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《Journal of Medical Science Yanbian University》 2013-02
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Content detection of aloin and aloe emodin in active aloe aphtha sustained-release film by high performance liquid chromatography

LIN Jing;FANG Xian-hao;Yanbian University College of Clinicine;Dpartment of Oral Teaching and Research,Yanbian University;  
OBJECTIVE To establish the condition of HPLC method for detecting the content of aloin and aloe emodin in active aloe aphtha sustained-release film,and to formulate the quality specifications for active aloe film.METHODS Using a column of ZORBAX-SA-C 18(5μm,200.0mm×4.6mm)with a mobile phase of methanol:water(volume ratio as 70∶30),1.0mL/min of flow velocity,25℃of post temperature,and sample size of 20μL,the content of aloin was detected at 360nm and of aloe emodin at 430nm.RESULTS Formulated the quality specifications of aloin and aloe emodin in one of active aloe film(1.0cm×1.0cm) was shown that aloin content was 40.67μg and aloe emodin content was 1.8μg.CONCLUSION The established the condition of HPLC method is rapid,simple and accurate,and can be used for the simultaneous determination of aloin and aloe emodin in aloe at the same time.
【Fund】: 延边大学资助项目(编号:200726)
【CateGory Index】: R286
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