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《ROCK AND MINERAL ANALYSIS》 1995-03
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Chromogenic Reaction of Nickel with o-Carboxybenzenediazoaminoazobenzene and Its Application

Guo Zhongxian;Tao Yuguo;Zhang Shuyun(Department of Chemical Engineering,Sichuan Institute of Light Industry and Chemical Technology,Zigong,643033)  
ickel forms a red 1 :2 complex with o-carboxybenzenediazoaminoazobenzene in the presence of p-octylpolyethyleneglycol phenylether(OP)in a borax buffer(pH 9.7~10.0).The complex developed has a maximum absorption at 540 nm, with contrast △λ=126 nm,and its apparent molar absorptivity is 1.99 × 10 ̄5 L· mol ̄(-1)·cm ̄(-1),and Sandell sensitivity is 2. 95 × 10 ̄(-4) μg/cm ̄2.The development is complete in 20 min and the color is stable for at least 12 h.Most metal ions do not interfere. Beer’s law is obeyed up to 0. 20μg/ml nickel,the detection limit being 0.0004 μg/ml.The method has been applied to the determination of nickel in ore and alloy steel samples in the presence of masking agents,and the results obtained agreed with the certified values,theRSDs(n=6)were 1.8% and 3.1% respectively,there coveries were 95.0%~101.2 %.
【Fund】: 四川省教委科研基金
【CateGory Index】: O614.813.0
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