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《Acta Physico-Chimica Sinica》 2007-12
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Hydrogen Production from Water Splitting Using Perylene Dye-Sensitized Pt/TiO_2 Photocatalyst

LIU Fu-Sheng1,2 JI Ren2 WU Min1 SUN Yue-Ming1,(1School of Chemistry and Chemical Engineering,Southeast University,Nanjing 210096,P.R.China;2Department of Chemistry and Materials Science,Nanjing Forestry University,Nanjing 210037,P.R.China)  
The photocatalyst(DPPBI/Pt/TiO2)was prepared using N,N'-di(4-pyridyl)-3,4,9,10-perylene tetracarboxylic acid bisimide(DPPBI)sensitized Pt/TiO2 and characterized by infrared spectroscopy(IR),UV-Vis diffuse reflectance spectroscopy(UV-Vis DRS),scanning electron microscopy(SEM),X-ray photoelectron spectroscopy(XPS),and X-ray diffraction(XRD).The results of characterization showed that the crystal form of TiO2 was anatase,Pt was highly dispersed on the surface of TiO2 and DPPBI was adsorbed on the surface of Pt/TiO2 in DPPBI/Pt/TiO2.Hydrogen production from water splitting using photocatalyst(DPPBI/Pt/TiO2)was studied.It has been found that the rate of hydrogen evolution reaches 6.69 μmol·h-1·g-1 under visible light irradiation for 8 h with 300 W Xe-lamp cold light source when 250 mL reactive liquid contains 0.8 g·L-1 photocatalyst(0.1% DPPBI/0.4%Pt/TiO2)and 0.2 mol·L-1 KI.
【Key Words】: Perylene Dye Photocatalyst Hydrogen production
【Fund】: 江苏省高技术研究基金(BG2005034);; 教育部高等学校博士点科研基金(20030286012)资助项目
【CateGory Index】: TQ116.2;O643.3
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