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《Textile Auxiliaries》 2007-05
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Influence of the solvents on the synthesis of glycidyltriethylammonium chloride

ZHOU Jia-da,FANG Kuan-jun,ZHANG Xia(Key Lab Sci.Technol.Eco-Text.,Ministry Educ.,Jiangnan Univ.,Wuxi 214122,China)  
The reaction of epichlorohydrin with triethylamine in non-polar and polar solvents(including protonic and non-protonic solvents) was researched.The influence of solvent type and polarity on the reaction rate and epoxy value was analyzed,and the solvent behavior under different reaction temp.and time conditions were also investigated.The results demonstrated that the non-protonic polar solvents gave the best effect,the protonic polar ones brought the largest destruction of the epoxy groups,the reaction was slowed in non-polar solvents,and the increased temp.lowered the influence of the solvents.
【Fund】: 国家自然科学基金资助项目(2047025)
【CateGory Index】: O621.3
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