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《Journal of Tianjin Medical University》 2001-01
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The study on qualitative analysis and quantitative analysis method of Semen Cassiae in JiangZhiLing tablet

SONG Wei1,YANG Jin-Rong2, ZHANG Qing-Wei2, ZHANG Qi*, FANG Zhi-Zhong2(1.Tianjin Tanggu Hospital,300450;2.Tianjin Medical university Pharmacy College)  
Objective:The quality of JiangZhiLing tablet was controlled based on the qualitative analysis and quantitative analysis of Semen Cassiae.Methods: Qualitative analysis of Semen Cassiae was performed by TLC (thin-layer-chromatograph); HPLC(high-performance liquid chromatograph) was applied to determine the quantity of Emodin in Semen Cassiae at 365nm wavelength, in which ODS-C18 volume, 0.1% methanol flow phase and PCA (perchloric acid) were used. Results: Emodin's detection linear range is 0.05~0.8mg/L. The regression equation is Y=33.92+5391.86X, r=0.9998, average recovery is 98.70%. Conclusion: This method is simple and reliable enough to be used as the method of quality-control.
【CateGory Index】: R284
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4 ZHU Hong ZHU Ling Guangdong food and drug vocational college,Guangzhou 510520,China;Determination of the content of Emodin in Caoxiangwei tablets by RP-HPLC[J];Chinese Medicine Modern Distance Education of China;2008-05
Chinese Journal Full-text Database 4 Hits
1 He Liyi and Luo Shurong (Institute of Materia Medica, Chinese Academy of Medical Sciences, Beijing);STUDIES ON THE ANALYSIS OF ANTHRAQUINONE DERIVATIVES OF CHINESE MEDICINAL HERBS I. SEPARATION AND DETERMINATION OF CONSTITUENTS OF CHINESE RHUBARB[J];Acta Pharmaceutica Sinica;1980-09
2 Hong Xiaokun; Wang Zmhua; et al.(Shanghai University of TCM, Shanghai, 200032 );Qualitative and Quantitative Study on Muticomponent Anthraquinone Components in Chinese Patent Medicine with Radix et Rhizoma Rhei[J];CHINESE TRADITIONAL PATENT MEDICINE;1996-04
3 Wang Xuefen (National Instituents of Pharmacetical Research and Development ,Beijing 100083)Zheng Junhua;Chen Qingyun(Department of Pharmacognosy Beijing Medical University ,Beijing 100083);GC/MS in the study of chemical constituents of volatile oil from Rheumtanguticum[J];CHINESE PHARMACEUTICAL JOURNAL;1995-12
4 Cao Aimin, Sha Ming, Meng Shuzhi and Jiang Li (Liaoning College of Traditional Chinese Medicine, Shenyang 110032) Zhang Zhenxue (Liaoning Research and Development Center of New Chinese Drugs, Shenyang 110032);Determination of Chrysophanol in Semen Cassiae by HPLC[J];CHINA JOURNAL OF CHINESE MATERIA MEDICA;1997-02
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4 LIN yi-xing. (Hainan Provincial Institute for Drug Inspection, Haikou 570216, Hainan, P. R. China);Determination of the content of naringin by using high performance liquid chromatography.[J];China Tropical Medicine;2005-07
5 Cai Xiaoxia,Liu Zhongyi∥Pan Zhihua institute for Drug Congrol,Si Chuan,617000;Determination the Emodin Content in Gong Kangsu Capsules by RP Hplc[J];JOURNAL OF SICHUAN CONTINUING EDUCATION COLLEGE OF MEDICAL SCIENCES;2000-01
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9 ZHU Ri-ran,MIN Ju,YANG Bin(Affiliated Hospital of Shandong University of Traditional Chinese Medicine,Ji′nan 250011);Determination of puerarin in Xinanning Tablet by HPLC[J];Qilu Pharmaceutical Affairs;2009-06
10 Wang Ruiming et al. (Shanxi Institute of Traditional Chinese Medicine,Taiyuan Shanxi 030012);Determination of Matrine in Ganyu Capsules by TLC Scanning[J];Journal of Shanxi College of Traditional Chinese Medicine;2001-02
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2 YANG Xiaoyun (Qingdao Institute for Drug Control,Qingdao Shandong266071);Studies on Quality Standard of jieyu anshen Capsule[A];[C];2005
Chinese Journal Full-text Database 2 Hits
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2 LIU Jian-hua,ZHANG Su-mei,ZHANG Xin-hou,HUANG Jin-peng,LI Feng-juan(Engineering College of Animal Husbandry and Veterinary Science,Henan AgricultruraL University,Zhengzhou,Henan 450002;China);Determination of Emodin in Different Processed Rhubarb by HPLC[J];Chinese Journal of Veterinary Drug;2006-03
【Secondary References】
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1 LIU Yi,ZHANG Li-yan,YANG Yu-qin,LI Jian,ZHONG Zheng-ling,XIE Yu(Guiyang College of Traditional Chinese Medicine,Guiyang 550002,China);Study on the quality control standard of Wuzhuyu Jiangya granules[J];Chinese Journal of Pharmaceutical Analysis;2009-01
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