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《Journal of Tianjin Medical University》 2001-01
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The study on qualitative analysis and quantitative analysis method of Semen Cassiae in JiangZhiLing tablet

SONG Wei1,YANG Jin-Rong2, ZHANG Qing-Wei2, ZHANG Qi*, FANG Zhi-Zhong2(1.Tianjin Tanggu Hospital,300450;2.Tianjin Medical university Pharmacy College)  
Objective:The quality of JiangZhiLing tablet was controlled based on the qualitative analysis and quantitative analysis of Semen Cassiae.Methods: Qualitative analysis of Semen Cassiae was performed by TLC (thin-layer-chromatograph); HPLC(high-performance liquid chromatograph) was applied to determine the quantity of Emodin in Semen Cassiae at 365nm wavelength, in which ODS-C18 volume, 0.1% methanol flow phase and PCA (perchloric acid) were used. Results: Emodin's detection linear range is 0.05～0.8mg/L. The regression equation is Y=33.92+5391.86X, r=0.9998, average recovery is 98.70%. Conclusion: This method is simple and reliable enough to be used as the method of quality-control.
【Key Words】： JiangZhiLing tablet Semen Cassiae Emodin TLC HPLC
【CateGory Index】： R284
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