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《Journal of Shenyang Pharmaceutical University》 2010-10
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Separation and identification of new sucrose esters from root of Polygala tenuifolia Willd.

WU Xue-ying1,LIU Ming1,WU Ying-liang2,GUO Yuan-qiang3,LI Yu-shan1(1.School of Traditional Chinese Materia Medica,Shenyang Pharmaceutical University,Shenyang 110016,China;2.School of Life Science and Biopharmaceutics,Shenyang Pharmaceutical University,Shenyang 110016,China;3.College of Pharmacy,Nankai University,Tianjin 300071,China)  
Objective To study the constituents of the extract from the root of Polygala tenuifolia Willd.Methods The chemical constituents were isolated by silica,Sephadex LH-20 gel column chromatography and HPLC.Chemical characters and spectroscopic analysis were employed for the structural identification.Results Eleven compounds were obtained and their structures were identified as sibiricose A5(1),tenuifolioside A(α-D-glucopyranoside,3-O-[(2Z)-3-(4-hydroxy-3-methoxyphenyl)-1-oxo-2-propen-1-yl]-β-D-fructofuranosyl,2),tenuifolioside B(α-D-glucopyranoside,3-O-[(2E)-3-(3,4-dimethoxyphenyl)-1-oxo-2-propen-1-yl]-β-D-fructofuranosyl,3),tenuifolioside C(α-D-glucopyranoside,3-O-[(2Z)-3-(3,4-dimethoxyphenyl)-1-oxo-2-propen-1-yl]-β-D-fructofuranosyl,4),sibiricose A6(5),glomeratose A(6),sibiricaxanthone B(7),polygalaxanthone Ⅺ(8),1,2,3,7-tetramethoxyxanthone(9),onjixanthoneⅡ(10),and polygitol(11).Conclusions Compounds 24,named tenuifolioside A-C respectively,are new sucrose esters which have not been reported before.
【Fund】: 辽宁省自然科学基金资助项目(200620576)
【CateGory Index】: R284
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Chinese Journal Full-text Database 2 Hits
1 WANG Yu-ping, YANG Jun-shan, ZHANG Yu-mei, CHEN Jian-min(Institute of Medicinal Plant, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100094, China);Chemical constituents of Polygala tenuifolia[J];Chinese Traditional and Herbal Drugs;2005-09
2 JIANG Yong, TU Peng-Fei Modern Research Center of TCM, School of Pharmaceutical Sciences, Peking University, Beijing 100083, China;Study on Chemical Constituents of Polygala tenuifolia Ⅲ[J];Chinese Journal of Natural Medicines;2003-03
Chinese Journal Full-text Database 10 Hits
1 ZHANG Ru-Xue,FAN Jun-Jie,JIA Zheng-Ping,KONG Ling-Yuan,MA Hui-Ping,LI Mao-Xing,REN Jun,WANG Juan (Base of Clinical Pharmacology,Lanzhou General Hospital of PLA,Lanzhou 730050,Gansu China);Extraction and Separation Process of Oligosacchrides from Rehmannia Glutinosa[J];Pharmaceutical Journal of Chinese People's Liberation Army;2005-01
2 ZHENG Lu~1,QIU Lei~1,ZHANG Yao~1,FENG Tian-jiao~1,YU Jian-chun~2,ZHANG zhan-jun~(1#) (1 State Key Laboratory of Cognitive Neuroscience and Learning,Beijing Normal University,Beijing 100875;2 First Hospital Affiliated to Tianjin University of Traditional Chinese Medicine);Influences of tenuigenin on learning and memory ability and neurotransmitters in senescence-accelerated mice[J];Journal of Beijing University of Traditional Chinese Medicine;2010-03
3 YAN Ming,LI Ping(1.Liaoning People's Hospital,Shenyang 110016,China;2.Jilin University,Changchun 130021,China);Studies on antiaging action of Polygala tenuifolia Wild.[J];Practical Pharmacy and Clinical Remedies;2006-01
4 YU Huizhen1,WU hui2 (1.Chien-Shiung Institute of Technology,Suzhou,Jiangsu,215411,China; 2.School of Chemistry & Chemical Engineering,Xuzhou Normal University,Xuzhou,Jiangsu,221116,China);Studies on Anti-snake Venom Activity of Ethanol Extract from Polygala sibirica L.var megalopha Fr.[J];Chinese Journal of Ethnomedicine and Ethnopharmacy;2008-01
5 Song Cheng-zhi Wu Zhang-kang Hua Yan(Southwest Forest College,Kunming 650224,China);Advances in study on chemical constituents and pharmacological activities of Polygala[J];Chinese Journal of Ethnomedicine and Ethnopharmacy;2008-03
6 LIU Jun-mei,HU Yao-hui (College of food engineering,JiLin Agriculture University,Changchun 130118);The application of TLC in polyalcohol[J];Food Science and Technology;2007-06
7 XIA Hou-lin,DONG Min,SHENG Yan,WU Xi,TAN Ling,ZHOU Xiao-mei,WANG Jian(Chengdu College of Traditional Chinese Medicine & Pharmacology,Chengdu 610075,China);Comparative Study on Contents of Radix Polygala and the Prepared[J];LiShiZhen Medicine and Materia Medica Research;2006-09
8 ZHAO Jian-guo,QU Wei-hong(Department of Pharmacology of Jiujiang University,Jiujiang,Jiangxi 332000,China);Advances on the Analytical Technologies of Chemical Components in Radix Polygalae[J];Lishizhen Medicine and Materia Medica Research;2009-12
9 DENG Feng-xiang(The Second Medical College of Ji'nan University,Pharmacy Department of Shenzhen People's Hospital,Shenzhen,Guangdong 518020,China);Study on Isolation Method of Polygalic Acid from Polygala Tenuifolia[J];Pharmacy Today;2009-09
10 LU Yi,HUA Yan(Faculty of Resources,Southwest Forestry University,Kunming Yunnan 650224,China);Identification on Five Types of Xanthones Abstracted from Polygala crotalarioides[J];Journal of Southwest Forestry University;2009-03
【Secondary Citations】
Chinese Journal Full-text Database 2 Hits
1 SL Mao;SX Liao;JH Wu;HQ Liang;HS Chen and CK Zhang(Department of Medicinal Chemistry of Natural Products,School of Pharmacy,Second Military Medical University,Shanghai 200433;Drug Control Institute of Kunming,Kunming 650011);STUDIES ON CHEMICAL CONSTITUENTS OF POLYGALA ARILLATA BUCH-HAM[J];ACTA PHARMACEUTICA SINICA;1996-02
2 WANG Gang li, HOU Qing yun, ZHANG Ji, XU Ji min, PENG Ji feng, LIN Rui chao (National Institute for the Control of Pharmaceutical and Biological Products, Beijing 100050,China);Studies on the Chemical Conbstituents of the Stems of Alyxia sinensis(Ⅰ)[J];China Journal of Chinese Materia Medica;2002-02
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