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《The Food Industry》 2010-05
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Study on Analytical Method of 4 Diuretics in the Weight-loss Functional Foods with UPLC/MS/MS

Ma Chang-Lu1,Fu Li2,Ma Li-qing2,He Hao3,Wang Hai-bo4 1.Beijing Vocational College of Agriculture(Beijing 102442);2.Zhengzhou College of Animal Husbandry Engineering(Zhengzhou 450011);3.Suifenhe Entry-exist Inspection and Quarantine Bureau(Suifenhe 157300);4.Dongning Entry-exist Inspection and Quarantine Bureau(Dongning 157200)  
A comprehensive based on ultra performance liquid chromatography tandem mass spectrometry has been developed for the simutaneous determination of 4 diuretics(triamterene,bumetanide,indapamide,torasemide).After various weight-loss functional foods were extracted with methnal(1% acetic acid) under ultrasoniccation.Qualitative and quantitative analysis was carried out for the analyte under the MRM mode after the chromatographic separation on Waters ACQUITY UPLC HSS T3(1.8 μm,100 mm×2.1 mm) column.The limits of detection for 4 diuretics in tea,coffee,capsule and table were(0.3~7.0) mg/kg and the limits of detection for 4 diuretics in solvent was(0.3~7.0) mg/kg.The mean recoveries at the three spiked levels were 80.0%~105.1%,with the intra-day precision less than 8% and the inter-day precision less than 10%.The method is accurate,sensitive,simple,and adapts to the determination of 4 diuretics in the different weight-loss functional foods.
【CateGory Index】: TS218
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【Citations】
Chinese Journal Full-text Database 2 Hits
1 QIN Yang, ZHU Shao _ tang, ZHANG Chang _ jiu (China Doping Control Center, National Research Institute of Sports Medicine, The State Sport General Administration, Beijing 100029, China);Determination of Diuretics in Doping[J];Journal of Instrumental Analysis;2001-02
2 QIN Yang1, 2, ZHU Shao _ tang2, WANG Chao1, ZHAO Ming1, PENG Shi _ qi1 (1. College of Pharmaceutical Sciences, Peking University, Beijing 100083, China; 2. China Doping Control Center, National Research Institute of Sports Medicine, The State Sport General Administration, Beijing 100029, China );Analysis of 13 Diuretics by HPLC[J];Journal of Instrumental Analysis;2003-01
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 Zhang Shaohong~1, 2, Xi Juan~1, He Zhike~*1 ~1(College of Chemistry & Molecular Sciences, Wuhan University, Wuhan 430072) ~2(Xiangfan Vocational and Technical College, Xiangfan 441021);Detection of Furosemide with Tris-(2,2′-bipyridyl)ruthenium- Ce(Ⅳ) Chemiluminescence System[J];Chinese Journal of Analytical Chemistry;2005-09
2 FU Ruo nong (Department of Chemistry, Beijing Institute of Technology, Beijing 100088),Fenxi Shiyanshi,2003,22(2):94~107;Advances on gas chromatography in China[J];Analytical Laboratory;2003-02
3 CHEN Fei, LUO Guangsheng, WANG Yujun (State Key Lab of Chemical Engineering, Department of Chemical Engineering Tsinghua University, Beijing 100084);STUDIES ON ADSORPTION PROPERTIES OF CHEMICALLY MODIFIEDCHITOSAN RESINS TO DIURETICS[J];Acta Polymerica Sinica;2005-01
4 LI Guo-Ping (Department of Police Technology,Liaoning Police Academy,Dalian,Liaoning 116033,P.R.China);Determination of Trifluoperazine in Blood by Fluorescence[J];Chinese Journal of Spectroscopy Laboratory;2004-01
5 HU Lin-lin,YU Hui-juan,FANG Wen-hong*,ZHOU Shuai(East China Sea Fisheries Research Institute,Chinese Academy of Fisheries Science,Key and Open Laboratory of Marine and Estuarine Fisheries,Ministry of Agriculture,Shanghai 20009);Determination of Flumequine in Marine Fish Tissues by Reversed Phase-High Performance Liquid Chromatography[J];Journal of Analytical Science;2011-03
6 WANG Yujun, XIONG Ying, CHEN Fei, LUO Guangsheng and DAI Youyuan(Department of Chemical Engineering, Tsinghua University, Beijing 100084,China);POLYSULFONE MICROSPHERES PREPARED BY MIXING TWO EMULSION SYSTEMS AND THEIR ABSORPTION CHARACTERISTICS[J];Journal of Chemical Industry and Engineering(China);2004-10
7 WU Li-ping1,SUN Cheng-jun2,CHEN Cong1,YE Li-ming1(1.West China School of Pharmacy,Sichuan University,Chengdu,Sichuan,610041 P.R.China;2.West China School of Public Health,Sichuan University,Chengdu,Sichuan,610041 P.R.China);Determination of diuretic in functional foods by HPLC with tandem MS[J];West China Journal of Pharmaceutical Sciences;2009-01
8 ZHAO Hai-xiang1,3,GUO Zhen-fu1,WANG Li-ping4,YUAN Guang-yao1,ZHAO Meng-bin3,QIU Yue-ming2*(1.Dept.of Agricultural and Forestal Technology,Northern College of Hebei,Zhangjiakou 075131,China;2.China Research Institute of Standardization,Beijing 100088,China;3.Beijing Splendid Land Agricultural Co.Ltd.,Beijing 100049,China;4.Research Institute of the State Administration of Grain,Beijing 100037,China);GC-MS Determination of 6 Diuretics in Tea Drink[J];Physical Testing and Chemical Analysis(Part B:Chemical Analysis);2010-07
9 ZHANG Liang-xiao (China University of Geosciences(wuhan) Faculty Of Material Science And Chemical Engineering,Hubei,Wuhan,430074);The Progress of Application Study of the HPLC in Pharmaceutical Analysis[J];Inner Mongolian Petrochemical Industry;2005-07
10 Li,Cuixia Liu,Shaopu Liu,Zhongfang Hu,Xiaoli(Key Laboratory on Luminescence and Real-Time Analysis,Ministry of Education,School of Chemistry and Chemical Engineering,Southwest University,Chongqing 400715);Study on the Interaction between Torasemide and Bovine Serum Albumin by Fluorescence Spectroscopy and Its Analytical Application[J];Acta Chimica Sinica;2011-12
China Proceedings of conference Full-text Database 1 Hits
1 LU Qiao-mei QIU Li-jun LIU Wei ZHANG Lan~* Guo-nan (Ministry of Education Key Laboratory of Analysis and Detection Technology for Food Safety,The Sport Science Research Center,Fuzhou University,350002);Rapid screening analysis of diuretics with macroprogram by gas chromatography mass spectrometry[A];[C];2007
【Secondary Citations】
Chinese Journal Full-text Database 3 Hits
1 QIN Yang, ZHU Shao _ tang, ZHANG Chang _ jiu (China Doping Control Center, National Research Institute of Sports Medicine, The State Sport General Administration, Beijing 100029, China);Determination of Diuretics in Doping[J];Journal of Instrumental Analysis;2001-02
2 Zhang Yizhong;Liu Xin;Yie Li;Zhang Changjiu;Zhu Shaotang;Yang Zeyi(National Research Institute of Sports Medicine,1 AndingRoad,Beijing 100029,China)Zhang Ji,Zhou Tonghui(Chinese Academy of Material Medica,1 Xian NongTan Road,Beijing 100050,China);Studies on Mass Spectra of Androgenic-Anabolic Steroids[J];JOURNAL OF CHINESE MASS SPECTROMETRY SOCIETY;1995-01
3 Qin Yang;Wang Xiaobin;Yang Shuming;Zhu Shaotang(National Institute of Sport Medicine,Beijing 100029,China);GC/MS Study on Indapamide in Human Urine[J];JOURNAL OF CHINESE MASS SPECTROMETRY SOCIETY;1996-04
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