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《Food Science》 2007-11
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Determination of Organic Acids in Shanxi Ageing Vinegar by High Performance Liquid Chromatography

LU Li-hua1,LIANG Li-rong2,ZHAO Liang-qi1, (1.Chemical Biology and Molecular Engineering Laboratory of Education Ministry, Shanxi University, Taiyuan 030006, China; 2.The Center for Disease Control and Prevention of Taiyuan, Taiyuan 030001, China)  
An ion-exclusion HPLC method for rapid determination of 8 organic acids in Shanxi ageing vinegar was developed in this paper. 8 organic acids were separated by the use of PRP-X300 ion-exclusion column, and the optimal separation conditions are as follows: 0.05mmol/L H2SO4 as mobile phase, flow rate at 1ml/min, column temperature at room temperature, UV detector at 210 nm, and sample size as 5 μl. The RSD is 0.72%~5.47%, and the recovery rate is 95.1%~105%. The method has the advantages of rapid and simple operation, good selectivity and high accuracy.
【Fund】: 山西省重大科技攻关项目
【CateGory Index】: TS264.22
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