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《Food Science》 2008-07
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Determination of Aloin in Dry Aloe Powder

WANG Ming-yue1,GUI Wei-xing2,ZOU Dong-mei3 (1.Center of Analysis and Test,Chinese Academy of Tropical Agricultural Sciences , Haikou 571101, China; 2. Vegetable Sciences Institute of Nanchang City, Nanchang 330001, China; 3.Tropical Crops Genetic Resources Institute,Chinese Academy of Tropical Agricultural Sciences, Danzhou 571737, China)  
Aloin was extracted from dry aloe powder with methanol, further purified by solid phase extraction column, and then determined by high performance liquid chromatograph (HPLC). The HPLC operation conditions were as follows: C18 column (4.6 mm×150 mm, 5μm), methnaol-1% acetic acid water (1:1, V/V) as mobile phase, and UV detector wavelength 359 nm. The quantitative and qualitative analyses were performed with external standard method. The results of determination showed that there is a good linear calibration curve in the range from 0 to 100 mg/L (r=0.9999) with relative standard deviations of 2.5% to 3.2% (n=6). The recovery rates of spiked aloin range from 98.1% to 101%, and the detection limit is 0.02 mg/kg. This method is rapid, sensitive, simple, accurate and repeatable.
【CateGory Index】: R284
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【References】
Chinese Journal Full-text Database 1 Hits
1 Zou Dongmei1, Wang Mingyue2, Chen Chenghai3, Wang Jianrong1, Jinag Changshun1 1 Tropical Crops Genetic Resources Institute, CATAS, Danzhou, Hainan 571737; 2 Ministry of Agriculture Quality Supervision and Testing Centre for Tropical Agricultural Products, Haikou, Hainan 666100; 3 Ministry of Agriculture Centre for Food Quality Supervision and Testing, Zhanjiang, Guangdong 524001;Quantitative Determination of Aloin in Aloe and Its Products by High Performance Liquid Chromatography[J];Chinese Journal of Tropical Crops;2009-04
【Citations】
Chinese Journal Full-text Database 3 Hits
1 Fu Yin-long, Qian He (School of Food Science & Technology, Southern Yangtze University, Jiangsu Wuxi 214036);Study on Extraction and Detection of Aloin[J];Jiangsu Food and Fermentation;2002-03
2 Li Duowei et al.;Study on TLC Scanning Determination of Barbaloin in Aloe Barbadensis[J];Food Science;2002-05
3 Chen Wei(Chen W),Lin Xinhua(Lin XH),Huang Liying(Huang LY),et al(Fuzhou 350004,Department of Pharmaceutical,Fujian Medical University);Determination of the aloin by dual-wavelength spectrophotometry[J];Chinese Journal of Modern Applied Pharmacy;2002-05
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 Pan Hong(Shaoxing Branch of Zhejiang Econamia&Trade Polytechnic);The Health Protectional Virtue and Exploiture of Aloe[J];Anhui Agricultural Science Bulletin;2007-23
2 WU Qiang,DONG Yin-mou,LU Xin-mei(College of Chemical and Environmental Engineering, Beijing Technology and Business University, Beijing 100037, China);STUDY ON TOXICITY OF ALOE EXTRACTIONS[J];Journal of Beijing Technology and Business University (Natural Science Edition);2005-03
3 MA Jing-jun~1,FANG Zheng~1,WU Qiu-hua~1,SUN Huan-ming~2,WEN Ya-jun~2(1.Agricultural University of Hebei,Baoding 071001, China;2.Beijing Agro-Tech Extension Station, Beijing 100029, China);On determination of Aloin and Aloe-emodin in Aloe barbadensis mill by HPLC[J];Journal of Agricultural University of Hebei;2005-02
4 CHAI Yi feng ,WU Yu tian andLI Xiang(Department of Pharmaceutical Analysis ,College of Pharmacy ,Second Military edical University ,Guohe Road 32 5 , Shanghai 2 0 0 4 33);Pharmaceutical Analysis (Ⅱ)[J];Analytical Laboratory;2004-07
5 GENG Mei, DU Hai-yan, SUN Jia-yue and WU Ai-ping (College of Chemical and Environmental Engineering, Beijing Technology and Business University, Beijing 100037);Simultaneous determination of aloin and aloe-emodin by using four working curves[J];Analytical Laboratory;2005-01
6 PANG Hui-zhong~1,YU Zhi-xiong~(2*),SHI Jian-min~2,XIAO Zhen~1,JIANG Mu-lan~1,JIE Zheng-ping~2 (1.Department of Bioengineering,JAU,Nanchang 330045,China;2.College of Art and Landscape,JAU,Nanchang 330045,China);The Anti-oxidation Effect of Polysaccharide Extracted from Sinomanglietia glaula Leaf[J];Acta Agriculturae Universitatis Jiangxiensis;2006-06
7 Zou Dongmei1, Wang Mingyue2, Chen Chenghai3, Wang Jianrong1, Jinag Changshun1 1 Tropical Crops Genetic Resources Institute, CATAS, Danzhou, Hainan 571737; 2 Ministry of Agriculture Quality Supervision and Testing Centre for Tropical Agricultural Products, Haikou, Hainan 666100; 3 Ministry of Agriculture Centre for Food Quality Supervision and Testing, Zhanjiang, Guangdong 524001;Quantitative Determination of Aloin in Aloe and Its Products by High Performance Liquid Chromatography[J];Chinese Journal of Tropical Crops;2009-04
8 Du Hai yan, Geng Mei, Sun Jia yue (College of Chemical and environmental engineering, Beijing Technology and Business University, Beijing 100037 China);Current situation on analytical methods of Aloin[J];Life Science Instruments;2003-06
9 CAI Jian(Department of Food,Suzhou Polytechnical Institute of Agriculture,Suzhou 215008,China);Function Components and Health Function of Aloe[J];Food and Drug;2006-08
10 ZHAN Yong LU Tian-jian TAN Hong-jun SONG Fan ZHU Lu-yi (Chongqing Academy of Chinese Materia Medica,Chongqing 400065,China);The extracting and decoloring technique of aloe gel liquor[J];Food and Machinery;2004-03
China Proceedings of conference Full-text Database 2 Hits
1 Pan Qinghua Wang Xiuqin Lu Renqiang (Foresty and Pomology Research Institute,Beijing Academy of Agricultural Science,Beijing 100093);Preliminary study on prevention and cure technology of Cracking fruit in Jinzao39[A];[C];2005
2 Cheng Lihua Wang Guotuan Zhang Weidong (Pharmacy of Central Hospital of Kelamayi Xinjiang 834000)r;Preparation and Qulity Control of Compound Aloe Cream[A];[C];2006
【Co-references】
Chinese Journal Full-text Database 2 Hits
1 Li Duowei et al.;Study on TLC Scanning Determination of Barbaloin in Aloe Barbadensis[J];Food Science;2002-05
2 Chen Wei(Chen W),Lin Xinhua(Lin XH),Huang Liying(Huang LY),et al(Fuzhou 350004,Department of Pharmaceutical,Fujian Medical University);Determination of the aloin by dual-wavelength spectrophotometry[J];Chinese Journal of Modern Applied Pharmacy;2002-05
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 Zhao Huichun; Feng Ruiqin; Deng Xiaoguang ZhangYongan(Department of Chemistry, Beijing Normal University, 100875, Beijing, China);A STUDY OF THE FLUORESCENCE SYSTEM OF BARBALOIN-BORAX SYSTEM AND THE DETERMINATION FOR BARBALOIN[J];JOURNAL OF BEIJING NORMAL UNIVERSITY(NATURAL SCIENCE);1997-02
2 LIN Xin\|hua, CHEN Jun, CHEN Wei, HUANG Li\|ying, LUO Hong\|bin Division of Pharmacy, Fujian Medical University, Fuzhou 350004, China;Extraction and Determination of Polysaccharide from Aloe[J];Journal of Fujian Medical University;2003-02
3 DENG Jun wen( The University Journal Editing Division, Foshan University, Foshan 528000 ,China);The chemical compositions of Aloe and its pharmacological action[J];JOURNAL OF FOSHAN UNIVERSITY(NATURAL SCIENCE EDITION);2000-02
4 Chen Dan Bao Guorong Zhen Yujin,et al (Dept.of TCM Pharmacology,FUTCM);Ingredient Analysis on Three Kinds of Fujian Produced Aloe[J];JOURNAL OF FUJIAN COLLEGE OF TRADITIONAL CHINESE MEDICINE;1996-04
5 Liu Jie Liu Changhong Qian He(College of Food, Jiangnan University, Wuxi, 214036);Analysis Methods of Aloe polysaccharide[J];Chemical Industry Times;2002-08
6 Ye YiBing Zhang Xiao Hua Beijing Institute of Light Industry;The Extraction Separation and Identification of Anthraquinones in Aloe[J];Chinese Journal of Ethnomedicine and Ethnopharmacy;1999-02
7 GAO Ju-yi, CHEN Ran (Bioengineering College, Fujian Teachers University, Fuzhou 350007, China);THE ISOLATION AND PURIFICATION OF LECTIN FROM ALOE VERA L. VAR. CHINENSIS (HAW.) BERGER AND ITS CHARACTERISTICS[J];JOURNAL OF TROPICAL AND SUBTROPICAL BOTANY;2000-02
8 (College of Chemincal and environmental engineering, Beijing Technology and Business University, Beijing 100037 China) Duhaiyan Gengmei Sunjiayue;Progress of Research on Quantifying determination of Aloe polysaccharide[J];Life Science Instruments;2003-05
9 Deng Yuqinog;Determination of Total Content of Barbaloin in Aloe Vera Gel[J];FOOD SCIENCE;2000-06
10 WANG De xian, YANG Geng liang, WANG Lin ying, SONG Xiu rong (Department of Chemistry, Hebei University, Baoding 071002, China);Determination of the Active Components in Chinese Herb Aloe vera L.var. chinensis (Haw.) Berger by Capillary Zone Electrophoresis[J];Chinese Journal of Chromatography;2000-05
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