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《China Pharmaceuticals》 2014-08
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Content Determination of Astraloside in Naoluotong Capsules by HPLC-ELSD

Yue Li;Huaibei Municipal Institute for Food and Drug Control;  
Objective To determine the content of astraloside in Naoluotong Capsules by HPLC-evaporative light scattering detector(ELSD).Methods The Hypersil ODS2column(150 mm × 4.6 mm,5 μm) was adopted,the mobile phase was acetonitrile-water(30 ∶ 70),the flow rate was 1.0 mL / min,the drift tube temperature was 105 ℃.The column temperature was 25 ℃.Results The linear range of astraloside was 0.066 7-0.466 8 mg /mL(r = 0.999 9),the average recovery rate was 100.70%(n = 9),RSD = 1.28%.Concluslon This method is simple to operate,accurate,stable,and highly sensitive,and can be used as the the quality control method of this preparation.
【CateGory Index】: R286.0
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