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《Chinese Journal of Natural Medicines》 2005-01
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Chemical Constituents of Euphorbia antiquorum

SANG Yi-Shu,SHI Hai-Ming,JIA Liang,LIU Xue-Ting,MIN Zhi-Da* Department of Natural Medicinal Chemistry,China Pharmaceutical University,Nanjing 210009,China  
AIM:To study the chemical constituents of Euphorbia antiquorum L.METHOD:Column chromatography was used in the isolation procedure,while the structures of the isolated compounds were elucidated by spectral data.RESULT:Ten compounds were isolated and their structures were identified as glutinol(Ⅰ),taraxerol(Ⅱ),friedelanol(Ⅲ),stigmasterol(Ⅳ),23-cycloarten-3β,25-diol(Ⅴ),ent-13S-Hydroxy-16-atisene-3,14-dione(Ⅵ),6,7,8-trimethoxylcoumarin(Ⅶ),3,3′,4′-tri-O-methylellagic acid(Ⅷ),ent-kaurane-3-oxo-16β,17-diol(Ⅸ)and daucosterol(Ⅹ).CONCLUSION:Compound Ⅶ was firstly isolated from Euphorbia genus.Compounds Ⅰ,Ⅳ,Ⅴ,Ⅷ,Ⅸ and Ⅹ were obtained from this plant for the first time.The ~~ ~13 C NMR data of 23-cycloarten-3β,25-diol(Ⅴ)was reassigned based on their 2D NMR experiments.
【CateGory Index】: R284
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