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《Chinese Journal of Applied Chemistry》 2004-05
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Synthesis of a Cationic Gemini Surfactant with Amide Group

DUAN Ming, HU Xing-Qi~*, ZUO Xiao-Ling, CHEN Yuan-Dong (Department of Chemical Engineering,Southwest Petroleum Institute,Chengdu 610500)  
A novel Gemini surfactant bis[N,N′-(dodecanoylamino)ethyl]triethylenediamine bromide( BDEDE) was synthesized from ethyl bromide and bis(2-dodecanoylaminoethyl) ethylene diamine(BDEE), the latter was prepared from lauric acid and N,N′-bis(2-aminoethyl) ethylenediamine. The structure of the Gemini surfactant was characterized by elemental analysis, IR, ~1H NMR and ~13C NMR. Its critical micelle concentration( 0.105 mmol/L) and γ_cmc(31.0 mN/m) were determined. The cmc value of Gemini surfactant decreased by appoximately two orders of magnitude than cmc of dodecyltrimethylammonium bromide.
【Fund】: 油气藏地质及开发工程国家重点实验室开放基金 (PLN0 12 0 );; 四川省重点学科建设基金资助项目
【CateGory Index】: TQ423
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