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《Chinese Traditional and Herbal Drugs》 2015-04
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Studies on chemical constituents in n-butanol extracts from epicarp of green fruit of Juglans mandshurica

YANG Bing-you;JIANG Yan-qiu;MENG Ying;LIU Yu-xin;LIU Zhao-xi;XIAO Hong-bin;WANG Xiao-li;ZHOU Yuan-yuan;College of Pharmacy, Heilongjiang University of Traditional Chinese Medicine;Experimental Center, Heilongjiang University of Traditional Chinese Medicine;College of adult education, Heilongjiang University of Traditional Chinese medicine;  
Objective To study the chemical constituents in n-butanol extracts from the epicarp of green fruits of Juglans mandshurica. Methods The compounds were isolated and purified by silica gel, ODS, Sephadex LH-20 columns, high preparative performance liquid chromatography, etc. And their structures were identified by spectral analysis. Results Fourteen compounds were obtained and identified as 5-O-cafffeoyl quinic acid butyl ester(1), 3,5-di-O-caffeoylquinic acid butyl ester(2), vanillic acid-4-O-β-D-(6′-O-galloyl) glucopyranoside(3), 4-hydroxy-2,6-dimethoxyphenol-1-O-β-D-glucopyranoside(4), 4,5,8-trihydroxy-α-tetralone-5-O-β-D-glucopyranoside(5), 1,4,8-trihydroxynaphthalene-1-O-β-D-glucopyranoside(6), 1,4,5-trihydroxynaphthalene-1,4-di-O-β-D-glucopyranoside(7), kaempferol-3-O-β-D-glucopyranoside(8), quercetin-3-O-β-D-glucopyranoside(9), quercitrin(10), myricitrin(11), afzelin(12), hyperin(13), and daucosterol(14). Conclusion Compounds 1—4 are isolated from the plants of Juglans L. for the first time, Compounds 5, 8—12 are isolated from the epicarps of J. mandshurica for the first time.
【Fund】: 国家自然科学基金资助项目(81202890);; 中国博士后特别资助(2014T70374);; 中国博士后面上资助(一等)(2013M530164);; 黑龙江省博士后基金(LBH-Z13195);; 黑龙江省教育厅科学技术研究项目(12541818);; 哈尔滨市青年科技创新人才项目(2013RFQXJ052);; 黑龙江中医药大学博士创新基金项目(B201103);; 黑龙江中医药大学优秀创新人才支持项目(051248)
【CateGory Index】: R284
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