan-ming,CHEN Hui-ling,WANG Jian-ke, MA Xiu-ping,LI Jian,ZHOU Xing-nan(Department of Pharmacology,Guiyang College of Traditional Chinese Medicine,Guiyang 550002,China);The Contents of General Flavone,Icariin and Chlorogenic Acid in Epimedium wushanense and Its Differently-processed Products[J];Journal of Guiyang Medical College;2006-03
2 FENG Wei1,WANG Wen-quan1*,ZHAO Ping-ran2,CHEN Yun-hua1,LIU Li1(1.Beijing University of Chinese Medicine,Beijing 100102,China;2.Hebei Medical University,Shijiazhuang 050017,China);Comparison of the Active Components in Glycyrrhiza uralensis Fisch Processed by Water[J];Lishizhen Medicine and Materia Medica Research;2007-08
3 CHEN Hui-ling, WANG Jian-ke, REN Yong-quan, WU Zhen-yun (Guiyang College of Traditional Chinese Medicine, Guiyang 550002, Guizhou, China);Contents of Ten Trace Elements in Epimedium acuminatum Franch. and ItsDifferent Processed Produts[J];China Journal of Chinese Materia Medica;2001-03
4 DU Shu shan, Lin Hong ying, ZHOU Yu xin, WEI Lu xue (Beijing University of Traditional Chinese Medicine,Beijing 100029,China);Contents of total flavonoids in Rhizoma Arisaematis[J];China Journal of Chinese Materia Medica;2001-06
5 PEI Li-kuan,GUO Bao-lin(Institute of Medicinal Plant Development,Chinese Academy of Medical Science and Peking Union of Medical College,Beijing 100094,China);A review on research of raw material and cut crude drug of Herba Epimedii in last ten years[J];China Journal of Chinese Materia Medica;2007-06
6 CHEN Yan1,2,CAI Yin2,JIA Xiao-bin2,DING An-wei1(1.Nanjing University of Chinese Medicine,Nanjing 210046,China;2.Jiangsu Provincial Academy of Chinese Medicine,Jiangsu Engineering and Technology Research Center for Modern Chinese Pharmaceutical Preparation,Nanjing 210028,China);Content comparison of main constituents in Yinyanghuo Granules from different manufactories[J];China Journal of Chinese Materia Medica;2008-02
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 WANG Hong rui 1, YANG Fan 2 ,CHEN Jian yong ** , TAN Xin ** , LIANG Hui ming ** (1.The Pharmaceutical Section of The Shi Yan People Hospital of Baoan, Shenzhen,Guangdong 518000; 2.Department of Pharmaceuticals,Guangdong College of Pharmaey,Guangzhou Guangdong 510224);Optimization of the extraction process of Herba Epimedii by orthogonal design[J];Academic Journal of Guangdong College of Pharmacy;2003-01
2 Sun Xiuhua (孙秀华), Yang Zhengyu (杨正裕), Kang Yuling (康玉玲) (Beijing University of Traditional Chinese Medicine, Beijing 100029);A Research on the Extraction Technology of GuJian Granules[J];JOURNAL OF BEIJING UNIVERSITY OF TRADITIONAL CHINESE MEDICINE;1999-04
3 LIU Xu , YANG Xue-mei , XU Jiang-ping , LI Lin , ZHU Bo-hua ( Department of Pharmacology, the First Military Medical University, Guangzhou 510515, China; Guangzhou Qixing Pharmaceutical LTD Co. ,Guangzhou 510310, China);studies on process for extraction of Ligusticum Chuanxiong Hort. by orthogonal experiments[J];Guangdong Pharmaceutical Journal;2003-06
4 ZHAO Li lian, XIA Xing hua (Hunan College of Traditional Chinese Medicine; Changsha 410004, China);Study on alcohol extraction process of Rhizoma Chuanxiong[J];Chinese Traditional Patent Medicine;2002-03
5 XU Yue hong1, WANG Ning sheng2, CHEN Bao1, XU Li1 (1.School of Pharmaceutical Sciences, Sun Yat sen University, Guangzhou 510080, China; 2.Institute of Clinic Pharmacology, Guangzhou University of Traditional Chinese Medicine, Guangzhou 510405, China);Effect of micronization on the powder characteristic of Angelica Sinennsis and extraction of ferulic acid[J];Chinese Traditional Patent Medicine;2004-10
6 MA Qiang~1, ZHOU Yu-xin~2, LEI Hai-min~3, WANG Chang-hai~1(1. Department of Bioscience and Biotechnology, School of Environmental and Biological Science and Technology, Dalian University of Technology, Dalian 116024, China; 2. Beijing MedSun Pharmaceutical Co., Ltd, Beijing 100029, China;3.College of Chinese Materia Medica, Beijing University of Chinese Traditional Medicine, Beijing 100102, China);Determination of icariin and adenosine in Cordyceps Vigorine Tablet by HPLC[J];Chinese Traditional Patent Medicine;2005-06
7 Liu Guihua Bai Cuihua Kong Xiangyun Li Shi * (Jili Provincial Sanitary and Anti-epidemic Station, Changchun 130021);EXPERIMENTAL OBSERVATION ON BACTERICIDAL EFFICACY OF WATER DECOCTION OF RADIX ANGELICAE SINENSIS AND RADIX ANGELICAE DAHURICAE[J];CHINESE JOURNAL OF DISINFECTION;2000-01
8 Chang Mingxiang;Yao Chuiyu;Liu Xiaoping; Ma Zhuo;Liu Jinxin and Huang Dianyun(Affiliated Hospital,Hubei College of Traditional Chinese Medicine,Wuhan 430061);Study on Bacteriostasis of Rhizoma Coptidis Combined with TMP[J];CHINA JOURNAL OF CHINESE MATERIA MEDICA;1994-12
9 Wang Haiyan,Chen Ruxian and Xu Hongzhang(Institute of Medicinal Biotechnology,Chinese Academy of Medical Scicences & Peking Union Medical College  ,Beijing 100050);Studies on Chemical Constituents of Radix Angelicae Sinensis[J];CHINA JOURNAL OF CHINESE MATERIA MEDICA;1998-03
10 BAI Hai\|bo,WANG JIan\|fei,SONG Zi\|rong (Hainan Yangshengtang Medical Research Center,Hangzhou 310007,China);Study on Optimizing the Extraction Process of Ferulic Acid and Ligustilide in Ligusticum Chuanxion Hort.[J];Chinese Journal of Experimental Traditional Medical Formulae;2003-04
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