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《Modern Scientific Instruments》 2006-03
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Determination of Tetracyclines Residue in Animal Tissues by High Performance Liquid Chromatography

Hu Haishan,Long Zhouxiong,Wan Chunhua(Jiangxi Institute of Analysing and Testing,Nanchang 330029,China)  
The residual of oxytetracycline(OTC),tetracycline(TC),chlortetracycline(CTC) in animal tissues could be separated and determined by high performance liquid chromatography,after deproteinized by 5% HClO4.A Kromasil C18 column(250 × 4.6mm,5μm) was used;0.01mol/L NaH2PO4.2H2O(pH=3)-60/40 acetonitrile-water was used as a mobile phase;The flow rate of the mobile phase was kept at 1.0mL/min;The residues using gradient elution were monitored by UV detector at 355nm.The recoveries of tetracyclines were 89.4 ̄101.2%,and the relative standard were less than 3.50%.This method was reliable,sensitive,economical and rapid.
【Fund】: 江西省科学技术厅科技攻关重大项目“畜禽、水产品中四环素及磺胺类药物残留的研究”
【CateGory Index】: O657.72
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