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《Journal of Yili Normal University(Natural Science Edition)》 2018-04
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Rapid Separation and Purification of Hydrolysates from Prunus Cerasifera Ldb Leaves

AN Xue-rui;LIU Xiao;GE Yu-wei;LIU Tian-qi;Alimila;LIU Wei;College of Chemistry and Environmental Science, Yili Normal University;  
The chemical constituents of hydrolysates from Prunus cerasifera Ldb leaves were analyzed and sepa-rated by UPLC-UV-QDA and different column chromatography. The results showed that the hydrolysates mainlycontain phenylpropanoids and flavone aglycones, such as caffeoylquinic acid methyl ester, ferulic acid, quercetinand kaempferol. The silica gel column was better than macroporous adsorption resin, ferulic acid(6.3 mg) was isolat-ed by column chromatography of sephadex LH-20, kaempferol(27.1 mg) was easily isolated by recrystallizationwith high yield. However, caffeoylquinic acid methyl ester and quercetin were not isolated by using column chroma-tography.
【Fund】: 伊犁师范学院应用化学自治区重点专业大学生创新项目(SIE-2017YH005)
【CateGory Index】: O658.1;O629
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