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《Journal of Instrumental Analysis》 2003-01
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Analysis of 13 Diuretics by HPLC

QIN Yang1, 2, ZHU Shao _ tang2, WANG Chao1, ZHAO Ming1, PENG Shi _ qi1 (1. College of Pharmaceutical Sciences, Peking University, Beijing 100083, China; 2. China Doping Control Center, National Research Institute of Sports Medicine, The State Sport General Administration, Beijing 100029, China )  
A procedure for simultaneous analysis of 13 diuretics in human urine by HPLC is described. The recoveries of liquid-liquid extraction(LLE) at acidic and basic pH and solid phase extraction were studied and compared. The detection limits of these compounds were below 5 ng at absolute amount. The method is suitable for diuretics screen in doping control. Excretion _ time profiles in human urines for some diuretics were also examined.
【CateGory Index】: O657.7
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【Citations】
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1 QIN Yang, ZHU Shao _ tang, ZHANG Chang _ jiu (China Doping Control Center, National Research Institute of Sports Medicine, The State Sport General Administration, Beijing 100029, China);Determination of Diuretics in Doping[J];Journal of Instrumental Analysis;2001-02
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1 WANG Yujun, XIONG Ying, CHEN Fei, LUO Guangsheng and DAI Youyuan(Department of Chemical Engineering, Tsinghua University, Beijing 100084,China);POLYSULFONE MICROSPHERES PREPARED BY MIXING TWO EMULSION SYSTEMS AND THEIR ABSORPTION CHARACTERISTICS[J];Journal of Chemical Industry and Engineering(China);2004-10
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