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《Chinese Journal of Information on Traditional Chinese Medicine》 2010-06
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Simultaneous Determination of Five Contents of Rhubarb in Huangxiong Kangshuan Capsule by HPLC

HAN Yan-quan1,HONG Yan2,XIA Lun-zhu1,et al(1.The First Affiliated Hospital,Anhui College of TCM,Grade 3 Laboratory of TCM Preparation,State Administration of TCM,Hefei 230031,China;2.Anhui College of TCM,Hefei 230031,China)  
Objective To establish an HPLC method for the determination of Aloeemodin,Rhein,Chrysophanol,Emodin and Physcione in Huangxiong Kangshuan Capsule.Methods The determination was performed on Kromasil-C18 column(250 mm×4.6 mm,5 μm) with mobile phase consisted of methanol-0.1% phosphoric acid(85:15) at a flow rate of 1.0 mL/min.Column temperature was 25 ℃.The UV detection wavelength was set at 254 nm.Results The calibration curves were linear in the range of 0.230~3.68 μg(r=0.999 8) for Aloeemodin,0.224~3.584 μg(r=0.999 9) for Rhein,0.223~3.568 μg(r= 0.999 8) for Emodin,0.257~4.112 μg(r=0.999 9) for Chrysophanol and 0.287~4.592 μg(r=0.999 8) for Physcion.The average recovery was 98.48%,98.10%,99.08%,100.34%,97.52% and RSD was 1.39%,1.54%,1.44%,2.40%,2.03% respectively.Conclusion The determination method is simple,reliable,accurate,and it can be used for quality control of Huangxiong Kangshuan Capsule.
【CateGory Index】: R286
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【Citations】
Chinese Journal Full-text Database 2 Hits
1 Xie Daojun , Jiang Tingzhan , Li Zhihe , et al. (The First Affiliated Hospital, Anhui College of Traditional Chinese Medicine, Anhui 230031);Effects of Tongnaojing Capsules on Hyperinsulinemia and Insulin Sensitivity in the Rat Model of Insulin Resistance Complicated with Focal Cerebral Ischemia[J];Journal of Beijing University of Traditional Chinese Medicine;2003-01
2 TANG Hongmei1,LI Detang2,YAN Xue2,QIU Zhenwen1,CAI Qingqun1(1.The First Affiliated Hospital of Guangzhou University of Chinese Medicine,Guangzhou 510405,China;2.Guangzhou University of Chinese Medicine,Guangzhou 510405,China);Simultaneous Determination 5 Contents of the Rhubarb in the Liaojin Film by HPLC[J];Chinese Journal of Modern Applied Pharmacy;2009-05
【Co-citations】
Chinese Journal Full-text Database 1 Hits
1 Gong Peng,Chen Zhen,Xu Dujuan Department of Pharmacy,the First Affiliated Hospital of Anhui Medical University,Hefei 230022,China;Simultaneous determination of the contents of emodin,chrysophanol and physcione in Bahao burn slurry via HPLC[J];Anhui Medical Journal;2010-02
【Secondary Citations】
Chinese Journal Full-text Database 9 Hits
1 Zhou Xiying,et al;Study on Method for Eexperimental Cerebral Ischemia in Rat[J];Hebei Medical Journal;1997-03
2 ;Determination of Archen and Chrysophanol in Liuhuangzhibao Pills with RP-HPLC[J];Guiding Journal of TCM;2007-08
3 Zhang Yonghong (Department of Pharmacy,Lanzhou Medical College);A Method Selection of Extract Anthraquinone from Chinese Rhubarb[J];JOURNAL OF LANZHOU MEDICAL COLLEGE;1996-02
4 Dong Fuyun\ Cao Youling\ Tang XinzhiDepartment of Biochemistry, Tianjin Medical University (300070);Study on High Sucrose Diet-induced Insulin Resistance inSprague-Dawley Rats[J];LABORATORY ANIMAL SCIENCE AND ADMINISTRATION;1998-04
5 Yang Zhifeng (Ningbo Institute for Drug Control,Ningbo,Zhejiang,China 315040);Determination of Emodin and Rhein in Yankening Tablets by HPLC[J];China Pharmaceuticals;2007-12
6 DU Li yun 1, MO Ya xiong 2 (1. Yunnan Institute for Drug Control, Kunming 650011, China;2. Kunming Medical College No.1 Attached Hospital, Kunming 650011, China);Content Determination of Emodin in Danqing Tablet by TLC scanning[J];CHINESE TRADITIONAL PATENT MEDICINE;2000-09
7 LI Shu ying 1, GUO Zeng jun 2, WANG Li 3 (1.Shanxi Xinghua Institute of Materia Medical, Xi'an 710075, China; 2.Pharmacy College, Xi'an Jiaotong University, Xi'an 710061, China; 3.First Clinical Medical College, Xi'an Jiaotong University, Xi'an 71;Determination of Emodin, Chrysophanol and Baicalin in Three Yellows Tablets by HPLC[J];Chinese Traditional Patent Medicine;2001-06
8 HU Yun chang (Zhejiang Provincial Medical School, Ningbo 315100, China);Determination of Emodin in Kangyanning Granules by TLC-scanning[J];Chinese Traditional Patent Medicine;2002-09
9 YANG Liu1,XU Shun-jun2(1.College of Chinese Medicine,Guangzhou University of TCM,Guangdong Guangzhou 510405,China;2.Nstitute of Life and Health Engineering,Jinan University,Guangdong Guangzhou 510630,China);Study on content changes of the anthraquinones of Radix et Rhizoma Rhei by different extract methods[J];Chinese Journal of Hospital Pharmacy;2007-07
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