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《Acta Physico-chimica Sinica》 2004-06
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Synthesis of MoO_x Nano-arrays on Anodic Aluminum Oxide Template by Thermal Diffusion

Wang Fan Zhang Yu-Ling Wei Qing-Shuo Wu Kai Xie You-Chang (State Key Laboratory for Structural Chemistry of Unstable and Stable Species, Institute of Physical Chemistry, College of Chemistry and Molecular Engineering, Peking University, Beijing 100871)  
MoO2 nano-arrays were simply prepared by reduction of thermally diffused MoO3 on anodic aluminum oxide(AAO) template. The structure and morphology of the nano-arrays were studied by XRD, SEM, TEM and HRTEM. The results showed that, after hydrogenation of the evaporates under 600 ℃ in H2/N2 mixture, single crystalline MoO2 nanotubes/nanowires were produced on 70 nm AAO template, while on 50 nm AAO template yielded was the piling-up of MoO2 nanocrystallites in nanotubes. Addition of ethanol into the powdered MoO3 precursors greatly improved the morphology of the nanowires. Further reduction of MoO2 at above 650 ℃ in H2 led to the production of Mo nanotube arrays.
【Fund】: 国家自然科学基金(20125309 90206012);; 国家重点基础研究发展规划(G2000077503);; 教育部博士点基金和留学回国人员基金资助项目~~
【CateGory Index】: TB383
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