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《Journal of The Chinese Rare Earth Society》 2001-06
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Application of Microwave Reaction in Preparation of Rare Earth Fluorescence Complex Materials

CHEN Wei wei, YANG Zhan lan, LIU Ming zhao, XIA Guo yao, MAO Yu chun, WENG Shi fu, WU Jin guang (State Key Laboratory of Rare Earth Material Chemistry and Applications, College of Chemistry and Molecular Engineering, Peking University, Beijing 10  
The application of synthesizing rare earht fluorescence complex materials was studied by using microwave heating way. The results indicate that the microwave heating way is a good method for preparation of rare earth fluowescence complex materials. For preparation of the Tb o aminobenzoate complex, the optimal initiator is water. As a reactant, Tb(OAC) 3 is better than Tb(OH) 3 because Tb(OH) 3 is insoluble in water. When total amount of reactants was 1 g, the optimal adding amount of water (inducing reagent) was 40 μl and the optimal microwave irradiation time was 4 min.
【Fund】: 国家重点基础研究发展规划资助项目 (G19980 613 11)
【CateGory Index】: TQ422
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