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《China Feed》 2010-10
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Determination of deoxynivalenol in silage feed by immuno-affinity column-HPLC method

Dong Yingchao,Li Jun,Li Junguo,et al.  
A method was developed for determination of deoxynivalenol in silage feed by high performance liquid chromatographic(HPLC) method.Sample of silage was extracted with water and cleaned up by an immuno-affinity column (DON-test),then analyzed by HPLC.Linear range of DON was 0.1 ~ 5.0 mg/kg with correlation coefficient of 0.9997.The average recovery at the spiked levels of 0.5,1.0 and 2.0 mg/kg for silage feed was 82 % ~ 117 %,and the relative standard deviation was 5.1 % ~ 7.8 %.The detection limit(S/N=3)was 0.05 mg/kg for deoxynivalenol.
【Fund】: 生鲜乳质量安全隐患饲料因素排查监测项目
【CateGory Index】: S816.17
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【Secondary Citations】
Chinese Journal Full-text Database 1 Hits
1 ZHANG Hai bin,LU Cheng ping (College of Veterinary Medicine, Nanjing Agric Univ, Nanjing 210095,China);Detection of Penicillium roqueforti in feed[J];Animal Husbandry & Veterinary Medicine;2003-01
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