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《Chinese Journal of Hospital Pharmacy》 2011-11
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Study on the separation and purification of anthraquinone aglycone by polyamide resin

TAN Zhi-jian,LI Fen-fang,LIU Tai-ping(College of Chemistry and Chemical Engineering,Central South University,Hunan Changsha 410083,China)  
OBJECTIVE To optimize the method of separation and purification of total anthraquinone aglycone in aloe using polyamide resin.METHODS Using the adsorption ratio and desorption rate of anthraquinone aglycone as the evaluating quotas,orthogonal experimental designs and variance analysis were applied to optimize the manipulation parameters of polyamide resin,meanwhile the resin regeneration was studied.RESULTS The optimal exchange adsorption condition of polyamide resin was as follows: the flow velocity was 1.0 mL·s-1,solution concentration was 0.22 g·L-1 at pH 5.0,the dynamic saturated adsorption capacity reached to 10.5 mg·g-1.After being eluted with twice as much 10% ethanol and quadruple as much 80% ethanol,the desorption rate was 94.5%.CONCLUSION A technique for purification of anthraquinone aglycone was established,which provided the supporting for the industrialized production of aloe anthraquinone aglycone.The efficiency was demonstrated by analysis of aloe-emodin before and after purification using polyamide resin.
【Fund】: 国家自然基金项目(编号:20956001)
【CateGory Index】: R284.2
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