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《Food Science》 2009-12
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HPGPC Determination of Relative Molecular Mass of Inulin

ZHANG Ze-sheng,ZHANG Jian-ping,SHI Shen,SHI Jia-ning,ZHANG Jie(Laboratory of Food Additives and Nutrition,Tianjin University of Science and Technology,Tianjin 300457,China)  
A high performance gel permeation chromatography(HPGPC) method was developed for the determination of relative molecular mass of inulin.Separation was performed on a GPC column with triple distilled water as a mobile phase at the flow rate of 0.8 ml/min and 30℃ and determination was carried out using a refractive index detector.A direct linear relationship within the range of 1.0×103-2.5×105 of relative molecular mass(r = 0.9894) was found between retention time of dextranum and lgMw.Insulins obtained from jerusalem artichoke by hot water reflux method and ultrasonic-assisted and microwave-assisted water extraction methods possessed varying relative molecular mass of 3500,2405 and 3864,respectively.Methodology evaluation experiments revealed that the RSDs for precision,repeatability and stability were 0.24%,0.21%,and 0.38%,respecitively,and the relative error for accuracy was around 0.4%.This method is proved to be fast,simple,sensible and repeatable.
【CateGory Index】: TS207.3
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Chinese Journal Full-text Database 4 Hits
1 Wei Lingyun~1,2 Wang Jianhua~2 Zheng Xiaodong~1 Yang Yalin~21(Food Science and Nutrition Department, Zhejiang University, Hangzhou, 310029, China) 2(Institute of Feed Research,Chinese Academy of Agricultural Sciences,Beijing, 100081,China);Review and Prospects of the Inulin Research[J];Food and Fermentation Industries;2005-07
2 ZHANG Hui LIU Zong-min LI Ji-lie(Central South University of Forestry and Technology , Changsha,Hunan 410004,China);The application of microwave extraction in food industry[J];Food & Machinery;2006-06
3 HUANG Yong-chun,MA Yue-fei,XIE Qing-ruo,HUANG Xiao-yan,HUANG Ying-na (Department of Biological and Chemical Engineering, Guangxi University of Technology, Liuzhou 545006, China);Study on Effects of Ultrasonic on Extracion of Tea Polysaccharide and Changes of Molecular Weight[J];Food Science;2007-07
4 Rao ZhijuanZheng JianxianJia Chengxiang(College of Food & Bioengineering,South China Univ.of Tech.,Guangzhou,510641);Development of Functional Food Ingredient--Inulin[J];China Beet & Sugar;2002-04
Chinese Journal Full-text Database 10 Hits
1 WU Hong-xin et al (Grassland Research Institute,Chinese Academy of Agricultural Sciences, Hohhot,Inner Mongolia 010020);Study on the De-coloration of Chicory Inulin by Active Carbon Method[J];Journal of Anhui Agricultural Sciences;2008-07
2 WU Hong-xin et al (Institute of Grassland Research,Chinese Academy of Agricultural Sciences,Huhhot,Inner Mongolia 010020);Study On the Detection of Inulin by the Method of UV-VIS Spectrophotometry[J];Journal of Anhui Agricultural Sciences;2008-13
3 LI Jing-qi (College of Life Science, Shaanxi Institute of Education,Xi’an,Shaanxi 710061);Enzymatic Browning and Its Control During Sweet Stem Tuber Processing of The Artichoke[J];Journal of Anhui Agricultural Sciences;2008-21
4 GAO Jian et al (College of Pharmaceutical Engineering and Life Science,Nanjing University of Technology,Nanjing,Jiangsu 210009);Study on Extraction and Separation of Inulin from Jerusalem artichoke[J];Journal of Anhui Agricultural Sciences;2009-01
5 LI Cheng-wei,YAO Xiao-hui,CHEN Xin-bing(Department of Live Science,Shangqiu Normal University,Shangqiu,Henan 476000,China);Effect of 2,4-D and 6-BA on Callus Induction of Helianthus tuberosus Linn[J];Northern Horticulture;2008-02
6 ZHOU Ling,Tang Jing,LI Jiao,DING Jie,LIU bo(College of Pharmacy,Dali University,Dali Yunnan,671000,China);Determination of Content of Polysaccharides in Wild and Man-cultivated Lentinus edodes and Auricularia auricular[J];Journal of Dali University;2008-08
7 HU Jia-qi, GAO Hai-bing, ZHOU Ming-da (College of Chemistry and Chemical Engineering,Central South University,Changsha 410083,Hunan,China);Extracting Fructose from Jerusalem Artichoke with Method of Acid Hydrolysis[J];Guangzhou Chemistry;2007-03
8 WANG Zhi-yong et al (College of Life Science,Northeast Forestry University,Harbin,Heilongjiang 150040);Progress in Comprehensive Utilization of Jerusalem Artichoke[J];Journal of Anhui Agricultural Sciences;2009-25
9 YANG Zhen;YANG Fu-min;WANG Xue-yan(College of Food Science and Engineering,Gansu Agricultural University,Lanzhou 730070,China);Optimizing of extraction techniques on inulin from Helianthus tuberosus L.[J];Journal of Gansu Agricultural University;2009-05
10 WU Hong-tea,SUN Xiao-qinb,LIU Duan-chaob(Yangtze University,a.College of Chemistry and Environmental Engineering;b.College of Life Science,Jingzhou 434025,Hubei,China);Study on the Extracting,Transparencing and Refining of Inulin[J];Hubei Agricultural Sciences;2007-01
China Proceedings of conference Full-text Database 1 Hits
1 CHENG Jun-wen~(1,2),WU Da-feng~2,WU Xue-qian~(1,2*),HE Liang~1,CHEN Ru-chu~2,LI Hai-bo~1, Wei Hai-long~(1,2),FU Li-zhong~1,SUN Ming-hua~(1,2),WU Qing-qi~(1,2) (1 Zhejiang Forestry Academy,Hangzhou 310023,China;2 Zhejiang Essence Fungi Development Company,Lishui 323000,China);Study on Extracting Lentinan from Lentinus edodes by Series of Enzymes[A];[C];2008
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 Wang Dongfeng;Xie Xiaofeng;Wang Shilin;Zheng Jun;Yan Jun;Yan Hongde;Wang Zenong(1 Department of Tea Scicoce,Anhui Agricultural University,Hefei 230036)(2 Kunming Institute of Botany,Academia Sinica,Kunming 650024);Composition and the Physical and Chemical Characteristics of Tea Polysaccharide[J];JOURNAL OF TEA SCIENCE;1996-01
2 YOU Ye-cheng; GUO Ming; ZHANG Xiao-hui(Department of Chemistry and Chemical Engineering, Dalian 116622, China);Study on Extracting the Ingredients from Garlic with MAE[J];JOURNAL OF DALIAN UNIVERSITY;1999-04
3 SHI Ruo fu 1, WANG Guan lin 2 ( 1. School of Chem. Eng., Dalian Univ. of Technol., Dalian 116012, China; 2. Res. Inst. of Plant and Biology Eng.,Liaoning Normal Univ., Dalian 116029, China );Essence oil of Pelargonium graveoleus L′Herit extracted by microwave method[J];Journal of Dalian University of Technology;2001-05
4 ZhANG Hu, LI Kai (Dalian University for National Minorities, 116600);Microwave-assisted Extraction of Lentinan[J];Journal of Dalian Nationalities University;2000-03
5 Li He, Li Gongke *, Zhang Zhanxia (School of Chemistry and Chemical Engineering, Sun Yat-sen University, Guangzhou 510275);Development of Microwave Assisted Extraction[J];Chinese Journal of Analytical Chemistry;2003-10
6 YANG Yun, LUAN Wei and LI Gongke(School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275);Determination of prometryne in vegetable samples by GC-MS using microwave-assisted extraction[J];Analytical Laboratory;2003-04
7 NIAN Bao-yi,WANG Zheng-min,HUANG He-ning (Department of Chemistry & Biological Engineering, Sanming College, Sanming 365004, China);Study on Methodology of Lentinan by Ultrasonic Extracted and Ultra-filtration[J];;2004-04
8 HAO Jin yu 1, HUANG Ruo hua 2, DENG Xiu 1* , WANG Ping yan 2 (1.Chemical Engineering Research Center ECUST, Shanghai 200237, China; 2.Department of Environmental and Chemical Engineering, Kunming University of Science and Technology, Kun;Microwave Extraction of Seed of Passionflower[J];Journal of East China University of Science and Technology;2001-02
9 FU Chang-e~(1,2),HAN Wei~1(1.Modern Engineering Center for Traditional Chinese Medicine,East China University of Science and Technology,Shanghai 200237,China;2.Nanjing College of Chemical Technology,Nanjing 210048,China);Microwave-Assisted Extraction and Enrichment of Arachidonic Acid from Green Algae[J];Journal of East China University of Science and Technology(Natural Science Edition);2006-04
10 NIAN Bao yi 1 , CHEN Ming 2 , WANG Zheng min 1 (1.Department of Chemistry & Biological Engineering, Sanming College, Sanming 365004,China; 2.Quality Inspection Division of Fujian Yaolong Chemical Group, Fuzhou 350011, China);Study on the separation of lentinan by ultrafiltration membrane[J];Journal of Chemical Industry & Engineering;2003-04
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