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《Chinese Traditional and Herbal Drugs》 2015-12
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Study on HPLC-DAD-ELSD fingerprint of Polygoni Cuspidati Rhizoma et Radix

YANG Hang;YIN Chun-mei;JIAO Lian-qing;CAO Yang;YU Min;College of Chinese Medicine Materials,Jilin Agricultural University;Jilin Academy of Chinese Traditional Medicine;  
Objective To establish the chromatography fingerprint of Polygoni Cuspidati Rhizoma et Radix with hyphenated technique of HPLC-DAD-ELSD and to evaluate Polygoni Cuspidati Rhizoma et Radix from 10 different origins.Methods Luna C_(18)(2) column(250 mm × 4.6 mm,5 μm) was used.Mobile phase was acetonitrile-H_2O;Flow speed was 1.0 mL/min;Temperature of column was set at 35 ℃;Detective wavelength was at 254 nm;Injection volume was 10 μL.The temperature of drift tube was 109℃ and the flow speed was 3.0 L/min.Results The chromatography fingerprint of Polygoni Cuspidati Rhizoma et Radix from 10 different origins was established.In the chromatography fingerprint with HPLC-DAD of Polygoni Cuspidati Rhizoma et Radix,19 common peaks were demarcated and the similarities of Polygoni Cuspidati Rhizoma et Radix were between 0.938—0.993.In the chromatography fingerprint with HPLC-ELSD of Polygoni Cuspidati Rhizoma et Radix,14 common peaks were demarcated and the similarities of Polygoni Cuspidati Rhizoma et Radix were between 0.905—0.999.Polydatin,resveratrol,emodin-8-O-β-D-glucoside,physcion-8-O-β-D-glucoside,emodin,and physcion were identified.Conclusion The method is accurate and stable,which can be used as the evidence for the quality evaluation of Polygoni Cuspidati Rhizoma et Radix.
【Fund】: 吉林省科技厅课题“虎杖有效部位治疗高脂型糖尿病的研究”(201307026YY)
【CateGory Index】: R284.1;O657.72
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