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《Lishizhen Medicine and Materia Medica Research》 2009-12
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Chemical Constituents from the Roots of Ilex pubescens

WU Ting1,3,ZHANG Xiao-qi2,3,WANG Ying 2,3,YE Wen-cai1,2,3,ZHAO Shou-xun1(1.Department of Natural Medicinal Chemistry,China Pharmacological University,Nanjing 210009,China;2.Institute of Traditional Chinese Medicine & Natural Products,Jinan University,Guangzhou 510632,China;3.Guangdong Provincial Key Laboratory of Pharmacodynamic Constituents of TCM and New Drugs Research,Jinan University,Guangdong 510632,China)  
Objective To study the chemical constituents of the roots of Ilex pubescens Hook.et Arn.Methods Chemical constituents were isolated and purified by several column chromatographic methods.The structures were identified by physicochemical properties and spectral data.Results Twelve compounds were isolated from the plant.Their structures were identified as ilexoside D(1),ilexgenin A(2),spinasterol(3),(+)-fraxiresinol-1-O-β-D-glucoside(4),liriodendrin(5),tortoside A(6),magnolenin C(7),syningin(8),sinapic aldehyde 4-O-β-D-glucopyrano-side(9),4,5-di-O-caffeoylquinic acid(10),β-sitosterol(11) and β-daucosterol(12),respectively.Conclusion Compounds 3,4 and 10 were isolated from this plant for the first time.
【Fund】: 国家自然科学基金(No.30625039);; 广东省自然科学基金(No.8351063201000003)
【CateGory Index】: R284.1
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