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《Chinese Journal of Modern Applied Pharmacy》 1998-03
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Synthesis of 3,5-bis[acetyl(2,3-dihydroxypropyl) amino]-N-(2-hydroxyethyl)-2,4,6-triiodo-benzamide

Zhou Pel ( Zhou P ), Luo Shineng ( Luo SN ), Xie Minghao ( Xie MH), et al ( Jiangsu Institute of Nuclear Medicine , State Key Laboratory of Nuclear Medicine , Wwd 214063)  
The synthesis of novel non - ionic X - CT contrast medium {3,5 - bis [ acetyl (2,3- dihydroxypropyl)amino] - N - (2 - hydroxyethyl) - 2,4,6- triiodo - benzamide} is reoported. This compound was synthesized through nitration, esterification, amidation, reduction, iodization, acetylation, alkylation using 3,5 -dinitrobenzoic acid as meterial. Element analysis, IR and 1 HNMR of synthetic product were conformable to the chemical structure of 3,5 - bis [acetyl (2,3 - dihydroxypropyl) amino] - N - (2 - hydroxyethyl) - 2,4,6 - triiodo - benzamide.
【CateGory Index】: R914
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【Citations】
Chinese Journal Full-text Database 1 Hits
1 LUO Shi-Neng; XIE Min-Hao; XI Yue-Fen; ZHANG Man-Da;MENG Hong; LIU Ya-Ling; HUANG He-Yun; ZOU Pei(State Key Laboratory of Nuclear Medicine, Jiangsu Institute of Nuclear Medicine, Wuxi 214063);SYNTHESIS OF NON-IONIC X-CT CONTRAST MEDIUM IOHEXOL[J];CHINESE JOURNAL OF PHARMACEUTICALS;1995-10
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 WANG Hui-li(Wuhan Chemical Industry Research Institute Co.,Ltd.,Wuhan 430064,China);Preparation of 5-Nitroisophthalic Acid Dimethyl Ester[J];Chemistry & Bioengineering;2009-10
2 Xie Heqing,Li Jingfen (Faulty of Life Science Huzhou Teachers College Huzhou 313000 );Improvement of Synthesis Techics of Medical Intermediat 17α-Hydroxy-21-iodopregn Progesterone[J];China Chemicals;2008-05
3 ZHANG Lai-guo 1,2,LUO Shi-neng *1,2,LIU Xiao-ya1,XIE Min-hao2,ZOU Pei2,LIU Ya-ling2,HE Yong-jun2 (1.School of Chemical and Material Engineering,South Yangtze University,Wuxi 214036,China;2.Jiangsu Institute of Nuclear Medicine,Wuxi 214063,China);The synthesis of N,N′-bismethyl-N,N′-bis-(2,3,4,5,6-pentahydroxyhexyl)-2,3,5,6-tetraiodoterephthalamide[J];Chemical Reagents;2006-07
4 LUO Shi neng 1,2 SHEN Yong jia 1, XIE Min hao 2, LIU Ya ling 2, ZOU Pei 2, HE Yong jun 2 (1.East China University of Science and Technology, Shanghai 200237, China; 2.Jiangsu Institute of Nuclear Medicine, Jiangsu Wuxi, 214063, Chin;Study on Viscosity of Non-ionic X-ray Contrast Agents[J];Huaxue Shijie (Chemical World);2002-08
5 LIU Ya ling, LUO Shi neng, XIE Min hao, HE Yong jun, ZOU Pei, YANG Zheng (Jiangsu Institute of Nuclear Medicine, Jiangsu Wuxi 214063, China);Synthesis of 5-(β-Hydroxyl-α-naphthalene azo)-N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide and Its Application[J];Huaxue Shijie (Chemical World);2003-05
6 ZHANG Lai-guo1,2,LUO Shi-neng2,1*,XIE Min-hao2,LIU Xiao-ya1,ZOU Pei2,LIU Ya-ling2,HE Yong-jun2 (1.School of Chemical and Materials Engineering,Southen Yangtze University,Wuxi 214122,China;2.Jiangsu Institute of Nuclear Medicine,Wuxi 214063,China);Synthesis of N,N′-Bis(Dihydroxypropxyl)-2,3,5,6-Tetraiodoterephthalamide[J];Journal of Southern Yangtze University(Natural Science Edition);2007-01
7 SUN Yue-jun,ZHENG Guo-jun*(College of Life Science and Technology,Beijing University of Chemical Technology,Beijing 100029,China);Optimization of synthetic process for iohexol[J];Chemical Reagents;2012-02
8 Xie Heqing,et al(Faulty of Life Science,Huzhou Teachers College,Huzhou 313000);Orthogonal Experimental Design in 17α-hydroxy-21-iodine Progesterone Improved Synthesis of the Application[J];Journal of Mathematical Medicine;2008-05
9 Xie Minhao(Xie MH),Luo Shineng(Luo SN),Liu Yaling(Liu YL),et al(Jingsu Institute of Nuclear Medicine,Wuxi 214063);The effects of booster on the stability of iohexol injections[J];CHINESE JOURNAL OF MODERN APPLIED PHARMACY;2000-04
10 XIE Min Hao, LUO Shi Neng, HE Yong Jun, LIU Ya Ling, ZOU Pei (Jiangsu Institute of Nuclear Medicine, State Key Laboratory of Nuclear Medicine, Wuxi 214063);Synthesis of 5-Methoxyacetamido-2,4,6-triiodoisophthaloyl Dichloride[J];Chinese Journal of Pharmaceuticals;2001-03
China Proceedings of conference Full-text Database 1 Hits
1 ;The development of iodinated X-ray contrast agents[A];[C];2004
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