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《Modernization of Traditional Chinese Medicine and Materia Medica-World Science and Technology》 2015-03
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Study on Chemical Constituents from Chemical Split Fractions of Mori Cortex

Feng Weisheng;Cao Yangang;Li Fang;Zhang Yanli;Li Chunge;Wang Xiaolan;Chen Wenjing;Kuang Haixue;Zheng Xiaoke;School of Pharmacy, Henan University of Traditional Chinese Medicine;Collaborative Innovation Center for Respiratory Disease Diagnosis And Treatment & Chinese Medicine Development of Henan Province;College of Pharmacy, Heilongjiang University of Chinese Medicine;  
This article was aimed to study the chemical constituents from the chemical split fractions of Mori Cortex. The compounds were isolated with Diaion HP-20, Toyopearl HW-40, Sephadex LH-20, MCI Gel CHP-20, Silica gel column chromatography and preparative HPLC. Structures of compounds were identified by physicochemical properties and spectral analysis. The results showed that 23 compounds were obtained. And their structures were identified. The 16 compounds were obtained from the 30% ethanol fraction as vanillic acid (1), 3,4-dimethoxyphenol (2), benzoic acid (3), syringic acid (4), kelampayoside A (5), p-hydroxyphenylpropionic acid (6), caffeic acid (7), hydroferulic acid (8), 6,7-dihydroxycoumarin (9), 5,7-dihydroxycoumarin (10), morin-7-O-β-D-glucopyranoside (11), liriodendrin (12), 2,3-trans-dihydromorin (13), 2,3-cis-dihydromorin (14), 2,3-trans-dihydroquercetin (15), 2,3-cis-dihydroquercetin (16). The 4 compounds were obtained from the 50% ethanol fraction as scopoletin (17), morin (18), kaempferol-7-O-β-D-glucopyranoside (19), umbelliferone (20). The 3 compounds were obtained from the 80% ethanol fraction as sanggenon R (21), cis-mulberroside A (22), resveratrol (23). It was concluded that compounds 2, 4-6, 11, 16, 19 were isolated from this plant for the first time.
【Fund】: 科学技术部国家重点基础研究发展计划“973计划”项目(2013CB531802):宣泻利水中药的药性研究 负责人:郑晓珂
【CateGory Index】: R284.1
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