Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Rock and Mineral Analysis》 2003-04
Add to Favorite Get Latest Update

Determination of Boron, Arsenic and Sulfur in Geological Samples by Inductively Coupled Plasma Atomic Emission Spectrometry with Sample Treatment by Pressurized Decomposition

LI Bing, MA Xinrong, YANG Hongxia, HE Hongliao (National Research Center of Geoanalysis, Beijing 100037, China)  
The application of ICPAES with an argonfilled CID spectrometer for determination of B, As and S in soils and sediments is described. H3PO4 is used in a pressurized acid digestion method with HF/HNO3/HClO4 for preventing the analytes from volatilization. In order to compensate for the signal drift caused by absorption of remainder air or water vapor, Se 196.0 nm is used as internal standard. The detection limits (10σ,DF=100) are 3.28,2.61,9.58 μg/g (dry mass) for boron, arsenic and sulfur respectively. The accuracy and precision of the method are demonstrated by analyzing different Chinese geological certified reference materials (soils and stream sediments). The results found are in a reasonable agreement with the certified values.
【Fund】: 国土资源部地质大调查实施项目(20026019;DKD9904013)
【CateGory Index】: P575
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【References】
Chinese Journal Full-text Database 10 Hits
1 LI Bing, YANG Hong xia (National Research Center of Geoanalysis, Beijing 100037, China);APPLICATIONS OF INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY IN EARTH SCIENCE[J];Earth Science Frontiers;2003-02
2 LI BingNational Research Center of Geological Analysis, Beijing, 100037;Application of Inductively Coupled Plasma Mass Spectrometry in Geological Survey[J];Geological Review;2006-06
3 YANG Shen-rong1, GE Tong2, LI Qing-cai1, ZHAO Qing-ling1(1. Lunan Geo-engineering Exploration Institute of Shandong Province, Yanzhou 272100, China;2. Huangdao Entry-exit Inspection And Quarantine Bureau, Qingdao 266555, China);Determination of Sulfur in Sulfide Ore by Inductively Coupled Plasma-Atomic Emission Spectrometry[J];Analysis and Testing Technology and Instruments;2010-04
4 CAO Chen-Dong WEI Yi(Lanzhou Testing and Quality Supervision Center for Geological and Mineral Products,The Ministry of Land and Resources,Lanzhou 730050,P.R.China);Rapid Determination of Total Sulfur in Soil by Inductively Coupled Plasma Atomic Emission Spectrometry[J];Chinese Journal of Spectroscopy Laboratory;2010-04
5 ZHA Li-Xin MA Ling LIU Hong-Qing SUN Wei(Anhui Province Geological Experiment Research Institute,Hefei 230001,P.R.China);Determination of Micro Sulphur in Geochemistry Samples by Inductively Coupled Plasma Optical Emission Spectrum[J];Chinese Journal of Spectroscopy Laboratory;2011-05
6 ZHANG Ting-zhong1,2,YANG Xi-sheng1(1.Zhangye Mine Exploration Institute of Gansu Nonferrous Metal Geological Exploration Bureau,Zhangye 734000,China; 2.Hexi Analysis and Testing Center of Gansu Nonferrous Metal Geological Exploration Bureau,Zhangye 734000,China);Quick Determination of Boron and Sulfur in Soil By ICP[J];Gansu Metallurgy;2012-03
7 LIU Jiu-Fen~(a,b) LIU Xiao-Hang~b ZHAO Zheng-Peng~b LIU Shu-Liang~b a(Changan College Resource Institute,Xian 710000,P.R.China) b(The 7th Gold Detachment of Chinese People's Armyed Police Force,Yantai,Shandong 264000,P.R.China);Simultaneous Determination of Cu,Pb,Zn,Fe,Mn,Mo and S in Soil Samples by ICP-AES With Aqua Regia Digesting[J];Chinese Journal of Spectroscopy Laboratory;2013-02
8 WEI Zhen-Hong DU Zuo-Peng LIU Huai-Qi SUN Feng-Quan CHEN Hong(Qinghai Province Geology Ore Test Application Center,Xining 810008,P.R.China);Determination of Sulfur in Multi-Purpose Regional Geochemical Survey Sample by ICP-OES[J];Chinese Journal of Spectroscopy Laboratory;2013-04
9 Kuang Fangcheng;Fujian Province Geological Test Research Center;;Determination of the Different Content of Sulfur in Geological Samples by High Frequency IR Carbon-sulfur Analyzer[J];Geology of Fujian;2013-03
10 WANG Hong1,SHA De-ren2,LI Yong2,WU Yong-kun2 (1.Dept.of Juri-Chemistry,Jiangsu Police Institute,Nanjing 210012,China;2.State Supervision and Testing Centre of Quality of Glass Fibre Products,Nanjing 210012,China);ICP-AES Determination of Total Amount of Sulfur in Glass[J];Physical Testing and Chemical Analysis(Part B:Chemical Analysis);2007-03
【Citations】
Chinese Journal Full-text Database 2 Hits
1 Zeng Xianjin, Miao Xiuzhen and Huang Benli(Changchun Institute of Applied Chemistry, Academia Sinica);SIMULTANEOUS DETERMINATION OF TOTAL BORON AND OTHER MICRO AND MAJOR ELEMENTS IN SOILS AND SEDIMENTS BY INDUCTIVELY COUPLED PLASMAATOMIC EMISSION SPECTROMETRY[J];Chinese Journal of Analytical Chemistry;1987-12
2 SHI Shi yun, WEN Hong li, LI Bing, HE Hong liao, LU¨ Cai fen (National Research Center of Geoanalysis, Beijing 100037, China);Determination of Carbon and Sulfur in Geological Samples by High Frequency IR-Absorption Spectrometric Method[J];Rock and Mineral Analysis;2001-04
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 ZHANG Hong,ZHENG Hua,GUO Yuan-heng,MA Li-yi,GAN Jin,ZHANG Zhong-heKey Laboratory of Cultivation and Utilization of Resource Insects,State Forestry Administration,Research Institute of Resource Insects,Chinese Academy of Forestry,Kunming 650224,China;Advance in cochineal red pigment refined process and utilization[J];Journal of Dalian Polytechnic University;2010-06
2 Zhang Zhilong, Cai Shuxing and Chen Shougen(Research Institute of Geology for Mineral Resources, China National Nonferrous Metals Industry Corporation, Guilin);Analysis of Rocks and Minerals[J];Chinese Journal of Analysis Laboratory;1990-04
3 Wu Cheng and Yan Juying(Shanghai Research Institute for Meterials, Ministry of Machine Building and Electronics Industries);Analysis of Light and Heavy Metals[J];Chinese Journal of Analysis Laboratory;1990-04
4 Chen Xinkun(Department of Chemistry, Nankai University, Tianjin 300071),;Atomic Emission Spectroscopy[J];Chinese Journal of Analysis Laboratory;1991-04
5 SHAO Xin LI Xiao-Dan HE Qi-Sheng (Yichang Institute of Geology and Mineral Resources,Yichang,Hubei 443003,P.R.China);Determination of Beryllium,Boron and Gallium in Geological Samples by ICP-AES[J];Chinese Journal of Spectroscopy Laboratory;2006-05
6 YANG Xiao-Li HE Qi-Sheng LI Xiao-Dan (Central-South Center for Mineral Resoures Supervision and Test,Yichang Institute of Geology and Mineral Resources, Yichang,Hubei 443003,P.R,China);Determination Zn and B in Leaves of the Orange by ICP-AES[J];Chinese Journal of Spectroscopy Laboratory;2006-05
7 CAO Chen-Dong WEI Yi(Lanzhou Testing and Quality Supervision Center for Geological and Mineral Products,The Ministry of Land and Resources,Lanzhou 730050,P.R.China);Rapid Determination of Total Sulfur in Soil by Inductively Coupled Plasma Atomic Emission Spectrometry[J];Chinese Journal of Spectroscopy Laboratory;2010-04
8 Chen Chaozi;Yang Jingrong(Institute of Geography,The Chinese Academy of Sciences,Building 917,Datunlu,Beijing 100101,P.R.China) Tian Xiaoya(Commission for Integrated Surrey of Natural Resources,The Chinese Academy of Sciences,Building 917,Datunlu,Beijing;Simultaneous Determination of Boron and Other Trace Elements,Macro-Elements in Soil and Deposit by ICP-AES[J];CHINESE JOURNAL OF SPECTROSCOPY LABORATORY;1995-05
9 SHAO Xin LI Xiao-Dan ZHU Yuan-Yuan YANG Mei(Wuhan Institute of Geology and Mineral Resources,Wuhan 430205,P.R.China);Determination of Trace Boron in Geological Samples by ICP-MS with Closed-Digestion[J];Chinese Journal of Spectroscopy Laboratory;2012-05
10 Kuang Fangcheng;Fujian Province Geological Test Research Center;;Determination of the Different Content of Sulfur in Geological Samples by High Frequency IR Carbon-sulfur Analyzer[J];Geology of Fujian;2013-03
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 ZHA Li xin, LIU Hong qing, MA Ling, DAI Xian rong(Institute of Geological Experiment of Anhui Province, Hefei 230001,China);IMMEDIATE DETERMINATION OF SULFATE IONS IN NATURAL MINERAL WATER BY ICP-AES[J];Geology of Anhui;2002-01
2 YANG Xiao-zhi XIA Qun-ke CHEN Hao WU Yuan-bao (1 Chemistry Geodynamics Research Laboratory,School of Earth and Space Science,University of Science and Technology of China,Hefei 230026,China);ION PROBE TECHNOLOGY APPLICATED IN GEOCHEMISTRY RESEARCH[J];Geology of Anhui;2004-01
3 MU Zhiguo\ GAO Yongjun (Department of Geology,Peking University,Beijing,100871);The Laser Microprobe Dating Drives K-Ar Geochronology into A New Milestone at the End of 20th Century[J];Acta Scicentiarum Naturalum Universitis Pekinesis;2001-01
4 LIU Junlong, OUYANG Baohua(Jingzhou Feilihua Quartz Glass Co.,Ltd,Jingzhou 434001, China);Study on Determination of B in Silex Glass by GFAAS[J];Glass & Enamel;2003-05
5 Li Xiao-juan;SEEDS IN FLOAT GLASS AND REFINING WITH GLAUBERS SALT[J];Glass;2005-02
6 LIN Ping~1, ZHANG Xin-quan~2, ZHANG Jin~1, KONG Gan-liang~1 (1.Jiangxi Centre of Diseased and Controlled, Nanchang 330029,China;2.Jiangxi Institute of Analyzing and Testing, Nanchang 330029,China);Determination of Rare-Expensive Elements in Geological Samples by Inductively Coupled Plasma Mass Spectrometry[J];Journal of Jiangxi Normal University (Natural Sciences Edition);2004-06
7 Li Chengfeng Xiao Jifeng ( Geological Research Institute of the Shengli Oil Field, Shandong Province );THE APPLICATION OF TRACE ELEMENT TO THE STUDY ON PALEOSALINITIES IN SHAHEJIE FORMATION OF DONGYING BASIN SHENGLI OILFIELD,[J];Acta Sedimentologica Sinica;1988-04
8 XU Pu de, ZHANG Hai yan (ANDA Aviation Forging Co Ltd , Anshun 561005, China);Study on Determination of Element B in High-temperature Alloys by ICP-AES[J];Journal of Materials Engineering;2002-12
9 Li Shushen(China Institute for Radiation Protection,Taiyuan,030006);Review of Nuclear Environmental Science over the Last 40 Years[J];Radiation Protection Bulletin;2002-04
10 Meng Wenbin Ge Hong Yu Haiyan Wang Guanghua Wu Zhixin Shang Dongtao (Shenyang San Ding Environmental Protection Co. Ltd.,Shenyang,110015);Standards for Indoor Radiation[J];Radiation Protection Bulletin;2003-03
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 WANG Yuan-zhong et al(Institute of Medicinal Plant,Yunnan Academy of Agricultural Sciences,Kunming,Yunnan 650223);Determination of Effective Boron in the Soil for Boletus tomentipes Growth by ICP-MS[J];Journal of Anhui Agricultural Sciences;2009-15
2 SHA Deren1,LI Yong1,WU Yongkun1,YANG Chunying1,JIN Xuexia1,ZHANG Xuelei2,CHEN Jianliang3(1.Quality Testing Center of Nanjing Fiberglass Research & Design Institute,Nanjing 210012;2.Beijing Office of Leeman Labs Inc.,Beijing 100029;3.Jushi Group Co.Ltd,Tongxiang 314500);Revision of GB/T 1549 "Methods of Chemical Analysis for Fiber Glass"[J];Fiber Glass;2009-02
3 LI BingNational Research Center of Geological Analysis, Beijing, 100037;Application of Inductively Coupled Plasma Mass Spectrometry in Geological Survey[J];Geological Review;2006-06
4 WANG Yimin CHEN Youping National Research Center for Geoanalysis,Beijing,100037;Review on Important Achievements of Geoanalysis in Last 30 Years of China[J];Geological Review;2008-05
5 RAO ZhuNational Research Center for Geoanalysis,Beijing,100037,China;Application Research of Environmental Organic Pollutants Test Techniques[J];Acta Geologica Sinica;2011-11
6 WANG Jian-bo,HUANG Xing-hua,WANG Yu-gong,Yuan Xiu-ru (Lanzhou Testing and Quality Supervision Center for Geological and Mineral Products,Ministry of Land and Resources,Lanzhou 730050,China);Rapid Determination of Copper,Lead,Cadmium,Cobalt and Nickel in Tartary Buckwheat Tea by Inductively Coupled Plasma-Mass Spectrometry[J];Analysis and Testing Technology and Instruments;2010-02
7 ZHOU Li-ping and LI Zhong-xi(Northwest Geological Research Institute, Xi′an 710054);Determination of silver, cadmium and bismuth in geological samples by inductively coupled plasma mass spectrometry with aqua regia treatment[J];Analytical Laboratory;2005-09
8 YANG Hong-xia, Li Bing and Ma Xin-rong(National Research Center of Geoanalysis, Beijing 100037);Determination of boron in blood and sperm by inductively coupled plasma mass spectrometry (ICP-MS)[J];Analytical Laboratory;2005-10
9 TANG Zhi-yong~*,QIU Hai-ou and ZHENG Hong-tao(Faculty of Materia Science and Chemical engineering,China University of Geosciences,Wuhan 430074);Analysis of rocks and minerals[J];Chinese Journal of Analysis Laboratory;2006-09
10 TANG Zhi-yong,QIU Hai-ou and ZHENG Hong-tao(Faculty of Materia Science and Chemical engineering,Chin University of Geosciences,Wuhan 430074);Analysis of rocks and minerals[J];Chinese Journal of Analysis Laboratory;2008-10
China Proceedings of conference Full-text Database 3 Hits
1 Yin Ming;Progress and Prospect on Geoanalytical Techniques[A];[C];2008
2 YANG Hong-xia, LI Bing~* (National Research Center of Geoanalysis, Beijing 100037, China);Determination of Boron and other Elements in Water and Urine by Inductively Coupled Plasma Mass Spectrometry[A];[C];2005
3 HE Xiao-jiao,LIU Chun-guang(Key Laboratory of Pollution Processes and Environmental Criteria,Ministry of Education,Nankai University,Tianjin 300071,China);Investigation of Boron in Soils of a Typical Sewage Irrigation Area,Tianjin,China[A];[C];2011
【Secondary Citations】
Chinese Journal Full-text Database 1 Hits
1 左天明;Advances in Metallurgical Optical Emission Spectroscopy[J];METALLURGICAL ANALYSIS;1994-02
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved