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《Journal of Shenyang Pharmaceutical University》 2019-03
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Simultaneous determination of gerberinside and 8-methoxypsoralen in Gerbera piloselloides (L.) Cass.by RP-HPLC-UV

WANG Na;CAO Weiwei;QIU Weihua;BAI Yuhua;HE Fa;College of Pharmacy,Harbin Medical University;  
Objective To develop a method of high performance liquid chromatography for the content determination of Gerberinside and 8-Methoxypsoralen in Gerbera piloselloides(L.) Cass..Methods The analysis was performed on a WondaCract ODS-2 column(250 mm×4.6 mm,5 μm) with gradient elution.The mobile phase was water(B) and acetonitrile(A).The detection wavelength was 282 nm.The column temperature was set at 25 ℃.Results Gerberinside and 8-methoxypsoralen were separated well with a good linearity,the r values were 0.999 3 and 0.999 4,respectively.The precision,stability and repeatability of the experiment all meet the requirements.The average recovery rate of gerberinside was 99.30%,the average recovery rate of 8-methoxypsoralen was 99.40%.The above two composition could be separated from the baseline,and they had no interference from other component peaks.Conclusion The method has the advantages of simple steps,fast analytical speed and strong specificity,and can be used for the quality control of Gerbera piloselloides(L.) Cass..
【Fund】: 哈尔滨医科大学创新科学研究资助项目(2017JCZX02);; 大庆市指导性科技计划项目(zdy-2017-97)
【CateGory Index】: R284.1
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