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《ACTA ENERGIAE SOLARIS SINICA》 1998-03
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THE EFFECT OF SULFIDATION PARAMETERS ON THE FORMATION OF POLYCRYSTALLINE FeS_2 THIN FILMS

Meng Liang Tu Jiangping Liu Maosen (Zhejiang University,Department of Materials Science and Engineering,Hangzhou 310027)  
The polycrystalline FeS 2 thin films are prepared by thermal sulfidation of iron layers sputtered on glass substrates.In this paper,the effect of the sulfidation process (sulfidation temperature and annealing time)on the formation of FeS 2 thin films has been investigated.The test results show that the equiaxed FeS 2 grains in the preferred orientation can be synthesized when the sulfidation temperature is in 400—600℃ and the annealing time in 10—30h.There is a quicker growth of FeS 2 crystal if the iron layers is sulfurated for 10 h at 400℃. Above 400℃ and 10 h the rate to form FeS 2 crystal increases insignificantly with the increase of sulfidation temperature or annealing time.
【CateGory Index】: TQ031.9
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