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《Food Science》 2015-22
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Optimization and Kinetic Analysis of Ultrasonic-Assisted Extraction of Triterpenoids from Pomegranate Rind

WANG Zhanyi;ZHENG Dandan;WANG Jinglong;JIN Meihua;ZHANG Lihua;WANG Yuhai;College of Life Science,Zaozhuang University;College of Pharmacy,Medical University of Tianjin;  
This study examined the ultrasonic-assisted extraction conditions of tnterpenoids from pomegranate rind.Single factor method and Box-Behnken experimental design were used to optimize the extraction process employing triterpenoids yield as the response and ethanol concentration,solid/liquid ratio,ultrasonic power and extraction time as the independent variables.Using the optimized extraction conditions,the kinetics of the extraction process was studied by establishing four mathematical models,and the applicability of these models was analyzed by four model evaluation parameters including coefficient of determination(R~2),accuracy factor(A_f),bias factor(B_f) and root mean square error(RMSE).Results showed that the optimal extraction conditions for triterpenoids were determined as follows:ethanol concentration,71.2%;solid/liquid ratio,1:20.2;ultrasonic power,318 W;and ultrasonic time,36.7 min.Under these conditions,the yield of triterpenoids was 0.563%,and two nonlinear growth models,namely Sgompertz model and Logistic model,could better fit the kinetics.Both the optimized ultrasound-assisted extraction technique and the kinetic mathematical models can be used for industrial scale-up and optimal control of triterpenoids extraction from pomegranate rind.
【Fund】: 2012年度国家星火计划项目(2012GA740049);; 山东省自然科学基金项目(ZR2013BL018)
【CateGory Index】: R284.2
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