Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Textile Auxiliaries》 2010-04
Add to Favorite Get Latest Update

Preparation of nano-TiO2 using metatitanic acid as raw materials

GUO Qiong,XIAO Gao,SHI YI-dong,CHEN Yan-xia,JIN Sheng-ji,LI Ting(College of Light Industry,Textile and Food Engineering,Sichuan University,Chengdu 610065,China)  
The preparation method of nano titania using metatitanic acid as raw material was introduced.The factors of producing nano titania using homogeneous precipitation method,such as the ratio of acid and Ti,concentration of H2SO4 and TiOSO4,dosage of urea,forging temperature,were discussed.The results showed that the decomposition condition of metatitanic acid was: the ratio of acid and Ti was 3,8.2 mol/L of H2SO4,the reaction temperature was 100 ℃,and the dissolution time was 1 h.The nano TiO2 with smallest particle size could be obtained when the dosage of urea was three times of theoretical dosage under 90 ℃,other conditions were equal.The obtained sample was anatase nano-titania,and rutile type occurred at 850 ℃ of calcination temperature.Huge amount of rutile nano-titania occurred when the temperature reached 900 ℃,that is,the initial temperature that anatase type converted to rutile type was 850 ℃.
【CateGory Index】: O614.411
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
Chinese Journal Full-text Database 2 Hits
1 Zhang Xiyun Zhong Zhaoping Yao Jie(Key Laboratory of Energy Thermal Conversion and Control of Ministry of Education,Southeast University,Nanjing 210096,China);Preparation of nano-TiO_2 by homogeneous precipitation intensified with ultrasound[J];Journal of Southeast University(Natural Science Edition);2012-04
2 MOU Jun-li,LI Zheng-ran,CHEN Yan-xia,SHI Yi-dong, XIAO Hong-yan,WANG Hai-ying(College of Textile and Food Engineering,Sichuan University,Chengdu 610065,China);Preparation and structure properties of TiO_2/MMT composite photocatalysis material[J];Textile Auxiliaries;2012-03
China Proceedings of conference Full-text Database 1 Hits
1 Xiao Hong-yan,Mou Jun-li,Chen Yan-xia,Shi Yi-dong College of Textile and Food Engineering,Sichuan University,Chengdu 610065,China;Preparation and Structure Properties of TiO_2/MMT Composite Photocatalysis Material[A];[C];2012
Chinese Journal Full-text Database 6 Hits
1 WANG Xiaohui;WANG Zichen;LI Xi;ZHANG Lihua;XIAO liangzhi(Jiin University);THE PREPARATION OF TiO_2 UFP BY USING COLLID CHEMICAL METHOD[J];;1992-06
2 LUO Ju DING Xingzhao CHENG Lifang MA Xueming DONG Yuanda (Institute of Solid State Physics,Academia Sinica);STUDY ON THE STRUCTURE OF NANOMETER-SIZED TITANIA POWDERS PREPARED BY A SOL-GEL METHOD[J];;1993-01
3 Shi Liyi Hua Bin Zhang Jianping(School of Chemistry, and Chemical Engineering, Shanghai University,Shanghai, 200072,China);Structure of Microemulsion and Application of W/O Microemulsion in the Preparation of Ultrafine Particles[J];JOURNAL OF FUNCTIONAL MATERIALS;1998-02
4 WEI Shao-dong,WANG Xing (East China Engineering Science & Technology Co., Ltd., Hefei 230024,China);Effects of heat treatment on TiO_2 crystal type and particle size[J];Drying Technology & Equipment;2005-01
5 LIU Zhao-hui 1 , YANG Huai-xia 2 , SHEN Xin-yuan 3 , DONG Hui-cao 1 , WEN Li 1 (1.Department of Chemical Engineering , Zhengzhou Inst. of Light Ind. , Zhengzhou 450002 , China ; 2.Department of Traditional Medicine , Henan Coll;Research Progress on Preparation of Nanometer TiO_2[J];Henan Chemical Industry;2002-08
6 Chen Zao-ming Zheng Dian-mo (College Of Environmental and Chemical Engineering,Nanchang University,Nanchang,China,330029);The Preparation Methods for Nanosized Titania[J];Jiangxi Chemical Industry;2003-01
Chinese Journal Full-text Database 10 Hits
1 Li Da cheng,Zhou Da li,Liu Heng,Zhang Ping,Chen Chao zhen,Quan Xue jun (Institute of UFP Materials,Sichuan University,Chengdu,Sichuan 610051,China);Brief Introduction on High Performace and High Function of Titanium Dioxide(PartⅠ)[J];Sichuan Nonferrous Metals;2001-03
2 Li Dacheng Zhou Dali Liu Heng Zhang Ping Zhang Yun (Institute of UFP Materials,Sichuan University (west) Chengdu 610065) Gong Jiazhu (Sichuan Lomon Titanium Industry Go,Ltd Mianzhu City 618200);Preparation of Nanometer TiO_2[J];Sichuan Nonferrous Metals;2003-02
3 ZHANG Li 1,2, CHU Dao-bao 1 (1. College of Chemistry and Materials Science ,Anhui Normal University, Wuhu 241000,China; 2. Suzhou Teachers' College, Suzhou 234000, China);THE INFLUENCE OF ACIDITY ON THE PREPARING OF TiO_2 NANOPARTICLES FROM H_2 TiO_3 WITH HYDROTHERMAL METHOD[J];Journal of Anhui Normal University(Natural Science);2002-01
4 JIANG Yanlan, ZHANG Jinchun, WANG Jie, ZHANG Yong (Naval Aeronautic Engineering Academy,Yantai 264001,China);Properties and applications of nano-materials -metals and their alloy[J];Ordnance Material Science and Engineering;2001-06
5 ZHANG Mei 1,YANG Xu-jie 2,LU Lu-de 2,WANG Xin 2 (1.Beijing Institute of Special Engineering Machinery, Beijing 100076,China;2.School of Chemical Engineering, Nanjing University of Science and Technology, Nanjing 210094,China);Nanmeter TiO_2 powder prepared by stearic acid gel method[J];Ordnance Material Science and Engineering;2002-01
6 LIN Yu-long, WEI Yu, JIA Zhen-bin (College of Chemistry, Hebei Normal University, Shijiazhuang 050016, China);Synthesis of nanoscaled titania powders by liquid phase methods[J];Micronanoelectronic Technology;2003-03
7 GUO Xing-long 1 ,YU Xian-jin 2 ,XUE Cheng-shan 1 ,DONG Zhi-hua 1 ,GAO Hai-yong 1(1.Institute of Semiconductors,Shandong Normal University,Jinan250014,China;2.College of Chemical Engineering,Shandong University of Technology,Zibo255012,China);Making rutile by using magnetron sputtering[J];Micronanoelectronic Technology;2003-12
8 RUAN Ji-feng LI Chun-xi WANG Zi-hao(College of Chemical Engineering, Beijing University of Chemical Technology, Beijing 100029, China);Preparation and photocatalytic performance of ultrafine titanium dioxide powder[J];Journal of Beijing University of Chemical Technology;2002-03
9 SHEN ShuLing1 WU Wei2 GUO Kai1 CHEN JianFeng1,2 (1.Research Center of the Ministry of Education for High Gravity Engineering and Technology;2.Key Laboratory for Nanomaterials,Ministry of Education,Beijing University of Chemical Technology,Beijing 100029,China);Preparation of ultrafine silica with different morphologies using reverse microemulsions[J];Journal of Beijing University of Chemical Technology(Natural Science Edition);2007-05
10 TAN Huai-qin, QUAN Xue-jun, ZHAO Qing-hua, SANG Xue-mei(School of Bioengineering, Chongqing Institute of Technology, Chongqing 400050,China);Research Progress on Titanium Dioxide Photocatalytic Technology[J];Journal of Chongqing Institute of Technology;2005-03
China Proceedings of conference Full-text Database 3 Hits
1 Liu Yajin, Liang Xiaoping , Jiang Qiang, Li Wandeng (Tianjin Municipal Key Lab of Fiber Modification and Functional Fiber, Tianjin Polytechnic University, Tianjin 300160, China);Preparation and Evaluation of Nanoscale ZnO Anti-UV Agents[A];[C];2005
2 LEI Ting;LOU Feng-lan;TANG Guang-ming;BO Xin-wei Chongqing Instrument Materials Research Institute, Chongqing, 400700, China;Synthesis of the Nickel Ferrite Nano Powder by Hydrothermally Method[A];[C];2001
3 Feng Kong~* Jingbo Lv;Preparation of Silver Halide Nanoparticles by w/o Microemulsion Method[A];[C];2007
Chinese Journal Full-text Database 10 Hits
1 Li Dacheng,Zhou Dali,Liu Heng,Zhang Ping,Zhang Yun (Institute of UFP Materials,Sichuan University(west),Chengdu 610065,China)Gong Jiazhu (Sichuan Longmong Titanium Industry Co.,Ltd,Mianzhu City 618200,China);Application of Nanometer TiO_2[J];Sichuan Nonferrous Metals;2002-04
2 GU Donglin,WANG Xu,YU Lei,CHEN Jiaxing (College of Materials Engineering,Yancheng Institute of Technology,Yancheng 224003,China);Study on TiO_2 powder prepared by sol-gel method[J];Ordnance Material Science and Engineering;2010-01
3 XU Zhi-bing~1,WEI Xian-wen~2(1 Department of Chemistry,Anqing Normal College,Anhui Anqing 246003;(2 School of Chemistry and Material College,Anhui Normal University,Anhui Wuhu 241000,China);Preparation and characterization of TiO_2 hollow microspheres[J];Journal of Chinese Electron Microscopy Society;2006-03
4 LI Xiang-qi, TANG De-ping, WENG Guo-jian, HUANG Shi-chu (College of Materials Science and Engineering, Fuzhou University, Fuzhou, Fujian 350002, China);The structure and characterization of calcined titaniam-pillared clays[J];Journal of Fuzhou University(Natural Sciences Edtion);2002-06
5 Liu Xiaoxia1,Qu Rui2(1.Center of Information,The Northwest Research Institute of Chemical Industry,Xi’an 710600;2.The First Design Department of General Technique,BeiJing CCI Architecture Design LTD.Northwest Branch,Xi’an 710075,China);Advances in the SCR Catalysts Abroad[J];Guangdong Chemical Industry;2008-11
6 GAO Wei 1, WU Feng Qing 1* , LUO Zhen 1, FU Ju Xia 1, WANG De Jun 1, XU Bao Kun 2 (1. Department of Chemistry, Jilin University; 2. Department of Electronic Egineering, Jilin University, Changchun 130023, China);Studies on the Relationship Between the Crystal Form of TiO_2 and Its Photocatalyzing Degradation Efficiency[J];Chemical Research In Chinese Universities;2001-04
7 ZHANG Jianfeng; ZHENG Qiang;GAO Changyou; YI Xiaosu ( Department of Polymer Science and Engineering, Zhejiang University, Hangzhou, 310027, China; National Key Laboratory of Advanced Composites, Beijing, P. O. Box 81 - 3, 100095, China);The Polymer /Inorganic Composites Prepared through Sol-Gel Process[J];JOURNAL OF FUNCTIONAL MATERIALS;2000-04
8 LI Xiaoping1,XU Baokun1,LIU Guofan1,WU Fengqing2 1 Department of Electronic Engineering,2 Department of Chemistry,Jilin University,Changchun,130023,China;The Research and Development of Photocatalytic Degradation of Organic Contaminant Over Nanosized TiO2 in Water[J];JOURNAL OF FUNCTIONAL MATERIALS;1999-03
9 Huang Hui Luo Hongjie Yang Ming (Department of Materials Science and Engineering,Northwest Institute of Light Industry,Xianyang 712081) Liu Jiang (Xianyang Research and Design Institute of Ceramics,Xianyang 712081);Preparation of Nanocrystalline Titania Powders by Hydrothermal Precipitation[J];BULLETIN OF THECHINESE CERAMIC SOCIETY;2000-04
10 Yu Haihu Wu Hongbiao Wu Yiwen Li Xiaofu ('Fiber Optic Sensing Technology Research Center, Wuhan University of Technology, Wuhan 430070; 2Dept. of Materials Science and Engineering, Wuhan University of Technology, Wuhan 430070);Study on TiO_2 -Based Thin Films by Electrostatic Self - Assembled on Glass Substrates[J];Bulletin of the Chinese Ceramic Society;2004-03
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 Huang Jianyan (Applied Chemistry Institute of Anhui University Hefei 230039);The Effect of Phase Transition on the Growth Ofultrafine TiO 2 Particles[J];JOURNAL OF ANHUI UNIVERSITY(NATURAL SCIENCES);1998-03
2 WANG Xiaohui;WANG Zichen;LI Xi;ZHANG Lihua;XIAO liangzhi(Jiin University);THE PREPARATION OF TiO_2 UFP BY USING COLLID CHEMICAL METHOD[J];;1992-06
3 LUO Ju DING Xingzhao CHENG Lifang MA Xueming DONG Yuanda (Institute of Solid State Physics,Academia Sinica);STUDY ON THE STRUCTURE OF NANOMETER-SIZED TITANIA POWDERS PREPARED BY A SOL-GEL METHOD[J];;1993-01
4 Yang Jun 1, Xu Dingkan 2,Zhang Qichao 2(1 Wuhan Institute of Chemical Technology,Hubei Wuhan 430073; 2 Chongqing University,Chongqing 400044 China);Preparation of Fine Powder Titanium Oxide with Sol gel Method[J];CHINA POWDER SCIENCE AND TECHNOLOGY;1999-05
5 GUO Wei Lin 1,2 , WANG Xi Kui 2* , LIN Zhi Ming 1, SONG Guang Zhi 1 (1. Engineering Research Center of Microsphere Materials, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100101, Chian; 2. School;Sonochemical Synthesis of Nanocrystalline TiO_2 by Hydrolysis of Titanium Alkoxides[J];Chemical Research In Chinese Universities;2002-08
6 GUAN Zi-Sheng, YAO Jian-Nian, MA Ying, SONG Yan-Lin, JIANG Lei * (Center for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, China);A Study of Influence on TiO_2 Sol with UV Irradiation[J];Chemical Research In Chinese Universities;2002-10
7 YU Wang-Lh;YANG Phg;XU Qiu-Yun; ZHU Ying;XI Zheng-Kai(Department of Applied Chemistry,Shandong Institute of Building Materials,Jinan,250022)CHEN Zong-Qi(Department of Applied Chemistry,Qingdao Chemical Industry Institute,Qingdao);A Study of the Preparation of Monodispersed TiO_2 Particles[J];CHEMICAL RESEARCH IN CHINESE UNIVERSITIES;1994-11
8 CHEN Long-Wu; GAN Li-Hua; YUE Tian-Yi(Department of Chemistry,Tongji University,Shanghai,200092)ZHOU En-Xuan(The Ninth Department,Beijing University of Aeronauties,Beijing);Studies on the Preparation of Aluminium Oxide (Hydrous)Ultrafine Particles by the Method of Microemulsion Reaction[J];CHEMICAL RESEARCH IN CHINESE UNIVERSITIES;1995-01
9 ZHAO Jing\|Zhe, WANG Zi\|Chen\+*, LIU Yan\|Hua, WANG Li\|Wei, \= SONG Qing, YANG Hua, ZHAO Mu\|Yu (Department of Chemistry, Jilin University, Changchun, 130023) FENG Shou\|Hua, XU Ru\|Ren (Key Laboratory of Inorganic Hydrothermal Synthesis, J;Preparation of Ultrafine Rutile Titania Crystals by Liquid Method[J];CHEMICAL RESEARCH IN CHINESE UNIVERSITIES;1999-03
10 Ha Runhua;Hou Sijian;Li Fuping;Wang Desong(Department of Applied Chemistry,Tianjin University,Tianjin 300072);Structure of Microemulsion and the Inverse Microemulsion Polymerization of Acrylamide[J];;1995-01
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved