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《Natural Product Research and Development》 2009-05
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Analysis of Anthraquinones in Different Samples of Aloe with HPLC-DAD and LC-MS/MS

CHEN Xin-xia1,ZHANG Yu-hang2,LIN Ying1,XIE Zhi-yong1,WAN Jin-zhi11Laboratory for Pharmaceutical Analysis and Quality Evaluation,School of Pharmaceutical Sciences,Sun Yat-sen University,Guangzhou 510006,China;2The No.5 People's Hospital of Zhuhai,Zhuhai 519000,China  
A HPLC-DAD and LC-MS/MS method was established not only for the assay of anthraquinones but also for the determination of aloin and aloe-emodin in different samples of aloe.The analysis was performed on Nucleodur-silica C18(250 mm4.6 mm,5 μm)column with a methanol-water(containing 0.4% acetic acid) gradient at ambient temperament.The flow rate was 1.0 mL/min,the wavelength scanned from 190-370 nm and the detection was at 254 nm and 356 nm.The ionic source of LC-MS was ESI.Samples were analyzed in two modes:MS and MS/MS full can modes.Aloin A,B and aloe-emodin were the main anthraquinones in different samples of aloe while rhein,emodin,chrysophanol and physcion were not found;the aloe powder contained the highest amount of aloin.The method could be used to control the quality of aloe product.
【Fund】: 2005年度广东省中医药管理局计划项目(1050163);; 2005年度珠海市科技计划项目(PC20051072)
【CateGory Index】: R284.1
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【Citations】
Chinese Journal Full-text Database 2 Hits
1 Yang Wenyuan and Wang Tian yong  (The Center of Analysis and Testing,Ningxia University,Yinchuan 750021;Simultaneous Determination of Aloe Emodin and Emodin in Cassia tora L.by Reversed Phase High Performance Liquid Chromatography[J];ANALYTICAL LABORATORY;1997-02
2 LU Chaoguo1),WANG Hongzhuan2),LI Yanhong1),LIU Guoji1),LUO Tingliang1) 1)Institute of Chemical Engineering,Zhengzhou University,Zhengzhou 450001 2)Nylon 66 Salt Company of China Shenma Group,Pingdingshan 467013;Simultaneous determination of Aloin and Aloe-emodin in Aloe by HPLC[J];Journal of Zhengzhou University(Medical Sciences);2008-03
【Co-citations】
Chinese Journal Full-text Database 4 Hits
1 MA Jing-jun~1,FANG Zheng~1,WU Qiu-hua~1,SUN Huan-ming~2,WEN Ya-jun~2(1.Agricultural University of Hebei,Baoding 071001, China;2.Beijing Agro-Tech Extension Station, Beijing 100029, China);On determination of Aloin and Aloe-emodin in Aloe barbadensis mill by HPLC[J];Journal of Agricultural University of Hebei;2005-02
2 CHEN Wei,ZHANG Ya-feng,LUO Hong-bin,LIN Xin-hua,HUANG Li-ying(College of Pharmacy, Fujian Medical University,Fuzhou 350004;China);Determination of Aloe-emodin by Differential Pulse Voltammetry[J];Strait Pharmaceutical Journal;2004-05
3 YU Chao, LAN Hongmei, WANG Yu (Chongqing Institute of Traditional Chinese Medicine, Chongqing 400065,China);Determination of Anthraquinone Compounds in Cemen cassiae by RP-HPLC[J];Primary Journal of Chinese Materia Medica;2002-02
4 GONG Kui,SUN Xiao-yun,REN Fei,GUAN Peng-lai(Shenyang Institute of Aeronautical Engineering,Liaoning Shenyang 110136,China);Analysis of Trace Elements in Aloe[J];Contemporary Chemical Industry;2009-05
【Secondary Citations】
Chinese Journal Full-text Database 3 Hits
1 HUANG Li-ying, LIN Xin-hua, LAI Li-Min, ZHENG Yan-jie, LIU Si-yi College of Pharmacy, Fujian Medical University, Fuzhou 350004, China;Determination of Aloe-Emodin and Aloin without Separation by Dual-Wavelength Spectrophotometry[J];Journal of Fujian Medical University;2005-01
2 Li Jinxin Feng Mei (Ninxia Agricultural College, Yonging Ningxia, 750105);MEDICINAL EFFECT AND DEVELOPMENT OF BARBADOS ALOE[J];JOURNAL OF NINGXIA AGRICULTURAL COLLEGE;1999-04
3 FANG Zi Ji,XU Zi Ming,XU Xia (401th Hospital of PLA China,Shandong Qingdao 266071);Determination of Aloin and Aloe-emodin in Aloe by HPLC[J];Chinese Journal of Hospital Pharmacy;2002-09
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