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《Chinese Journal of Pharmaceutical Analysis》 2010-11
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Electrochemical behavior and determination of chrysophanol on a glassy carbon electrode

LIU Ai-lin1,JIANG Wei-wei2,CHEN Wei1,XU Nan1,LIN Xin-hua1(1.Department of Pharmaceutical Analysis of the Fujian Meidical University,Fuzhou 350004,China;2.Affiliated Hospital of Jining Medical College,Jining 272129,China)  
Objective:To study the voltammetric behavior and establish a novel method for the determination of the concentration of chrysophanol.Methods:The electrochemical behavior of chrysophanol was studied by voltammetry on a glassy carbon electrode.The results shows that a pair of well-defined redox peak of chrysophanol was observed and the electrode process is adsorption-controlled.Results:The relationship between oxidation peak current and the concentration of chrysophanol is linear in the range of 1.0 ×10-7 -9.0×10-6 mol·L-1 by differential pulse voltammetric method.The detection limit had been estimated as 5.0×10-8 mol·L-1.Conclusion:The method has been successfully used to detect chrysophanol in Rhubarb.
【Fund】: 国家“863”计划资助项目(No.2008AA02Z433);; 国家自然科学基金资助项目(No.20805006);; 福建省科技厅重点基金资助项目(No.2008Y0045);; 福建省自然科学基金资助项目(No.C0710024);; 福建医科大学引进人才启动基金(No.bs06002);; 苗圃科研基金(No.2010MP043)资助项目
【CateGory Index】: R284
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