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《Textile Auxiliaries》 2010-04
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Preparation of nano-TiO2 using metatitanic acid as raw materials

GUO Qiong,XIAO Gao,SHI YI-dong,CHEN Yan-xia,JIN Sheng-ji,LI Ting(College of Light Industry,Textile and Food Engineering,Sichuan University,Chengdu 610065,China)  
The preparation method of nano titania using metatitanic acid as raw material was introduced.The factors of producing nano titania using homogeneous precipitation method,such as the ratio of acid and Ti,concentration of H2SO4 and TiOSO4,dosage of urea,forging temperature,were discussed.The results showed that the decomposition condition of metatitanic acid was: the ratio of acid and Ti was 3,8.2 mol/L of H2SO4,the reaction temperature was 100 ℃,and the dissolution time was 1 h.The nano TiO2 with smallest particle size could be obtained when the dosage of urea was three times of theoretical dosage under 90 ℃,other conditions were equal.The obtained sample was anatase nano-titania,and rutile type occurred at 850 ℃ of calcination temperature.Huge amount of rutile nano-titania occurred when the temperature reached 900 ℃,that is,the initial temperature that anatase type converted to rutile type was 850 ℃.
【CateGory Index】: O614.411
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