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《Chinese Traditional and Herbal Drugs》 2015-16
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Chemical constituents in roots of Ilex kudingcha

HUANG Yan;ZHENG Jin-yan;YANG Gang-jin;LAI Mao-xiang;HUANG Yun-feng;LIU Bu-ming;Guangxi Key Laboratory of Tradtitional Chinese Medicine Quality Standards, Guangxi Institute of Traditional Medical and Pharmaceutical Sciences;  
Objective To investigate the chemical constituents in the roots of Ilex kudingcha. Methods Column chromatography such as silica gel, Sephadex LH-20, and preparative HPLC were used to isolate and purify the compounds. Spectroscopic methods like MS, 1H-NMR, and 13C-NMR, and physical constants were used to elucidate their structures. Results Nineteen compounds were isolated from 95% ethanol extracts of I. kudingcha, including α-aromadendrol-3β-palmitate(1), β-sitosterol(2), α-amyrin(3), 3-acetoxyolean-12-en-28-ol(4), 3-acetoxyurs-12-en-28-ol(5), 3β-acetoxyurs-12-en-28-al(6), oleanolic acid(7), ursolic acid(8), quercetin(9), daucosterol(10), ficuscarpanoside B(11), 3β-hydroxy-28-norurs-12,17-dien(12), siaresinolic acid(13), pomolic acid(14), α-D-glucose(15), 2,6-dimethoxy-benzoquinone(16), syringaldehyde(17), dibutyl phthalate(18), and ilexoside D(19). Conclusion Compounds 6, 12, 16—18 are isolated from the plant for the first time. Compound 11 is isolated from Ilex L. for the first time.
【Fund】: 广西中药质量标准研究重点实验室系统性研究课题(桂科重201209);; 国家科技支撑计划(2011BAI01B04);; 广西科学研究与技术开发计划(桂科重14124002-3)
【CateGory Index】: R284.1
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