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《Chinese Traditional Patent Medicine》 2002-05
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Determination of rhien, emodin, and chrysophanol in Huangdanyinchen Granules by HPLC

HUA Xiao dong, WANG Zhi hua, WANG Ju mei, XIE Qin (Shanghai University of Traditional Chinese Medicine, Shanghai 200032, China)  
Objective:To develop a method to determine the contents of emodin, rhien and chrysophanol in Huangdanyinchen Granules. Methods: HPLC was used to determine the contents of emodin, rhien and chrysophanol in Huangdanyinchen Granules. The separation was performed on YWG ODS column with methol perchloric acid (1%) (8∶2) as a mobile phase and the wavelength of UV detector was 280nm.Results: The separating degree and the linearity of this method was well with the average recovery of rhien: 97.43%, RSD= 1.90%; Emodin:98.45%,RSD=1.62%;Chrysophanol: 98.87%, RSD=1.50%, respectively.Conclusions:The method is simple and rapid and gives satisfactory results. It can be suitable for quality controll of Huangdanyinchen Granules.
【CateGory Index】: R286
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【References】
Chinese Journal Full-text Database 7 Hits
1 CAO Wei-guo~(1,2),LIU Zhi-qin~1,SHAO Yun~1,TAO Yan-duo~(1*) (1 The Northwest Institute of Plateau Biology,Chinese Academic of Sciences,Xining 810000,China;2 Graduate School of Chinese Academy of Sciences,Beijing 100039,China);Determination of four anthraquinone derivatives in trueborn Rheum tanguticum of Qinghai Province[J];Acta Botanica Boreali-occidentalia Sinica;2004-11
2 CHAI Yi-feng, WU Yu-tian and LI Xiang(Department of Pharmaceutical Analysis, College of Pharmacy, Second Military Medical University, Guohe Road 325, Shanghai 200433), Fenxi Shiyanshi,2004,23(6):71~92;Pharmaceutical Analysis I[J];Analytical Laboratory;2004-06
3 ZHOU Jian-bo~1,2,JIANG Fu-quan~1,2,WEN Huai-xiu~1,2, SHAO Yun~1,SHI Zhi-xian~1 and TAO Yan-duo~*1(1.Northwest Institute of Plateau Biology,Chinese Academy of Sciences,Xining 810008;2.Graduate School of Chinese Academy of Sciences,Beijing 100049);Study on HPLC fingerprint of alcohol extracts from Rheum tanguticum[J];Chinese Journal of Analysis Laboratory;2006-11
4 Cao Jinhong1,Pan Weiqiao2,Lin Li2 1.Huzhou No.3 People’s Hospital,Zhejiang Province(313000);2.Institute for Drug Control;Determination of Emodin and Chrysophanol in Rhubarb Sodium Bicarbonate Table by HPLC[J];Journal of Zhejiang University of Traditional Chinese Medicine;2010-03
5 ;Determination of Emodin and Chrysophanol in Compound Huang Zha Capsule by HPLC[J];China Foreign Medical Treatment;2009-22
6 XU Xiongliang, ZHANG Zhirong, HUANG Yuan(West China School of Pharmacy, Sichuan University, Chengdu 610041, China);Analysis of Rhubarb for Injection by High Performance Liquid Chromatography[J];Chinese Journal of Chromatography;2003-06
7 CHEN Jing-ran1,XIE Fei2,YIN Xiao-fei1,LIU Jin-hua1,WANG Ai-ping1(1.Department of Pharmacy,the 251st Hospital of the PLA,Zhangjiakou 075000,China;2.Department of Pharmacy,the Fourth Hospital of Zhangjiakou City of Hebei Province,075000,China);Content Determination of Emodin and Chrysophanol in Niuhuang Jiedu Dropping Pill by HPLC[J];Herald of Medicine;2011-04
【Citations】
Chinese Journal Full-text Database 2 Hits
1 LI Shu ying 1, GUO Zeng jun 2, WANG Li 3 (1.Shanxi Xinghua Institute of Materia Medical, Xi'an 710075, China; 2.Pharmacy College, Xi'an Jiaotong University, Xi'an 710061, China; 3.First Clinical Medical College, Xi'an Jiaotong University, Xi'an 71;Determination of Emodin, Chrysophanol and Baicalin in Three Yellows Tablets by HPLC[J];Chinese Traditional Patent Medicine;2001-06
2 YAO Zhong qing (Institute of TCM, Nanjing Hospital of TCM, Nanjing Jiangsu 210001, China);Determination of emodin, chrysophanol, and physcion in HUANGLIAN SHANGQING PILL * by HPLC[J];Chinese Traditional and Herbal Drugs;2001-08
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 JIN Yu (Shanghai Haihong Group Chaohu C-dragon Pharmaceutical CO.,Ltd,Chaohu 238000);Determination of baicalin in sanhuang tablet by improved HPLC[J];Anhui Medical and Pharmaceutical Journal;2008-06
2 WANG Jie,ZHANG Yi-ming,LI Jin-ran,LI Xia,CHEN An-jia(Shanxi Medical University College of Pharmacy,Taiyuan Shanxi 030001,China);Determination and Relative Analysis of Emodin and Chrysophanol in Sanhuang Tablets[J];Journal of Hebei Polytechnic University(Natural Science Edition);2009-02
3 Sui Yanjun Harbin third Chinese Pharmaceutical Factory,Harbin Heilongjiang(150078);Using HPLC in assaying the content of Emodin and Chrysophanicacid in Fracture & Contusion capsule[J];Heilongjiang Medical Journal;2004-03
4 LI Wu-ying1, MENG Xiang-tao2, GUO Xin-she3 (1. Editorial Dept. of Henan University , Henan Kaifeng 475001, China; 2. Art and Design of School, Henan Province, 457000, China; 3.Pharmaceutical College of Henan University, Henan Kaifeng 475001, China );Study for the quality standard of RU AN membrane[J];;2005-02
5 ZHU Hong,YI Guo-fu ( Guangdong University of Techology,Guangzhou 510635,Guangdong,China);Determination of the Contents of Aloeemodin Rhein and Emodin in Tang Qing Capsule by HPLC[J];Liaoning Journal of Traditional Chinese Medicine;2009-12
6 ZENG Rong-xiang1a,LI Hong-liang1b,SUN Dong-liang2(1a.Department of Pharmacy;1b.Department of Haematology,Foshan Hospital of Traditional Chinese Medicine,Foshan 528000,China;2.Department of Pharmacy,Jiangxi Province Hospital of TraditionalChinese Medicine,Nanchang 330006,China);Determination of Emodin and Chrysophanol in ShenShuaiXieZhuo Granules by HPLC[J];Practical Clinical Medicine;2009-11
7 WANG Jie,ZHANG Qiang,ZHANG Yi-ming,LI Jin-ran,LI Xia,CHEN An-jia(Pharmay College,Shanxi Medical University,Taiyuan 030001,Shanxi,China);Ultrasonic Extraction-HPLC Determination of Emodin and Chrysophanol in Sanhuang Tablets[J];Journal of Liaoning University of Traditional Chinese Medicine;2010-11
8 XU Xiongliang, ZHANG Zhirong, HUANG Yuan(West China School of Pharmacy, Sichuan University, Chengdu 610041, China);Analysis of Rhubarb for Injection by High Performance Liquid Chromatography[J];Chinese Journal of Chromatography;2003-06
9 LI Lei, YUAN Bo, LI Fa-mei (School of Pharmacy, Shenyang Pharmaceutical University, Shenyang 110016, China);Determination of the contents of rhein and physcione in the Injectio Folii Isatidis Composita by HPLC[J];Journal of Shenyang Pharmaceutical University;2004-01
10 MA Wen1,LI Dan2(1.College of Chemistry and Chemical Engineering,Xinyang Normal University,Xinyang 464000,China;2.Xinyang Branch Corporation of Henan Lingrui Pharmaceutial Co.Ltd.,Xinyang 464000,China);The extraction of ursolic acid from Xia-Sang-Ju and its reliability[J];Journal of Xinyang Teachers College(Natural Science Edition);2003-03
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 LIU Xin~1, HU Fang-di~1, FENG Shi-lan~1, ZHAO Jian-xiong~1, LI Ying-dong~2, XU Jing-wen~1, SONG Ping-shun~3(1. Lanzhou Medical College, Lanzhou 730000, China; 2. Lanzhou Traditional Chinese Medical college, Lanzhou 730000, China; 3. Gansu Prorincial Institute for Drug Control, Lanzhou 730000, China);Study of Chromatography Fingerprint(CFP) of Dahuang[J];Analysis and Testing Technology and Instruments;2004-03
2 Qin Chuanguang, Huang Kaixun, Xu Huibi  (Pharmaceutical Institute, Huazhong University of Science and Technology, Wuhan 430074);Component Analysis and Molecular Weight Determination of Misgurnus Anguillicaudatus Polysaccharides by Gel Filtration Chromatography[J];Chinese Journal of Analytieal Chemistry;2002-04
3 Ni Kunyi 1 , Yu Qingfeng 1, Yu Jian 1, Zhou Helin 2, Tu Shuzi 1 1(China Pharmaceutical University, Nanjing 210009) 2(Wujin Zhiyao Chang, Changzhou 213172);Studies on the Quality of Benzbromarone and Its Impurities[J];Chinese Journal of Analytieal Chemistry;2002-05
4 Chen Benmei , Xia Lingwei, Liang Shaoxian, Chen Guohua, Deng Fuliang (Analytical Testing Center, Xiangya Medical School, Central South University, Changsha 410078) Zhang Weiru, Tao Lijian (Xiangya Hospital, Central South University, Changsha 4;Determination of L-Arginine and Methyled Arginie in Urine by High Performance Liquid Chromatography[J];Chinese Journal of Analytieal Chemistry;2002-05
5 Ma Dingyuan, Chen Jun, Li Ping * (Department of Pharmacognosy, China Pharmaceutical University, Nanjing 210038) Hu Zhuoyi (Department of Biochemistry, China Pharmaceutical University, Nanjing 210009);Analysis of Monosacchaaride Compositions in Polysaccharides by Pre-column Derivatization High Performance Liquid Chromatography[J];Chinese Journal of Analytieal Chemistry;2002-06
6 Qi Yunpeng 1, Sun Shengli 1, Wu Yutian *1, Li Tonghua 2, Mi Heming 1, Chai Yifeng 1 1(Department of Pharmaceutical Analysis, School of Pharmacy, Second Military Medical University, Shanghai 200433) 2(Department of Chemistry, TongJi Univ;Application of Heuristic Evolving Latent Projection to the Determination of Loureirin B in Resina Draconis Extracted by Different Methods[J];Chinese Journal of Analytieal Chemistry;2002-07
7 Zeng Zhi 1, Yang Donghui 1, Song Lifei 2, Yang Ting 1, Liu Xiangxiang 2, Yuan Min 1, Zeng Heping 1 1(Department of Chemistry, Analysis and Testing Center, South China Normal University, Guangzhou 510631)= 2(Guangzhou Xiangxue Pharmaceut;The Identification of Isatis Indigotica Fort. by High Performance Liquid Chromatographic Fingerprint[J];Chinese Journal of Analytieal Chemistry;2002-07
8 Yang Liuqing *1 , Wu Xiangyang 2, Chen Jun 3 1(School of Pharmacy,Jiangsu University,Zhenjiang 212001) 2(School of Chemistry and Chemical Engineering,Jiangsu University,Zhenjiang 212013) 3(Department of Pharmaceuticals Enginee;Determination of Ginkgolic Acids in Sarcotesta of Ginkgo Biloba by High Performance Liquid Chromatography[J];Chinese Journal of Analytieal Chemistry;2002-08
9 Hu Xiaoxue, Xin Jiaying , Xu Yi, Cui Junru, Li Shuben, Xia Chungu (State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000);Separation and Characterization of Candida Rugosa Lipase Isoenzymes by High Performance Liquid Chromatograpy[J];Chinese Journal of Analytieal Chemistry;2002-08
10 Liu Daojie *, Wang Xia (Department of Chemistry,Liaocheng Teachers College, Liaocheng 252059) Sun Jiling (Shandong Provincial Institute for Drug Control, Jinan 250012);Simultaneous Determination of Four Components in Commercial Analgesic Tablets by Reversed Phase High Performance Liquid Chromatography-Diode Array Detector[J];Chinese Journal of Analytieal Chemistry;2002-09
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 HU Yan-ping et al(Northwest Institute of Plateau Biology,Chinese Academy of Sciences,Xining,Qinghai 810001);Study on the Chromosome of Rheum tanguticum Maxim. ex Balf. in Guoluo[J];Journal of Anhui Agricultural Sciences;2007-03
2 CHE Guo-dong~(1,2),LI Yu-lin~(1,2),WANG Ling-yun~(1,2),ZHOU Guo-ying~(1,2),SUO You-rui~1,CHEN Gui-chen~(1*)(1 Northwest Plateau Institute of Biology,Chinese Academy of Sciences,Xining 810001,China;2 Graduate University of Chinese Academy of Sciences,Beijing 100039,China);Seasonal Change of Anthroquinone Content in Cultivated Rheum tanguticum[J];Acta Botanica Boreali-Occidentalia Sinica;2006-11
3 ZHOU Jian-bo~1,2,JIANG Fu-quan~1,2,WEN Huai-xiu~1,2, SHAO Yun~1,SHI Zhi-xian~1 and TAO Yan-duo~*1(1.Northwest Institute of Plateau Biology,Chinese Academy of Sciences,Xining 810008;2.Graduate School of Chinese Academy of Sciences,Beijing 100049);Study on HPLC fingerprint of alcohol extracts from Rheum tanguticum[J];Chinese Journal of Analysis Laboratory;2006-11
4 LI Nan1,2,PAN Hong1,DING Shao-dong1,WANG Yun1 and CAO Yuhua1(1.College of Chemical and Material Engineering,Southern Yangtz university,Wuxi 214122;2.College of Life Science and Engineering,Shanxi University of Science and Technology,Xi′an 710021);Application on fingerprint of rhubarb by microemulsion capillary electrokinetic chromatography[J];Chinese Journal of Analysis Laboratory;2008-09
5 MA Miao1,2,LUO Shi-Hong2,LIU Hui-Liang2(1.Key Laboratory of Phytomedicine Resources & Mordenization of TCM,Shihezi 832003,China;2.College of Life Sciences,Shihezi University,Shihezi 832003,China);Temporal variation in content of four anthraquinones in desert ephemeroid plant Eremurus inderiensis[J];Guihaia;2007-03
6 ZHANG Xiu-li,WANG Xin-ying,SHI Lan-xiang(College of Materials Science and Engineering,China Geology University,Beijing 100083,China);Determination of 7-amido acetoxy eicosanoic acid by ultraviolet spectrophotometric method[J];Chemical Engineer;2006-07
7 YANG Jian1,2 XIE Xiao-Long1,2 HU Yan-Ping1,2 WANG Li1 LI Yi1(1.Northwest Plateau Institute of Biology,Chinese Academy of Sciences,Xining 810001)(2.Graduate University of Chinese Academy of Sciences,Beijing 100049);Effects of Extracts from Root of Rheum tanguticum on Seed Germination and Seedling Growth of Triticum aestivum and Elymus nutans[J];Bulletin of Botanical Research;2009-03
8 New Sun,Li Zhihao,Wu Jin,Li Peng(Yunyang Affiliated Dongfeng Hospital,Hubei,Shiyan,442008,China);RP-HPLC determination of drugs in children scattered with the contents of emodin and chrysophanol[J];Guiding Journal of Traditional Chinese Medicine and Pharmacy;2010-10
9 LI Zhi-hao,LI Peng,ZHU Jun(The Dongfeng Hospital Affiliated to Yunyang Medical College,Shiyan 442008,China);Determination of Emodin and Chrysophanol in Muxiang Binglang Wan by HPLC[J];Research and Practice on Chinese Medicines;2011-02
10 LI Jin-ping et al(Department of life science,Qinghal Normal University,Xining China 810008);STATUS OF RHEUM TANGUTICUM MAXIM.EXBALF RESOURCES OF QINGHAI AND COUNTERMEASURES FOR PROTECTION[J];Qinghai Prataculture;2007-02
【Secondary Citations】
Chinese Journal Full-text Database 1 Hits
1 Guo Ping;Li Zhangwan;Jiang Xuehua; Liu Sankang;Guo Qun and Cao Wei(School of Pharmacy,West China University of Medical Sciences,Chengdu,610041);Determination of Baicalin in Scutellaria Baicalensis Georgi and in Chinese Patent Medicine by HPLC[J];CHINESE JOURNAL OF PHARMACEUTICAL ANALYSIS;1995-05
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