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《Chinese Journal of Pharmaceutical Analysis》 2008-03
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HPLC determination of berberine and quercetin in Migan granules

XU Guo-fang~1 GUO Na~1 LI Jun-ming~1 XIE Ai-fang~2 GUO Xing-jie~(1*) (1.Shenyang Pharmaceutical University,Shenyang 110016,China;2.Disha Pharmaceutical Group Co.,Ltd.,Weihai 264205,China)  
Objective:To develop an HPLC method for determination of berberine and quereetin in Migan granules. Methods:A Diamonsil C_(18)(250 mm×4.6 mm,5μm)column was used with a mobile phase of aeetonitrile-0.05 mol·L~(-1)potassium dihydrogen phosphate(27:73),and flow rate of 1.0 mL·min~(-1);The detection wavelength was set at 360 nm and the column temperature was room temperature.Results:The calibration curves were linear in the range of 8.33-41.6μg·mL~(-1)for berberine(r=0.9997) and 4.08-20.4μg·mL~(-1)for quercetin(r=0.9998). The average recovery(n=6)of berberine was 98.6% and that of quercetin was 97.8%.Conclusion:The method is convenient,selective and reproducible for determination of berberine and quercetin in Migan granules.
【CateGory Index】: R286.0
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