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《Chinese Journal of Natural Medicines》 2011-02
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Chemical Constituents of Toona ciliata var. pubescens

LIU Yu-Bo1, CHENG Xiang-Rong1, QIN Jiang-Jiang1, YAN Shi-Kai1, JIN Hui-Zi1, ZHANG Wei-Dong1, 2 1School of Pharmacy, Shanghai Jiao Tong University, Shanghai 200240, China; 2Department of Phytochemistry, Second Military Medical University, Shanghai 200433, China  
AIM: To study the chemical constituents of the leaves and stems of Toona ciliata var. pubescens. METHOD: Silica gel column chromatography, Sephadex LH?20 gel column chromatography and preparative HPLC were employed for the isolation and purfication. The structures were identified on the basis of spectroscopic data and chemical evidence. RESULTS: 23 Compounds were isolated from the 95% ethanol extract of the leaves and stems of T. ciliata var. pubescens, and their structures were identified as siderin (1), 4, 6, 7-trimethoxy-5-methylcoumarin (2), isoscopoletin (3), scopoletin (4), 6, 7-dimethoxycoumarin (5), 7-hydroxy-6, 8-dimethoxycoumarin (6), dehydrodiconiferyl alcohol (7),-lariciresinol (8), thero-2, 3-bis-(4-hydroxy-3-methoxypheyl)-3-methoxy-propanol (9), cycloeucalenol (10), 8(14), 15-isopimaradiene-2, 3, 19-triol (11), 3S, 5R-dihydroxy-6R, 7-megstigmadien-9-one (12),-loliolide (13), (+)-catechin (14), dimethyl malate (15), diisobutyl phthalate (16), dibutyl phthalate (17), 1, 3, 5-trimethoxybenzene (18), syringic acid (19), syringaldehyde (20), vanillic acid (21), vanillin (22), and 3, 3′, 5, 5′-tetra-tert-butyl-2, 2′-dihydroxybiphenyl (23). CONCLUSION: All compounds were isolated from this plant for the first time.
【Fund】: supported by the Scientific Foundation of Shanghai Committee of Science and Technology (No. 09DZ1972200)~~
【CateGory Index】: R284.1
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