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《Lishizhen Medicine and Materia Medica Research》 2009-08
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Determination of Anthraquinones Content in Liuwei Nengxiao Capsule by HPLC

ZENG Rui(Ethnic Pharmaceutical Institute of Southwest University for Nationalities,Chengdu 610041,China)  
Objective To establish an HPLC method for determination of anthraquinones content in Naomaitong.MethodsThe separation was performed on ODS column(250mm×4.6mm,5μm)of Kromasil.The mobile phase was a mixture of methanol-0.1% phosphoric acid solution(80∶20),the flow rate was 1.0 ml·min-1,and the wavelength was at 254 nm.ResultsThe total content of aloeemodin,rhein,emodin,chrysophanol and physcion was above 4%.The average recovery rate was100.54 %,RSD= 1.58%.Conclusion The method is simple,accurate,sensitive and can be used to control the quality of Liuwei Nengxiao Capsule.
【Fund】: 国家“十一五”支撑计划重大项目(No.07za026-011)
【CateGory Index】: R286.0
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【Co-citations】
Chinese Journal Full-text Database 2 Hits
1 SHI Tao~(1,2),MENG Xian-sheng~(2,3),LUO Guo-an~(2*),WANG Yi-ming~2,GONG Qian-feng~1(1.Jiangxi University of Traditional Chinese Medicine,Nanchang 330004,China;2.Modern Research Center of Traditional Chinese Medicine,Tsinghua University,Beijing 100084,China;3.Liaoning University of Traditional Chinese Medicine,Shenyang 110032,China);Studies on Qualitative and Quantitative Methods of Liangge Pills[J];Chinese Journal of Experimental Traditional Medical Formulae;2008-05
2 GAO Yu-ming,ZENG Rui(Ethnic Phamaceutical Institute of Southwest University of Nationalities,Chengdu 610041);Determination of rhein,emodin and chrysophanol in Weixinshu capsules by HPLC[J];Central South Pharmacy;2009-04
【Secondary Citations】
Chinese Journal Full-text Database 4 Hits
1 ;A study on Quality control for Dachengqi Granule[J];Hunan Guiding Journal of Traditional Chinese Medicine and Pharmacology;2002-04
2 LIU Dong-ping (Anqing Yicheng Hospital,Anqing246001,China);Quantitative Determination of Emodin and Chrysophanol in Dabaidu Capsules[J];Research and Practice of Chinese Medicines;2005-03
3 YAO Zhong qing (Institute of TCM, Nanjing Hospital of TCM, Nanjing Jiangsu 210001, China);Determination of emodin, chrysophanol, and physcion in HUANGLIAN SHANGQING PILL * by HPLC[J];Chinese Traditional and Herbal Drugs;2001-08
4 Cao Hong and Liu Yun(Institute for Drug Control of PLA,Beijing,100071);Determination of Rhein,Emodin,Chrysophanol,Physcion and Aloe-emodin in JinYiNiaoShi Granules and Radix Rhei by HPLC[J];CHINESE JOURNAL OF PHARMACEUTICAL ANALYSIS;1998-01
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