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《Chinese Traditional and Herbal Drugs》 2011-10
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Chemical constituents from Angelica sinensis

SONG Qiu-yue,FU Ying-bo,LIU Jiang,ZHENG Dan,HAN Li,HUANG Xue-shi Laboratory of Metabolic Disease Research and Drug Development,China Medical University,Shenyang 110001,China  
Objective To study chemical constituents from EtOAc extract of Angelica sinensis.Methods The compounds were isolated by various chromatographic techniques and the structures were elucidated on the basis of spectral analysis.Results Sixteen compounds were obtained and their structures were identified as senkyunolide G(1),senkyunolide H(2),senkyunolide I(3),senkyunolide J(4),(3Z,3′Z)-6,8′,7,3′-diligustilide(5),3R,8S-falcarindiol(6),11S,16R-dihydroxyoctadeca-9Z,17-dien-12,14-diynoic-1-yl acetate(7),4-(2-hydroxy-1-methoxyethyl) phenol(8),4-(2-hydroxy-1-ethoxyethyl)phenol(9),5-acetoxymethyl-furaldehyde(10),5-hydromethylfuraldehyde(11),brefeldin A(12),vanillin(13),4-methylphenol(14),ferulic acid(15),and ferulaldehyde(16).Conclusion Compounds 8—10 are firstly obtained from the plants of Angelica L.,and compounds 6 and 7 are isolated from A.sinensis for the first time.Furthermore,the assignments of 13C-NMR data of compound 1 are reported in this paper for the first time.
【Fund】: 教育部霍英东教育基金会高等院校青年教师基金资助项目(111046)
【CateGory Index】: R284.1
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