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《Pharmaceutical Care and Research》 2005-04
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Study of the chemical constituents of Hypericum sampsonii

GUO Cheng~(1),ZHENG Qing-Ming~(1,2),ZHENG Han-Chen~(2)(1.Departmemt of Pharmacy,Sixth People's Hospital,Shanghai Jiaotong University,Shanghai 200233,China;2.Department of Pharmacognosy,School of Pharmacy,Second Military Medical University,Shanghai 200433,China)  
Objective: To study the chemical constituents of Hypericum sampsonii Hance.Methods: The compounds were isolated by column chromatography using silica gel,polyamide,Sephadex LH-20 and macroreticular resin,and the structures were elucidated by UV,IR,MS,~(1)H-NMR,()~(13)C-NMR spectral analysis and their physicochemical properties.Results: From the CH_(2)Cl_(2) fraction of the EtOH extract of crude drug,5 compounds were isolated and identified as octacosanol(compound 1),triacontanoic acid(compound 2),stigmasterol(compound 3),benzoic acid(compound 4) and 1-hydroxy-7-methoxy-xanthone(compound 5);and from EtOAc fraction of the EtOH extract 3 compounds were isolated and identified as 3,4,5-trihydroxy-benzoic acid(compound 6),quercetin(compound 7) and 1,3,6,7-tetrahydroxy-xanthone(compound 8). Conclusion::All these compounds are obtained from H.sampsonii for the first time except compound 7.
【CateGory Index】: R284
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