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《Applied Chemical Industry》 2015-09
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Study on paired electrosynthesis of succinic acid and p-chlorobenzaldehyde by bipolar membrane technique

LI Zhong-gui;LU Min;CHEN Ri-yao;CHEN Xiao;ZHENG Xi;College of Environmental Science and Engineering,Fujian Normal University;  
The carboxymethyl cellulose( CMC)-polyvinyl alcohol( PVA)/chitosan( CS)-PVA bipolar membrane( BPM) was modified by nano silicon dioxide. Then the modified BPM was used as electrolytic cell septum to synthesize succinic acid and p-chlorobenzaldehyde. The results showed that the optimal preparation conditions were as following: current density was 60 m A/cm2,sulfuric acid concentration in the cathode chamber was 1. 0 mol/L,the molar ratio of p-chlorotoluene to Mn3 +was 4∶ 1.
【Fund】: 福建省自然科学基金项目(2013J01034);; 福建省科技厅重点项目(2012H0019);; 福州市科技局项目(2012-G-116)
【CateGory Index】: TQ225.144;TQ244.1
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