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《Journal of Shenyang Pharmaceutical University》 2008-12
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Megastigmane glucosides from the stems and leaves of the Physalis alkekengi L.var.francheti

QIU Li,LIU Hong-xia,JIANG Zhi-hu,QIN Geng-yao,CHEN Li-xia,QIU Feng(School of Traditional Chinese Materia Medica,Shenyang Pharmaceutical University,Shenyang 110016,China)  
Objective To study the chemical constituents from stems and leave of Physalis alkekengi L.var.francheti(Mast.)Makino.Methods The leaves and stems of Physalis alkekengi L.var.francheti(Mast.)Makino were extracted with EtOH-H2O(V∶V=60∶40).The extract was partitioned with n-hexane,EtOAc and n-BuOH,respectively.The nBuOH layer was subjected to column chromatography over polyamide,Sephadex LH-20,ODS and RP-PHPLC stepwisely to give four megastigmane glucosides.The spectral analyses and physicochemical characters were used to identify the structures of the compounds.Results All of the four compounds were identified as megastigmane glucosides.They are(6S,9R)-roseoside(1),(6S,9S)-roseoside(2),(6R,9S)-3-oxo-α-ionol-β-D-glucopyranoside(3) and citroside A(4).Conclusions Compounds 14 are isolated from Physalis genus(Solanaceae)for the first time.
【CateGory Index】: R284
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